scholarly journals Wood Surface Changes of Heat-Treated Cunninghamia lanceolate Following Natural Weathering

Forests ◽  
2019 ◽  
Vol 10 (9) ◽  
pp. 791
Author(s):  
Xinjie Cui ◽  
Junji Matsumura

To quickly clarify the effect of heat treatment on weatherability of Cunninghamia lanceolate (Lamb.) Hook., we investigated the surface degradation under natural exposure. A comparison between heat-treated and untreated samples was taken based on surface color changes and structural decay at each interval. Over four weeks of natural exposure, multiple measurements were carried out. Results show that color change decreased in the order of 220 °C heat-treated > untreated > 190 °C heat-treated. The results also indicate that the wood surface color stability was improved via the proper temperature of thermal modification. Low vacuum scanning electron microscopy (LVSEM) results expressed that thermal modification itself had caused shrinking in the wood surface structure. From the beginning of the weathering process, the heat treatment affected the surface structural stability. After natural exposure, the degree of wood structure decay followed the pattern 220 °C heat-treated > 190 °C heat-treated > untreated. Therefore, when considering the impact on the structure, thermal modification treatment as a protective measure to prevent weathering was not an ideal approach and requires further improvement.

Author(s):  
Marios Kazasidis ◽  
Elisa Verna ◽  
Shuo Yin ◽  
Rocco Lupoi

AbstractThis study elucidates the performance of cold-sprayed tungsten carbide-nickel coating against solid particle impingement erosion using alumina (corundum) particles. After the coating fabrication, part of the specimens followed two different annealing heat treatment cycles with peak temperatures of 600 °C and 800 °C. The coatings were examined in terms of microstructure in the as-sprayed (AS) and the two heat-treated conditions (HT1, HT2). Subsequently, the erosion tests were carried out using design of experiments with two control factors and two replicate measurements in each case. The effect of the heat treatment on the mass loss of the coatings was investigated at the three levels (AS, HT1, HT2), as well as the impact angle of the erodents (30°, 60°, 90°). Finally, the response surface methodology (RSM) was applied to analyze and optimize the results, building the mathematical models that relate the significant variables and their interactions to the output response (mass loss) for each coating condition. The obtained results demonstrated that erosion minimization was achieved when the coating was heat treated at 600 °C and the angle was 90°.


2011 ◽  
Vol 189-193 ◽  
pp. 3891-3894
Author(s):  
Ya Min Li ◽  
Hong Jun Liu ◽  
Yuan Hao

The casting Fe3Al intermetallics were solidified in sodium silicate sand mould and permanent mould respectively to get different cooling rates. After heat treatment (1000°С/15 h homogenizing annealing + furnace cooling followed by 600°С/1 h tempering + oil quenching), the microstructure and properties of Fe3Al intermetallics were investigated. The results show that the heat-treated Fe3Al intermetallics at higher cooling rate has finer grained microstructure than lower cooling rate, and the lattice distortion increases due to the higher solid solubility of the elements Cr and B at higher cooling rate. The tensile strength and hardness of the Fe3Al intermetallics at higher cooling rate are slightly higher also. However, the impact power of intermetallics at higher cooling rate is 67.5% higher than that at lower cooling rate, and the impact fracture mode is also transformed from intercrystalline fracture at lower cooling rate to intercrystallin+transcrystalline mixed fracture at higher cooling rate.


2007 ◽  
Vol 344 ◽  
pp. 383-390 ◽  
Author(s):  
Marion Merklein ◽  
Uwe Vogt

Tailored Heat Treated Blanks (THTB) are blanks that exhibit locally different strength specifically optimized for the succeeding forming process. The strength distribution is set by a local, short-term heat treatment modifying the mechanical properties of the material. Hence, THTB allow enhancing forming limits significantly leading to shorter and more robust manufacture process chains. In order to qualify the use of THTB under quasi series conditions, the interdependencies of the blank’s local heat treatment and the entire process chain of the car body manufacture have to be analyzed. In this respect, the impact of a short-term heat treatment on the mechanical properties of AA6181PX, a commonly used aluminum alloy in today’s car bodies, was studied. Also the influence of a short-term heat treatment on the coil lubricant, usually already applied by the material supplier, was given a closer look. Based on these experiments process restrictions for the application of THTB in an industrial automotive environment were derived and a process window for the THTB design was set up. In conclusion, strategies were defined how to enhance the found process boundaries leading to a more robust process window.


BioResources ◽  
2021 ◽  
Vol 16 (3) ◽  
pp. 5574-5585
Author(s):  
Intan Fajar Suri ◽  
Jong Ho Kim ◽  
Byantara Darsan Purusatama ◽  
Go Un Yang ◽  
Denni Prasetia ◽  
...  

