scholarly journals Development of a Stainless Austenitic Nitrogen-Alloyed CrMnNiMo Spring Steel

Crystals ◽  
2019 ◽  
Vol 9 (9) ◽  
pp. 456 ◽  
Author(s):  
Christina Schröder ◽  
Marco Wendler ◽  
Thilo Kreschel ◽  
Olena Volkova ◽  
Andreas Weiß

The generation of a nickel-reduced, stainless spring steel strip with a thickness of 0.2 mm, producible under industrial conditions, is the aim of a transfer project together with the Institute of Metal Forming/TU BAF and the Auerhammer Metallwerk GmbH within the DFG Collaborative Research Centre (CRC) 799. The spring steel strip should exhibit a tensile strength of ≥1700 MPa in work-hardened and partitioned state. The mechanical and corrosive properties of the steel strip should be equal or better than those given for 1.4310 steel (AISI 301). The article presents the results of laboratory alloys focused on the design of steel strips, which meet the requirements for a cost-effective production. The results presented relate to steel design, microstructure formation, temperature-dependent mechanical properties, and corrosion resistance. Four alloys of the type X5CrMnNiMoN16-x-4 with manganese contents of approximately 2 to 6 wt.-percent were investigated. The austenitic steel X5CrMnNiMoN16-4-4 with TRIP/TWIP effect was selected for deformation and partitioning treatments. Its deformation-induced α’-martensite formation significantly contributes to the work hardening of the steel. A short-time annealing treatment (partitioning) further increases the strength properties.

Crystals ◽  
2020 ◽  
Vol 10 (5) ◽  
pp. 392
Author(s):  
Christina Schröder ◽  
Marco Wendler ◽  
Olena Volkova ◽  
Andreas Weiß

The article presents the mechanical properties of the austenitic stainless steel X5CrMnNiMoN16-4-4 after deformation by cold rolling and subsequent short-term tempering (deformation and partitioning (D&P) treatment). Tensile strengths of 1700–900 MPa and beyond were achieved both after work hardening and in the D&P-treated strip. The initial state of austenite in terms of grain size and pre-strengthening, as well as the selected cold rolling temperature significantly influenced the deformation-induced formation of α’ martensite and thus the flow and hardening behavior of the steel. The usage of two different rolling temperature regimes showed that the strength properties in the cold strip can be specifically adjusted. Lower deformation-induced martensite fractions enabled a larger thickness reduction of the strip without increasing the rolling force, while high deformation-induced martensite fractions led to strong hardening at low deformation levels. The D&P-treatment permits the strength of the cold-rolled strip with a predominantly austenitic microstructure to be increased to the required level. The total elongation of such a D&P strip was well over 2%. The D&P treatment of the spring steel strip is a cost-effective alternative to conventional tempering treatment.


2021 ◽  
Vol 23 (1) ◽  
Author(s):  
Lisa Lindner ◽  
Anja Weiß ◽  
Andreas Reich ◽  
Siegfried Kindler ◽  
Frank Behrens ◽  
...  

