scholarly journals Interfacial Microstructure Characteristics and Mechanical Properties of a Press Bonded Ti–5Al–2Sn–2Zr–4Mo–4Cr Alloy

Crystals ◽  
2021 ◽  
Vol 11 (11) ◽  
pp. 1395
Author(s):  
Hong Li ◽  
Miaoquan Li
Keyword(s):  
Grain Size ◽  
Shear Strength ◽  
Volume Fraction ◽  
Base Alloy ◽  
Interfacial Microstructure ◽  
Quantitative Detection ◽  
Boundary Misorientation ◽  
Α Phase ◽  
Grain Boundary Misorientation ◽  
Press Bonding

The microstructure evolution characteristics and the shear strength of bond and base alloys were investigated during the press bonding of the Ti–5Al–2Sn–2Zr–4Mo–4Cr alloy. The quantitative detection of the interfacial void shows that the interfacial voids shrunk gradually with time and a bond free of voids could be obtained at the time above 10 min. The microstructure of the base alloy shows that the primary α phase tends to be equiaxed because of the increase in plastic deformation and the variation in the volume fraction and grain size of the primary α phase that are complicated with time. The grain boundary misorientation characteristics in bond and base alloys are not consistent. However, they tend to be comparable over time. The shear strength of bond and base alloys at different times was explained and compared. The compared results indicate that the enhanced strength of the bond is mainly due to the increase in the bonded area. However, the strength of the bond decreases slightly because of the slight coarsening of the grain size and the decrease in the volume fraction of the primary α phase at the time more than 20 min. The shear strength of the bond and base alloys tends to be highest and close at 10 min.

Influence of Isothermal Forging Temperature on Microstructure and Tensile Properties of Ti-5.8Al-4.0Sn-4.0Zr-0.7Nb-0.4Si-1.5Ta Near-α Titanium Alloy

2010 ◽  
Vol 97-101 ◽  
pp. 153-157
Author(s):  
Tao Wang ◽  
Hong Zhen Guo ◽  
Jian Hua Zhang ◽  
Ze Kun Yao
Keyword(s):  
Grain Size ◽  
Tensile Strength ◽  
Titanium Alloy ◽  
Tensile Properties ◽  
Room Temperature ◽  
Volume Fraction ◽  
Constant Strain Rate ◽  
Isothermal Forging ◽  
Α Phase ◽  
Transus Temperature

The microstructures and room temperature and 600°C tensile properties of Ti-5.8Al-4.0Sn-4.0Zr-0.7Nb -0.4Si-1.5Ta alloy after isothermal forging have been studied. The forging temperature range was from 850°C to 1075°C, and the constant strain rate of 8×10-3/S-1 was adopted. With the increase of forging temperature, the volume fraction of primary α phase decreased and the lamellar α phase became thicker when the temperatures were in range of 850°C -1040°C; The grain size became uneven and the α phase had different forms when the forging temperature was 1040°C and 1075°C respectively; The tensile strength was not sensitive to the temperature and the most difference was within 20MPa. Tensile strength and yield strength attained to the maximum when temperature was 1020°C; the ductility decreased with the increase of forging temperature, and this trend became more obvious if forging temperature was above the β-transus temperature.

Characterization of Zinalco Alloy Superplastically Deformed Using Orientation Imaging Microscopy

2009 ◽  
Vol 1242 ◽  
Author(s):  
Ramos A. Mitsuo ◽  
Martínez F. Elizabeth ◽  
Negrete S. Jesús ◽  
Torres-Villaseñor G.
Keyword(s):  
Grain Size ◽  
Grain Boundary ◽  
Grain Boundaries ◽  
Superplastic Deformation ◽  
Orientation Imaging Microscopy ◽  
Grain Boundary Sliding ◽  
Boundary Misorientation ◽  
Average Grain Size ◽  
Grain Boundary Misorientation ◽  
Misorientation Angles

ABSTRACTZinalco alloy (Zn-21mass%Al-2mass%Cu) specimens were deformed superplastically with a strain rate (ε) of 1×10-3 s-1 at homologous temperature (TH) of 0.68 (5 ). It was observed neck formation that indicate nonhomegeneus deformation. Grain size and grain boundaries misorientation changes, due superplastic deformation, were characterized by Orientation Imagining Microscopy (OIM) technique. It was studied three regions in deformed specimens and the results were compared with the results for a specimen without deformation. Average grain size of 1 mm was observed in non-deformed specimen and a fraction of 82% for grain boundary misorientation angles with a grain boundaries angles between 15° and 55° was found. For deformed specimen, the fraction of angles between 15° and 55° was decreced to average value of 75% and fractions of low angle (<5°) and high angle (>55°) misorientations were 10% and 15% respectively. The grain size and high fraction of grain boundary misorientation angles between 15° and 55° observed in the alloy without deformation, are favorable for grain rotation and grain boundary sliding (GBS) procces. The changes observed in the fraction of favorable grain boundary angles during superplastic deformation, shown that the superplastic capacity of Zinalco was reduced with the deformation.

