scholarly journals Creep Damage and Deformation Mechanism of a Directionally Solidified Alloy during Moderate-Temperature Creep

Crystals ◽  
2021 ◽  
Vol 11 (6) ◽  
pp. 646
Author(s):  
Jiachun Li ◽  
Ning Tian ◽  
Ping Zhang ◽  
Fang Yu ◽  
Guoqi Zhao ◽  
...  

Through creep performance tests, microstructural observations, and contrast analysis of the dislocation configuration, the deformation and damage mechanism of the directionally solidified nickel-based superalloy during creep at moderate temperatures was investigated. The findings suggested that the deformation of the alloy in the late stage of creep at moderate temperatures involved dislocations slipping in the γ matrix and shearing into the γ′ phase. The super-dislocations sheared into the γ′ phase could either be decomposed to form a <112> super-Shockley incomplete dislocation plus superlattice intrinsic stacking fault (SISF) configuration, or it could slip from the {111} plane to the {100} plane and decompose to form a dislocation configuration of the Kear–Wilsdorf (K-W) lock plus antiphase domain boundary (APB). The configurations of the dislocations could inhibit the slipping and cross-slipping of dislocations to enhance the alloy creep strength, which is thought to be one reason that the alloy displayed good creep resistance. In the late creep stage, the primary/secondary slipping systems were alternately activated, and the interaction of the slipping traces caused micro-holes to appear on the interface of the γ/γ′ phases at the intersection areas of the two slipping systems. The micro-holes gathered and grew to form micro-cracks, which extended along the grain boundary at 45° to the stress axis until creep rupture occurred. These were the damage and fracture characteristics of the alloy in the late stage of creep at moderate temperatures.

2019 ◽  
Vol 795 ◽  
pp. 123-129
Author(s):  
Guo Qi Zhao ◽  
Su Gui Tian ◽  
Shun Ke Zhang ◽  
Ning Tian ◽  
Li Rong Liu

By means of creep properties measurement, microstructure observation and contrast analysis of dislocation configuration, the creep behavior of a 4.5%Re/3.0%Ru-containing single crystal nickel-based superalloy at elevated temperature is investigated. Results show that the creep life of the alloy at 1040°C/160MPa is measured to be 725h to exhibit a better creep resistance at high temperature. In the primary stage of creep at high temperature, the γ phase in alloy has transformed into the N-type rafted structure along the direction vertical to the stress axis, the deformation mechanism of alloy during steady state creep is dislocations slipping in γ matrix and climbing over the rafted γ phase. In the latter period of creep, the deformation mechanism of alloy is dislocations slipping in γ matrix and shearing into the rafted γ phase. Wherein the dislocations shearing into the γ phase may cross-slip from {111} to {100} planes for forming the K-W locks to restrain the slipping and cross-slipping on {111} plane, which is thought to be the main reason of the alloy having a better creep resistance. As the creep goes on, the alternate slipping of dislocations results in the twisted of the rafted γ phase to promote the initiation and propagation of the cracks along the interfaces of γ/γ phase up to creep fracture, which is thought to be the damage and fracture mechanism of alloy during creep at high temperature.


2019 ◽  
Vol 29 (5) ◽  
pp. 810-830 ◽  
Author(s):  
Dao-Hang Li ◽  
De-Guang Shang ◽  
Jin Cui ◽  
Luo-Jin Li ◽  
Ling-Wan Wang ◽  
...  

A fatigue–oxidation–creep damage model that can take into account the effect of multiaxial cyclic feature on the damage mechanism is proposed under axial-torsional thermo-mechanical fatigue loading. In the proposed model, the effects of non-proportional additional hardening on fatigue, oxidation, and creep damages are considered, and the variation of oxidation damage under different high temperature loading conditions is also described. Moreover, the intergranular creep damage needs to be equivalent to the transgranular damage before accumulating with the fatigue and oxidation damages. The fatigue, oxidation, and creep damages can be expressed as the fractions of fatigue life, critical crack length, and creep rupture time, respectively, which allows the linear accumulation of different types of damages on the basis of life fraction rule. In addition, the proposed model is validated by various fatigue experimental results, including uniaxial thermo-mechanical fatigue, axial-torsional thermo-mechanical fatigue, and isothermal axial-torsional fatigue under proportional and non-proportional loadings. The results showed that the errors are within a factor of 2.