Abstract Background Clinical data collection requires correct and complete data sets in order to perform correct statistical analysis and draw valid conclusions. While in randomized clinical trials much effort concentrates on data monitoring, this is rarely the case in observational studies- due to high numbers of cases and often-restricted resources. We have developed a valid and cost-effective monitoring tool, which can substantially contribute to an increased data quality in observational research. Methods An automated digital monitoring system for cohort studies developed by the German Rheumatism Research Centre (DRFZ) was tested within the disease register RABBIT-SpA, a longitudinal observational study including patients with axial spondyloarthritis and psoriatic arthritis. Physicians and patients complete electronic case report forms (eCRF) twice a year for up to 10 years. Automatic plausibility checks were implemented to verify all data after entry into the eCRF. To identify conflicts that cannot be found by this approach, all possible conflicts were compiled into a catalog. This “conflict catalog” was used to create queries, which are displayed as part of the eCRF. The proportion of queried eCRFs and responses were analyzed by descriptive methods. For the analysis of responses, the type of conflict was assigned to either a single conflict only (affecting individual items) or a conflict that required the entire eCRF to be queried. Results Data from 1883 patients was analyzed. A total of n = 3145 eCRFs submitted between baseline (T0) and T3 (12 months) had conflicts (40–64%). Fifty-six to 100% of the queries regarding eCRFs that were completely missing were answered. A mean of 1.4 to 2.4 single conflicts occurred per eCRF, of which 59–69% were answered. The most common missing values were CRP, ESR, Schober’s test, data on systemic glucocorticoid therapy, and presence of enthesitis. Conclusion Providing high data quality in large observational cohort studies is a major challenge, which requires careful monitoring. An automated monitoring process was successfully implemented and well accepted by the study centers. Two thirds of the queries were answered with new data. While conventional manual monitoring is resource-intensive and may itself create new sources of errors, automated processes are a convenient way to augment data quality.


Water ◽  
2021 ◽  
Vol 13 (5) ◽  
pp. 661
Author(s):  
Luigi Piazzi ◽  
Stefano Acunto ◽  
Francesca Frau ◽  
Fabrizio Atzori ◽  
Maria Francesca Cinti ◽  
...  

Seagrass planting techniques have shown to be an effective tool for restoring degraded meadows and ecosystem function. In the Mediterranean Sea, most restoration efforts have been addressed to the endemic seagrass Posidonia oceanica, but cost-benefit analyses have shown unpromising results. This study aimed at evaluating the effectiveness of environmental engineering techniques generally employed in terrestrial systems to restore the P. oceanica meadows: two different restoration efforts were considered, either exploring non-degradable mats or, for the first time, degradable mats. Both of them provided encouraging results, as the loss of transplanting plots was null or very low and the survival of cuttings stabilized to about 50%. Data collected are to be considered positive as the survived cuttings are enough to allow the future spread of the patches. The utilized techniques provided a cost-effective restoration tool likely affordable for large-scale projects, as the methods allowed to set up a wide bottom surface to restore in a relatively short time without any particular expensive device. Moreover, the mats, comparing with other anchoring methods, enhanced the colonization of other organisms such as macroalgae and sessile invertebrates, contributing to generate a natural habitat.


2010 ◽  
Vol 139-141 ◽  
pp. 594-599
Author(s):  
Yan Qiu Zhang ◽  
Shu Yong Jiang ◽  
Yu Feng Zheng

The spring steel strip 50CrVA which is cold rolled was applied to manufacture the diaphragm of the automotive horn by means of sheet metal forming. The combination of the experiments with back-propagation artificial neural network (BPANN) is used to solve the springback problem of the diaphragm. Experiments have shown that a 4-8-1 BPANN is able to predict the springback of the diaphragm successfully, and the network is able to model the relationship between the springback of the diaphragm and the process parameters rationally. BPANN simulation results and experimental ones have shown that the springback of the diaphragm is particularly influenced by such parameters as blank thickness, Young’s modulus, punch radius and yield ratio. Furthermore, the springback of the diaphragm decreases with the increase of blank thickness and Young’s modulus, but increases with the increase of punch radius and yield ratio.


2012 ◽  
Vol 2012 ◽  
pp. 1-7 ◽  
Author(s):  
Vidya S. Taur ◽  
Rajesh A. Joshi ◽  
Ramphal Sharma