Abnormal Grain Growth in Metals

2007 ◽  
Vol 558-559 ◽  
pp. 717-722 ◽  
Author(s):  
J. Dennis ◽  
Pete S. Bate ◽  
John F. Humphreys
Keyword(s):  
Grain Growth ◽  
Volume Fraction ◽  
Abnormal Grain Growth ◽  
Grain Structure ◽  
Second Phase ◽  
Boundary Misorientation ◽  
Phase Volume Fraction ◽  
Abnormal Growth ◽  
Grain Boundary Misorientation ◽  
Dominant Characteristic

Grain growth may occur in two forms, normal grain growth, characterized by a constant grain size distribution during growth, and abnormal grain growth, where one or more abnormally large grains may form in the microstructure. The presence of abnormally large grains in an otherwise uniform microstructure may be detrimental to the mechanical properties of a polycrystalline structure. Little is understood of the exact cause of abnormal grain growth. The annealing conditions leading to the onset of abnormal grain growth have been investigated via a series of grain growth experiments carried out on an Al-4wt%Cu alloy. The structure of which consisted of equiaxed grains (<8μ) pinned by a fine dispersion of sub-micron second phase particles, which may dissolve upon annealing. Minority texture components may experience accelerated growth due to a higher energy and mobility compared to the surrounding grain structure. The combination of these two events may result in the abnormal growth of some grains. SEM imaging and EBSD data has then made it possible to characterize the influence of particle dissolution and grain boundary misorientation on the onset of abnormal grain growth. The stability of ‘island grains’ found to exist internally in abnormally large grains has also been investigated in relation to the misorientation relationship and localized second phase volume fraction found there. There was only weak evidence of special misorientation relationships between the island grains and the abnormally large grains in which they exist, and although there was evidence of an enhanced fraction of pinning particles at island grain boundaries, this was also true of boundaries in general. The larger size of island grains is their dominant characteristic, and grains which become island grains may have been incipient abnormal grains.

scholarly journals Microstructure Characteristics and Corrosion Resistance of Friction Stir Welded 2205 Duplex Stainless Steel

2021 ◽  
Vol 2021 ◽  
pp. 1-11
Author(s):  
Yunqiang Zhao ◽  
Chunlin Dong ◽  
Zhongxue Jia ◽  
Jiaqing You ◽  
Jinhong Tan ◽  
...  
Keyword(s):  
Grain Size ◽  
Stainless Steel ◽  
Corrosion Resistance ◽  
Duplex Stainless Steel ◽  
Corrosion Property ◽  
Stir Zone ◽  
Boundary Misorientation ◽  
Friction Stir ◽  
2205 Duplex Stainless Steel ◽  
Grain Boundary Misorientation

In this study, 2205 duplex stainless steel was friction-stir-welded at different welding speeds. The microstructural characteristics such as grain sizes, grain boundary misorientation angles, and phase contents in the stir zones of the joints were detected. The potentiodynamic polarization and electrochemical impedance spectroscopy were also measured to evaluate the corrosion property of the stir zones. The effects of the microstructures on the corrosion property for friction-stir-welded 2205 duplex stainless steel were analyzed. The results indicated that the FSW process refined the grains and increased the ferrite contents in the stir zones. With increasing the welding speed from 30 mm/min to 50 mm/min, the grain size in the stir zone decreased from 1.64 μm to 0.96 μm, the ferrite content decreased from 59% to 54.4%, and the fractions of low angle grain boundaries for austenite and ferrite phases decreased from 63.9% and 92.6% to 18.0% and 41.1%, respectively. In this study, the effect of grain size on the corrosion resistance was the most significant and it was followed by the phase composition and the grain boundary misorientation angle. The stir zone obtained at 50 mm/min has the highest corrosion resistance, and it is followed by the base material and the stir zone obtained at 30 mm/min.

