scholarly journals Oxidation of High Yield Strength Metals Tungsten and Rhenium in High-Pressure High-Temperature Experiments of Carbon Dioxide and Carbonates

Crystals ◽  
2019 ◽  
Vol 9 (12) ◽  
pp. 676 ◽  
Author(s):  
Raquel Chuliá-Jordán ◽  
David Santamaría-Pérez ◽  
Tomás Marqueño ◽  
Javier Ruiz-Fuertes ◽  
Dominik Daisenberger
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Yield Strength ◽  
High Pressures ◽  
Chemical Reactivity ◽  
High Yield ◽  
Reaction Products ◽  
High Yield Strength ◽  
High Pressure High Temperature ◽  
Diamond Anvil

The laser-heating diamond-anvil cell technique enables direct investigations of materials under high pressures and temperatures, usually confining the samples with high yield strength W and Re gaskets. This work presents experimental data that evidences the chemical reactivity between these refractory metals and CO2 or carbonates at temperatures above 1300 °Ϲ and pressures above 6 GPa. Metal oxides and diamond are identified as reaction products. Recommendations to minimize non-desired chemical reactions in high-pressure high-temperature experiments are given.

Advances in Computation of Temperature-Pressure Phase Diagrams of High-Pressure Nitrides

2008 ◽  
Vol 403 ◽  
pp. 77-80 ◽  
Author(s):  
Peter Kroll
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Elevated Temperature ◽  
Total Energy ◽  
Phase Diagrams ◽  
High Pressures ◽  
First Principle ◽  
Energy Calculations ◽  
High Pressure High Temperature ◽  
Pressure Phase

A combination of first-principle and thermochemical calculations is applied to compute the phase diagrams of rhenium-nitrogen and of ruthenium-nitrogen at elevated temperature and high pressure. We augment total energy calculations with our approach to treat the nitrogen fugacity at high pressures. We predict a sequential nitridation of Re at high-pressure/high-temperature conditions. At 3000 K, ReN will form from Re and nitrogen at about 32 GPa. A ReN2 with CoSb2-type structure may be achieved at pressures exceeding 50 GPa at this temperature. Marcasite-type RuN2 will be attainable at 3000 K at pressures above 30 GPa by reacting Ru with nitrogen.

Cryogenic gas loading in a Mao–Bell-type diamond anvil cell for high pressure-high temperature investigations

2008 ◽  
Vol 79 (7) ◽  
pp. 076103 ◽  
Author(s):  
M. Sekar ◽  
N. R. Sanjay Kumar ◽  
P. Ch. Sahu ◽  
N. V. Chandra Shekar ◽  
N. Subramanian
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Diamond Anvil Cell ◽  
High Pressure High Temperature ◽  
Diamond Anvil

Structural stability of WS2 under high pressure

2014 ◽  
Vol 28 (25) ◽  
pp. 1450168 ◽  
Author(s):  
Nirup Bandaru ◽  
Ravhi S. Kumar ◽  
Jason Baker ◽  
Oliver Tschauner ◽  
Thomas Hartmann ◽  
...  
Keyword(s):  
Crystal Structure ◽  
High Pressure ◽  
High Temperature ◽  
Structural Changes ◽  
High Pressures ◽  
Structural Phase ◽  
X Ray Diffraction ◽  
X Ray ◽  
Diamond Anvil ◽  
Heating Up

Structural behavior of bulk WS 2 under high pressure was investigated using synchrotron X-ray diffraction and diamond anvil cell up to 52 GPa along with high temperature X-ray diffraction and high pressure Raman spectroscopy analysis. The high pressure results obtained from X-ray diffraction and Raman analysis did not show any pressure induced structural phase transformations up to 52 GPa. The high temperature results show that the WS 2 crystal structure is stable upon heating up to 600°C. Furthermore, the powder X-ray diffraction obtained on shock subjected WS 2 to high pressures up to 10 GPa also did not reveal any structural changes. Our results suggest that even though WS 2 is less compressible than the isostructural MoS 2, its crystal structure is stable under static and dynamic compressions up to the experimental limit.

scholarly journals Carbide Formation in Refractory Mo15Nb20Re15Ta30W20 Alloy under a Combined High-Pressure and High-Temperature Condition