The Ag-doped nanostructured CdS thin films are grown by simple, cost effective chemical ion exchange technique at room temperature on ITO-coated glass substrate. These as grown thin films are annealed at 100, 200, 300, and 400°C in air atmosphere for 1 hour. To study the effect of annealing on physicochemical and optoelectronic properties, these as grown and annealed thin films are characterized for structural, compositional, morphological, optical, and electrical properties. X-ray diffraction (XRD) pattern reveals polycrystalline nature of these thin films with increase in crystallite size from 6.4 to 11.2 nm, from XRD the direct identification of Ag doping in CdS thin films cannot be judged, while shift in characteristics peak position of CdS is observed. The Raman spectrum represents increase in full width at half maxima and intensity of characteristic peak, confirming the material modification upon annealing treatment. Presence of Cd, Ag, and S in energy dispersive X-ray analysis spectra (EDAX) confirms expected elemental composition in thin films. Scanning electron microscopy (SEM) images represent grain growth and agglomeration upon annealing. Red shift in optical absorbance strength and energy band gap values from 2.28 to 2.14 eV is obtained.I-Vresponse obtained from as grown and annealed thin films shows an enhancement in photosensitivity from 72% to 96% upon illumination to 100 mW/cm2light source.


2009 ◽  
Vol 63 (1) ◽  
pp. 57-60
Author(s):  
Aleksandra Petrovic ◽  
Slavica Glisic

In the production of pocket type electrodes for Ni-Cd batteries perforation of proper steel strips and then nickel platting of perforated steel strips were made. In the nickel platting process, the organic solvent, trichloroethylene, has previously been used for cleaning. Due to the carcinogenic nature of trichloroethylene and the many operations previously required during cleaning, it was considered to do cleaning of perforated steel strips without use of the mentioned organic solvent. In the purpose of elimination of trichloroethylene from the cleaning process of perforated steel strips, the tests of perforation of steel strips with use of oils of different viscosity were made. It was shown that there was no dysfunction during the work of the perforation plants, meaning there was no additional heating of the strips, deterring of the steel filings, nor excessive wearing of the perforation apparatus. The perforation percent was the same irrelevant of the viscosity of the used oil. Before being perforated using the oils with different viscosity, the nickel platting steel strips were cleaned in different degreasers (based on NaOH as well as on KOH). It was shown that efficient cleaning without the use of trichloroethylene is possible with the use of oil with smaller viscosity in the perforated steel strips process and the degreaser based on KOH in the cleaning process, before nickel platting. It also appeared that the alkali degreaser based on KOH was more efficient, bath corrections were made less often and the working period of the baths was longer, which all in summary means less quantity of chemicals needed for degreasing of perforated steel strips.


2008 ◽  
Vol 1129 ◽  
Author(s):  
Shannon Patrick Farrell ◽  
Patti E. Quigley ◽  
Kyle J. Avery ◽  
Tim D. Hatchard ◽  
Stephanie E Flynn ◽  
...  

AbstractRecently, low-cost processing approaches that produce textured thin bodies have engendered interest as cost-effective approaches for fabrication of magnetostrictive Fe-Ga alloys. In particular, wire-forming methods that strictly control the solidification direction could lead to some measure of crystallographic texture control. This is critical for development of large magnetostriction in polycrystals and for use of the alloys in actuators, sensors, energy harvesters and other systems. Magnetostrictive Fe-Ga wires have been prepared using an innovative cost-effective approach – based on the Taylor wire method – that combines rapid solidification and deformation processes. The procedure for making magnetostrictive wires is discussed and the wires are evaluated in terms of microstructure, crystallographic texture and magnetostriction. Results show that the Taylor-based approach is an effective and versatile means to draw 1-3 mm diameter textured Fe-Ga wire. Experimentation on the influence of drawing technique and quench conditions on texture development resulted with production of a strong <100> fiber texture in the Fe-Ga wire. Magnetostriction measurements, in the absence of prestress, indicated a maximum magnetostriction of ˜165 ppm in a saturation field of less than 200 mTesla. This is considered a significant strain for bulk polycrystalline Fe-Ga alloys without a pre-stress or a stress-annealing treatment. The unique properties of wires made with the Taylor-based approach coupled with the low intrinsic cost make this an attractive approach for production of textured magnetostrictive wire for a variety of applications.