Measurement of solute segregation to grain boundaries in the AEM: A review

1988 ◽  
Vol 46 ◽  
pp. 606-607
Author(s):  
D. B. Williams ◽  
A. D. Romig
Keyword(s):  
Grain Boundary ◽  
Grain Boundaries ◽  
Boundary Migration ◽  
Grain Boundary Migration ◽  
Boundary Misorientation ◽  
Collector Plate ◽  
Segregation Process ◽  
Grain Boundary Misorientation ◽  
Structure Boundary ◽  
Equilibrium Segregation

The segregation of solute or imparity elements to grain boundaries can occur by three well-defined processes. The first is Gibbsian segregation in which an element of minimal matrix solubility confines itself to a monolayer at the grain boundary. Classical examples include Bi in Cu and S or P in Fe. The second process involves the depletion of excess matrix solute by volume diffusion to the boundary. In the boundary, the solute atoms diffuse rapidly to precipitates, causing them to grow by the ‘collector-plate mechanism.’ Such grain boundary diffusion is thought to initiate “Diffusion-Induced Grain Boundary Migration,” (DIGM). This process has been proposed as the origin of eutectoid transformations or discontinuous grain boundary reactions. The third segregation process is non-equilibrium segregation which result in a solute build-up around the boundary because of solute-vacancy interactions.All of these segregation phenomena usually occur on a sub-micron scale and are often affected by the nature of the grain boundary (misorientation, defect structure, boundary plane).

Direct imaging of order-disorder and antiphase domain structures in Ti3Al intermetallic compound

1990 ◽  
Vol 48 (4) ◽  
pp. 480-481
Author(s):  
H. Q. Ye ◽  
T.S. Xie ◽  
D. Li
Keyword(s):  
Intermetallic Compound ◽  
Volume Fraction ◽  
Fundamental Problem ◽  
Antiphase Domain ◽  
Atomic Scale ◽  
Orientation Relationships ◽  
Domain Structures ◽  
Α Phase ◽  
Diffraction Patterns ◽  
Two Phases

The Ti3Al intermetallic compound has long been recognized as potentially useful structural materials. It offers attractive strength to weight and elastic modulus to weight ratios. Recent work has established that the addition of Nb to Ti3Al ductilized this compound. In this work the fundamental problem of this alloy, i.e. order-disorder and antiphase domain structures was investigated at the atomic scale.The Ti3Al+10at%Nb alloys used in this study were treated at 1060°C and then aged at 700°C for 2 hours. The specimens suitable for TEM were prepared by standard jet electrolytic-polishing technique. A JEM-200CX electron microscope with an interpretable resolution of about 0.25 nm was used for HREM.The [100] and [001] projections of the α2 phase were shown in Fig.l.The alloy obtained consist of at least two phases-α2(Ti3Al) and β0 structures. Moreover, a disorder α phase with small volume fraction was also observed. Fig.2 gives [100] and [001] diffraction patterns of the α2 phase. Since lattice parameters of the ordered α2 (a=0.579, c=0.466 nm) and disorder α phase (a0=0.294≈a/2, c0=0.468 nm) are almost the same, their diffraction patterns are difficult to be distinguished when they are overlapped with epitaxial orientation relationships.

CM-R 411

Alloy Digest ◽  
1967 ◽  
Vol 16 (9) ◽  
Keyword(s):  
Shear Strength ◽  
High Temperature ◽  
Gas Turbine ◽  
Precipitation Hardening ◽  
Base Alloy ◽  
Heat Treating ◽  
Nickel Base Alloy ◽  
Jet Engine ◽  
Temperature Performance ◽  
Nickel Base

Abstract CM-R41 is a vacuum-melted, precipitation hardening nickel-base alloy possessing outstanding properties in the temperature range of 1200 F to 1800 F. It is recommended for jet engine and gas turbine components operating at high temperatures. This datasheet provides information on composition, physical properties, elasticity, tensile properties, and shear strength as well as creep. It also includes information on high temperature performance as well as forming, heat treating, machining, and joining. Filing Code: Ni-127. Producer or source: Cannon-Muskegon Corporation.

ALUMINUM A413.0

Alloy Digest ◽  
1984 ◽  
Vol 33 (5) ◽  
Keyword(s):  
Corrosion Resistance ◽  
Shear Strength ◽  
Physical Properties ◽  
Tensile Properties ◽  
Base Alloy ◽  
Heat Treating ◽  
Aluminum Base Alloy ◽  
Thin Walled ◽  
High Silicon ◽  
Aluminum Base

Abstract ALUMINUM A413.0 is a high-silicon (nominally 12%), aluminum-base alloy. It is recommended for applications where excellent castability and resistance to corrosion are required. Typical uses comprise miscellaneous thin-walled and intricately designed castings for such items as meter cases and automobile fittings. This datasheet provides information on composition, physical properties, elasticity, tensile properties, and shear strength as well as fatigue. It also includes information on corrosion resistance as well as casting, heat treating, machining, and joining. Filing Code: Al-251. Producer or source: Various aluminum companies.

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