Color changes were tested and compared for heat-treated Paulownia tomentosa and Pinus koraiensis wood treated with hot oil or hot air for further utilization of these species. Hot oil and hot air treatments were conducted at 180, 200, and 220 °C for 1, 2, and 3 h. Heat-treated wood color changes were determined using the CIE-Lab color system. Weight changes of the wood before and after heat treatment were also determined. The weight of the oil heat-treated wood increased considerably but it decreased in air heat-treated wood. The oil heat-treated samples showed a greater decrease in lightness (L*) than air heat-treated samples. A significant change in L* was observed in Paulownia tomentosa. The red/green chromaticity (a*) of both wood samples increased at 180 and 200 °C and slightly decreased at 220 °C. The yellow/blue chromaticity (b*) in both wood samples increased at 180 °C, but it rapidly decreased with increasing treatment durations at 200 and 220 °C. The overall color change (ΔE*) in both heat treatments increased with increasing temperature, being higher in Paulownia tomentosa than in Pinus koraiensis. In conclusion, oil heat treatment reduced treatment duration and was a more effective method than air heat treatment in improving wood color.


2014 ◽  
Vol 2 ◽  
pp. 345-352 ◽  
Author(s):  
Cristina Marinela Olarescu ◽  
Mihaela Campean

Heat treatment is renowned as the most environmentally friendly process of dimensional stabilization that can be applied to wood, in order to make it suitable for outdoor uses. It also darkens wood color and improves wood durability. The intensity of heat treatment can be appreciated by means of two parameters: the color change occured in wood due to the high temperature, and the mass loss, which is a measure of the degree of thermal degradation. In order to find a mathematical correlation between these two parameters, an experimental study was conducted with four European wood species, which were heat-treated at 180°C and 200ºC, for 1-3 hours, under atmosheric pressure.The paper presents the results concerning the color changes and mass losses recorded for the heat-treated wood samples compared to untreated wood.  For all four species, the dependency between the color change and the mass loss was found to be best described by a logarithmic regression equation with R2 of 0.93 to 0.99 for the soft species (spruce, pine and lime), and R2 of 0.77 for beech. The results of this study envisage to simplify the assessment procedure of the heat treatment efficiency, by only measuring the color – a feature that is both convenient and cost-effective. 


1990 ◽  
Vol 112 (1) ◽  
pp. 116-123 ◽  
Author(s):  
W. J. Mills ◽  
L. D. Blackburn

Heat-to-heat and product-form variations in the JIC fracture toughness for Alloy 718 were characterized at 24, 427, and 538°C using the multiple-specimen JR-curve method. Six different material heats along with three product forms from one of the heats were tested in the modified heat treated condition. This heat treatment was developed at Idaho National Engineering Laboratory to improve the impact toughness for Alloy 718 weldments, but it has also been found to enhance the fracture resistance for the base metal. Statistical analysis of test results revealed four distinguishable JIC levels with mean toughness levels ranging from 87 to 190 kJ/m2 at 24°C. At 538°C, JIC values were 15 to 20 percent lower than room temperature toughness levels. Minimum expected values of JIC (ranging from 72 kJ/m2 at 24°C to 48 kJ/m2 at 538°C) and dJR/da (27 MPa at 24 to 538°C) were established based on tolerance intervals bracketing 90 percent of the lowest JIC and dJR/da populations at a 95 percent confidence level. Metallographic and fractographic examinations were performed to relate key microstructural features and operative fracture mechanisms to macroscopic properties.


Forests ◽  
2019 ◽  
Vol 10 (2) ◽  
pp. 189 ◽  
Author(s):  
Vlastimil Borůvka ◽  
Roman Dudík ◽  
Aleš Zeidler ◽  
Tomáš Holeček

This work deals with the quality of birch (Betula pendula) wood from different sites and the impact of heat treatment on it. Two degrees of heat treatment were used, 170 °C and 190 °C. The resulting property values were compared with reference to untreated wood samples. These values were wood density, compressive strength, modulus of elasticity (MOE), bending strength (MOR), impact bending strength (toughness), hardness, swelling, limit of hygroscopicity, moisture content and color change. It was supposed that an increase in heat-treatment temperature could reduce strength properties and, adversely, lead to better shape and dimensional stability, which was confirmed by experiments. It was also shown that the properties of the wood before treatment affected their condition after heat treatment, and that the characteristic values and variability of birch properties from 4 sites, 8 stems totally, were reflected in the properties of the heat-treated wood. Values of static MOR were the exception, where the quality of the input wood was less significant at a higher temperature, and this was even more significant in impact bending strength, where it manifested at a lower temperature degree. Impact bending strength also proved to be significantly negatively affected by heat treatment, about 48% at 170 °C, and up to 67% at 190 °C. On the contrary, the most positive results were the MOE and hardness increases at 170 °C by about 30% and about 21%, respectively, with a decrease in swelling at 190 °C by about 31%. On the basis of color change and other ascertained properties, there is a possibility that, after suitable heat treatment, birch could replace other woods (e.g., beech) for certain specific purposes, particularly in the furniture industry.