2021 ◽  
Author(s):  
N. González Díez ◽  
S. P. C. Belfroid ◽  
T. Iversen Solfeldt ◽  
C. Kristiansen

Abstract Flow-induced pulsations (FLIP) are pressure oscillations generated inside of flexibles used in dry gas applications that can cause unacceptable vibration levels and eventually failure of equipment. Because of the design of inner layer of the flexibles, the carcass, the frequency of the pulsations is high, potentially leading to fatigue failures of adjacent structures in a relatively short time. The traditional carcass is made of a steel strip formed into an interlocked s-shape in a series of preforming and winding steps. To enable bending of the pipe, gaps are present between each winding with a shape that can cause FLIP. The gaps can be reduced, and the profiles optimized, but they will always be able to generate FLIP at a certain gas velocity. To remove the risk of FLIP in dry gas projects and ensure that operator does not get operational constraints, an alternative carcass design has been developed. This is essentially a conventional agraff carcass but with an additional cover strip to close the gap, making the resulting carcass nearly smooth bore in nature. With a smooth bore this carcass can be used for flexibles which have a risk of FLIP or to produce pipes with a lower internal roughness. This alternative design can be manufactured and can therefore build on the large manufacturing and design experience of the traditional strip carcass. This alternative carcass technology is to undergo a full qualification process, in which the risk of flow induced pulsations is an essential component. With the investigated alternative carcass design, the cavities present in the traditional agraff designs are covered. It is expected that the risk due to the appearance of FLIP is therefore eliminated. Theoretical analysis, numerical simulations and scaled experiments are used to explore the risk for the alternative technology to create FLIP. The theoretical analysis is based on existing knowledge and literature. The numerical simulations and scaled tests are done to generate direct evidence for the end statements resulting from the qualification process. Numerical simulations follow the power balance method presented by the same authors in earlier papers. The same applies to the techniques used for the scaled tests. The main outcome of the qualification presented here are the pressure drop performance and the anti-FLIP capabilities of the design. The new design performs significantly better than the nominal design carcass for the same purpose. The pressure drop coefficients found are close to those expected for a normal, non-corrugated pipe, and thus the recommendation given by the API 17J standard does not apply to this design. The pressure drop coefficient is dependent on the installation direction of the flexible with respect to the flow. No signs of FLIP are found for the nominal design of the investigated carcass technology. This is the case for either installation direction. This is explained from a theoretical point of view, but also numerical and experimental evidence are provided.


2019 ◽  
Vol 43 (1) ◽  
Author(s):  
Aruna Jyothi Kora

Abstract Background In India, the sand roasting technique is widely used by street food vendors, villagers and cottage industries for making various value-added food products from different cereals, millets and legumes. The traditionally produced sand-roasted products are commonly utilized as ready to eat snacks or for the preparation of various other snacks. Results During the high-temperature short-time treatment of sand roasting, the produced products are bestowed with characteristics such as higher puffing, crispiness, volume, and improved color, aroma, flavor and texture. In terms of nutrition, the roasting process enhances the carbohydrate and protein digestibility, β-glucan extractability, levels of dietary fiber, minerals, and antioxidants and reduces the inherent antinutrients levels in cereals and legumes. In addition, the complete destruction of seed microflora enhances the shelf life and thus consumer acceptance. The sand-roasted products act as prebiotic dietary fiber and serves as an alternative to polished grains for the consumers. Thus, the simplest, inexpensive, traditional sand roasting method of dry heat application is used for making precooked ready to eat weaning foods and preparation of cost-effective dietary pediatric and geriatric formulations. The technique is also employed for roasting various beans, fryums, nut, and pulse decortication and as a pretreatment process for tamarind kernel powder production, while the sand baking method is widely used for baking cakes, vegetables, meat, fish, eggs and starchy tubers. Conclusions The techniques of sand roasting and baking are gaining importance as cheap, effective, oil-free, healthier ways of cooking. However, further studies are needed on micronutrient availability and functional food development for community nutritional disorders. Also, the residual silica levels and difficult working environment mandates the development of energy-efficient and high-output-orientated technologies such as continuous, microwave, and fluidized bed roasters.


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