Antiphase domain boundary (APB) tubes have been observed in a slightly deformed Fe–30.5 at. % Al alloy in dark field electron microscope images taken in superlattice reflexions. The image contrast theory has been developed and accounts satisfactorily for the nature of the APB tube contrast observed. The contrast theory is used to estimate the heights of the tubes. The widths of the tubes range from 20 to 50 ņ, and the measured heights are in the range of one to six times the elementary height. Evidence is presented that tubes are generated by the Vidoz & Brown (1962) mechanism and by a mechanism of cross-slip and annihilation of screw superdislocations. The possible effects of tubes on flow stress are discussed.


Author(s):  
Yoshihiko Kanda ◽  
Yuji Oto ◽  
Yusuke Shiigi ◽  
Yoshiharu Kariya

The influence of cyclic strain-hardening exponents on fatigue ductility exponents for Sn-Bi solid solution alloys and Sn-Ag-Cu microsolder joints was investigated. In Sn-Bi solid solution alloys, the fatigue ductility exponent in Coffin-Manson’s law was confirmed to increase with a decrease in the cyclic strain-hardening exponent. On the other hand, in the Sn-Ag-Cu miniature solder joint, the fatigue ductility exponent increases with a rise in temperature and strain holding. Thus, the fatigue ductility exponents are closely related to the cyclic strain-hardening exponent: the former increases due to the depression of the latter with a rise in temperature and increase in intermetallic compound particle size during strain holding. The results differ for the creep damage mechanism (grain boundary fracture), which is the main reason for the life depression in large-size specimens.


1996 ◽  
Vol 03 (01) ◽  
pp. 65-69 ◽  
Author(s):  
T. TADAKI ◽  
A. KOREEDA ◽  
Y. NAKATA ◽  
T. KINOSHITA

Atomic structure of nanoscale particles of a Cu-Au alloy with a nominal composition Cu3Au and the phase transformation therein are studied by means of high-resolution electron microscopy and electron diffraction. The particles 8.8 nm in diameter on average prepared by simultaneous vacuum deposition of the constituent elements exhibit as a whole an fcc structure of an alloy with a composition of 26.4 at.% Au. The alloy particles are ordered into the L12-type superlattice structure when heat-treated at 563 K for 1 h. The superlattice reflections disappear upon heating up to 773 K. In a particle about 10 nm in size an antiphase domain boundary is observed. It thus appears that the nanoscale particles of the alloy undergo the order-disorder transition, as in the bulk. However, the critical temperature Tc for the order-disorder transition of the nanoscale particles is found to be by about 90 K lower than that of the bulk. The minimum size of the alloy particles in which lattice fringes whose spacing corresponds to the interplanar spacing of the {100}-type superlattice planes are observed is about 4 nm. These facts suggest that a certain critical size and size effects are present for atomic ordering in the Cu-Au alloy particles.


1987 ◽  
Vol 56 (4) ◽  
pp. 517-532 ◽  
Author(s):  
A. G. Khachaturyan ◽  
J. W. Morris

2012 ◽  
Vol 19 (06) ◽  
pp. 1250057 ◽  
Author(s):  
L. X. PANG ◽  
N. F. HAN ◽  
H. SHI ◽  
J. XU ◽  
X. H. HAO ◽  
...  

The modified Peirel–Nabarro model of dislocations is not valid for the superdislocation bounded by the antiphase domain boundaries in long-range ordered intermetallic. In this work, a new Peirel–Nabarro Stress model is developed to take into account the critical resolved shear stress of antiphase domain boundary (APDB). Based on it, the Peirel–Nabarro Stress of DO3 structure and B2 structure in iron aluminides are calculated. Comparing the Peirel–Nabarro Stress of dislocations and the crystal theoretical yield strength, the results demonstrate B2-type crystal has good plasticity. It coincides with the experimental results well.


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