2017 ◽  
Vol 24 (Supp02) ◽  
pp. 1850028
Author(s):  
BINFENG LU ◽  
YUNXIA CHEN ◽  
MENGJIA XU

(Cr, Fe)7C3/[Formula: see text]-Fe composite layer has been in situ synthesized on a low carbon steel surface by vacuum electron beam VEB irradiation. The synthesized samples were then subdued to different heat treatments to improve their impaired impact toughness. The microstructure, impact toughness and wear resistance of the heat-treated samples were studied by means of optical microscope (OM), X-ray diffraction (XRD), scanning electron microscope (SEM), microhardness tester, impact test machine and tribological tester. After heat treatment, the primary and eutectic carbides remained in their original shape and size, and a large number of secondary carbides precipitated in the iron matrix. Since the Widmanstatten ferrite in the heat affected zone (HAZ) transformed to fine ferrite completely, the impact toughness of the heat-treated samples increased significantly. The microhardness of the heat-treated samples decreased slightly due to the decreased chromium content in the iron matrix. The wear resistance of 1000[Formula: see text]C and 900[Formula: see text]C heat-treated samples was almost same with the as-synthesized sample. While the wear resistance of the 800[Formula: see text]C heat-treated one decreased slightly because part of the austenite matrix had transformed to ferrite matrix, which reduced the bonding of carbides particulates.


Holzforschung ◽  
2014 ◽  
Vol 68 (2) ◽  
pp. 185-193 ◽  
Author(s):  
Christian Brischke ◽  
Kathrin A. Sachse ◽  
Christian R. Welzbacher

Abstract A model has been developed aiming at the description of the effect of thermal modification on the electrical conductivity of wood. The intention was to calculate the moisture content (MC) of thermally modified timber (TMT) through the parameters electrical resistance R, wood temperature T, and CIE L*a*b* color data, which are known to correlate well with the intensity of a heat treatment. Samples of Norway spruce (Picea abies Karst.) and beech (Fagus sylvatica L.) samples were thermally modified in laboratory scale at 11 different heat treatment intensities and the resistance characteristics of the samples were determined. Within the hygroscopic range, a linear relationship between the resistance characteristics and the mass loss (ML) through the heat treatment was established. Based on this, a model was developed to calculate MC from R, T, and ML. To validate this model, color values of 15 different TMTs from industrial production were determined for estimation of their ML and fed into the model. MC of the 15 arbitrarily heat-treated TMTs was calculated with an accuracy of ±3.5% within the hygroscopic range. The material-specific resistance characteristics based on experimental data led to an accuracy of ±2.5%.


2017 ◽  
Vol 7 (3) ◽  
pp. 15-21 ◽  
Author(s):  
Михаил Ермоченков ◽  
Mihail Ermochenkov ◽  
Андрей Хроменко ◽  
Andrey Khromenko

Heat treatment is widely used to improve the properties of wood. Such processes include drying and thermal modification. Thermal modification is heating wood without oxygen, accompanied by heat destruction. Thermally modified wood can be used as structural and finishing materials. This puts the task of determining its thermal and physical, physical and chemical, biological, and ornamental properties and their change during heat treatment. The article presents the results of experimental and computational studies of color characteristics of the wood of birch, their change in the process of thermal modification. Thermal decomposition is a complicated multi-stage physical and chemical process. Thermal decomposition of material causes changes in its composition, structure, accompanied by alterations of its properties. Wood can be considered as a multicomponent composite material, consisting of hemicellulose, cellulose, lignin and other components. Each component decomposes in the temperature range that causes the multistage process of thermal degradation. The degree of thermal degradation of the material is determined by the kinetics of occurrence of each stage and the degree of its perfection. Thermal decomposition kinetics of wood can be determined by the results of thermal and gravimetric experiments. In the article the model of determining the color characteristics of wood as a function of the degree of completion of individual stages of thermal degradation is suggested. Model of decomposition of color for RGB components is used for identifying. Color identification of the samples of original birch wood in RGB coordinates was performed. The parameters of thermal effects, allowing to obtain wood with given degree of thermal decomposition are defined. Heat treatment of samples and identification of their color is made. The dependence of RGB parameters from time and intensity of heat treatment is studied. Empirical relations to determine the identifying characteristics of color, as a function of the degree of completion of stages of thermal destruction, in RGB and LAB systems are obtained in explicit form.


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