Entropy ◽  
2020 ◽  
Vol 22 (7) ◽  
pp. 718
Author(s):  
Congyan Zhang ◽  
Uttam Bhandari ◽  
Congyuan Zeng ◽  
Huan Ding ◽  
Shengmin Guo ◽  
...  
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Mechanical Performance ◽  
Ambient Pressure ◽  
High Entropy Alloy ◽  
Carbide Formation ◽  
High Entropy ◽  
Temperature Conditions ◽  
High Pressure High Temperature ◽  
Diamond Anvil

In this work, the formation of carbide with the concertation of carbon at 0.1 at.% in refractory high-entropy alloy (RHEA) Mo15Nb20Re15Ta30W20 was studied under both ambient and high-pressure high-temperature conditions. The x-ray diffraction of dilute carbon (C)-doped RHEA under ambient pressure showed that the phases and lattice constant of RHEA were not influenced by the addition of 0.1 at.% C. In contrast, C-doped RHEA showed unexpected phase formation and transformation under combined high-pressure and high-temperature conditions by resistively employing the heated diamond anvil cell (DAC) technique. The new FCC_L12 phase appeared at 6 GPa and 809 °C and preserved the ambient temperature and pressure. High-pressure and high-temperature promoted the formation of carbides Ta3C and Nb3C, which are stable and may further improve the mechanical performance of the dilute C-doped alloy Mo15Nb20Re15Ta30W20.

Friction-wear failure mechanism of tubing strings used in high-pressure, high-temperature and high-yield gas wells

Wear ◽  
2021 ◽  
Vol 468-469 ◽  
pp. 203576
Author(s):  
Xiaoqiang Guo ◽  
Jun Liu ◽  
Liming Dai ◽  
Qingyou Liu ◽  
Dake Fang ◽  
...  
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Failure Mechanism ◽  
High Yield ◽  
Gas Wells ◽  
High Pressure High Temperature

Wear Experiment and Influencing Factors Analysis of 13Cr-L80 Tubing String in High-Pressure, High-Temperature and High-Yield Gas Wells

2021 ◽  
Vol 1026 ◽  
pp. 169-175
Author(s):  
Xiao Qiang Guo ◽  
Jun Liu ◽  
Liang Huang ◽  
An Chao Wei ◽  
Da Ke Fang
Keyword(s):  
High Pressure ◽  
High Temperature ◽  
Service Life ◽  
Longitudinal Vibration ◽  
Control Variable ◽  
Contact Load ◽  
High Yield ◽  
Gas Wells ◽  
High Pressure High Temperature ◽  
Tubing String

Due to wear failures caused by tubing string vibrations in high-pressure, high-temperature and high-yield (3H) gas wells, a wear experiment was performed on the 13Cr-L80 tubing string. The influence of contact load, friction frequency, and reciprocating stroke length on the wear characteristics of the tubing string were effectively analyzed using the control variable method. The results demonstrate that, the wear patterns of the tubing-casing were primarily abrasive and adhesive wears, with minimal corrosion wear. The wear amount of tubing increases linearly with the increase of contact load and reciprocating stroke, but increases nonlinearly with the increase of friction frequency, and the friction coefficient of tubing string do not change with the increase of contact load, friction frequency and reciprocating stroke. In-field operations, the service life of the tubing string in 3H gas wells can be effectively augmented by reducing the contact load and longitudinal vibration displacement of the tubing-casing, maintaining the vibration frequency of the tubing string below 1.5 Hz. These results provide useful guidance for designing and implementing approaches to improve the service life of tubing strings in high-yield gas wells.

REPUBLIC HP 9-4-20

Alloy Digest ◽  
1971 ◽  
Vol 20 (12) ◽  
Keyword(s):  
Fracture Toughness ◽  
Corrosion Resistance ◽  
High Temperature ◽  
Yield Strength ◽  
Physical Properties ◽  
Surface Treatment ◽  
Heat Treating ◽  
High Yield ◽  
High Yield Strength ◽  
Temperature Performance

Abstract REPUBLIC HP 9-4-20 is designed especially for applications requiring optimum combinations of relatively high yield strength and toughness with good weldability. This alloy is capable of providing 180,000 psi yield strength in combination with a Charpy V-notch value of 50 ft-lb at 75 F in plate thicknesses up to at least 4 inches. This datasheet provides information on composition, physical properties, hardness, elasticity, and tensile properties as well as fracture toughness, creep, and fatigue. It also includes information on low and high temperature performance, and corrosion resistance as well as forming, heat treating, machining, joining, and surface treatment. Filing Code: SA-270. Producer or source: Republic Steel Corporation.

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