scholarly journals GTN Model-Based Material Parameters of AZ31 Magnesium Sheet at Various Temperatures by Means of SEM In-Situ Testing

Crystals ◽  
2020 ◽  
Vol 10 (10) ◽  
pp. 856
Author(s):  
Thorsten Henseler ◽  
Shmuel Osovski ◽  
Madlen Ullmann ◽  
Rudolf Kawalla ◽  
Ulrich Prahl
Keyword(s):  
Void Nucleation ◽  
Thin Sheet ◽  
Void Formation ◽  
Tensile Tests ◽  
Image Correlation ◽  
Ductile Damage ◽  
Material Parameters ◽  
Model Based ◽  
Simple Tension

Magnesium alloys are primarily associated with complex forming mechanisms, which yield ductility at high temperatures. In sheet metal forming, high triaxiality stress states that favor the ductile damage mechanisms of void formation and growth are known to malleable metals. The formulation of coupled damage models has so far failed, due to the incomplete experimental determination of damage parameters for magnesium AZ31 thin sheet. A quantitative investigation was conducted to determine the ductile damage behavior of twin-roll cast, hot rolled, and annealed AZ31 thin sheet. Results on the mechanisms of void nucleation-, coalescence- and growth-rate were established at temperatures ranging from room temperature to 350 °C. In-situ tensile tests were carried out in a scanning electron microscope with three different specimen types: Simple tension specimens, notched specimens for high triaxiality stress state testing, and shear specimens. Through a comparative analysis of local strains measured by digital image correlation and local void volume fractions determined through post-mortem analysis of specimen cross-sections, GTN (Gurson–Tvergaard–Needleman) model-based material parameters were determined by experiment, representing a novel departure in the magnesium research landscape. The procedure developed in this context should also be transferable to other metals in the form of thin sheets.

scholarly journals In Situ and Post-Mortem Characterizations of Ultrasonic Spot Welded AZ31B and Coated Dual Phase 590 Steel Joints

Metals ◽  
2020 ◽  
Vol 10 (7) ◽  
pp. 899 ◽  
Author(s):  
Jian Chen ◽  
Yong Chae Lim ◽  
Donovan Leonard ◽  
Hui Huang ◽  
Zhili Feng ◽  
...  
Keyword(s):  
High Speed ◽  
Tensile Tests ◽  
Fatigue Tests ◽  
Image Correlation ◽  
Joint Interface ◽  
Welding Time ◽  
Cross Sectional ◽  
Welding Condition ◽  
Lap Shear

Ultrasonic spot welding using different welding conditions was applied to join dissimilar metals of galvanized DP590 steel and AZ31B magnesium sheets. In situ high-speed imaging, digital image correlation, and infrared thermography were utilized to quantitatively study the interfacial relative motion, surface indentation, and heat generation across the joint faying interface and the sheet/sonotrode interfaces under the welding condition of moderate welding power and short welding time. For welds made with high power and long welding time, lap shear tensile tests as well as fatigue tests were carried out. Different fracture modes were observed after the lap shear tensile tests and fatigue tests performed under different peak loads. Post-weld cross-sectional analysis with scanning electron microscopy coupled with energy dispersive X-Ray spectroscopy revealed the variation of morphology and chemical composition at the joint interface for welds made with different welding conditions.

scholarly journals Damage investigation in A319 aluminum alloy by digital image correlation during in-situ tensile tests

2016 ◽  
Vol 2 ◽  
pp. 3415-3422 ◽  
Author(s):  
Zaidao Li ◽  
Nathalie Limodin ◽  
Amina Tandjaoui ◽  
Philippe Quaegebeur ◽  
Jean-François Witz ◽  
...  
Keyword(s):  
Aluminum Alloy ◽  
Digital Image Correlation ◽  
Digital Image ◽  
Tensile Tests ◽  
Image Correlation ◽  
Damage Investigation

Effects of Strain Rate and Temperature on Ductile Damage of Metals

2018 ◽  
Author(s):  
Alexander Sancho ◽  
Mike J. Cox ◽  
Tim Cartwright ◽  
Paul A. Hooper ◽  
John P. Dear ◽  
...  
Keyword(s):  
Strain Rate ◽  
High Speed ◽  
Damage Accumulation ◽  
Tensile Tests ◽  
Ductile Damage ◽  
Metallic Materials ◽  
Stiffness Reduction ◽  
Strain Behaviour ◽  
Experimental Rig

Ductile damage appears in ductile metallic materials when these undergo sufficient plastic deformation, and it is caused by voids and microcracks that are formed within the material due to those severe conditions. The main interest of the present research is to experimentally characterise ductile damage in different conditions of strain rate (from quasi-static to 103s−1) and temperature (from −80°C to 180°C). Estimations of damage accumulation along the plastic regime have been taken by measuring the stiffness reduction of the material. The effects of strain localisation and necking have been accounted for by monitoring the changes in the geometry of the specimens during the test. At high speed these experiments have required the use of an in-situ shadowgraph method to monitor the sample silhouette and accurately calculate stress-strain behaviour throughout the test. The design of a novel experimental rig to perform high speed interrupted tensile tests has also been needed, in order to measure the damage accumulation in those conditions. The low and high temperature tests have been carried out inside an environmental chamber maintaining the rest of the technique unchanged. These experiments at varying strain rate and temperature have allowed to better understand the effect these conditions have on damage properties.

scholarly journals Strain Evolution Measurement at the Microscale of a Dual Phase Steel Using Digital Image Correlation

2010 ◽  
Vol 24-25 ◽  
pp. 201-206 ◽  
Author(s):  
H. Ghadbeigi ◽  
C. Pinna ◽  
Steven Celotto ◽  
J.R. Yates
Keyword(s):  
Digital Image Correlation ◽  
Digital Image ◽  
Dual Phase Steel ◽  
Tensile Tests ◽  
Image Correlation ◽  
Scanning Electron Micrographs ◽  
Plastic Strains ◽  
Full Field ◽  
Loading Direction

Digital Image Correlation (DIC) together with in-situ tensile testing has been used to measure in DP1000 steel the evolution of plastic strains at the microstructure scale. Interrupted tensile tests were performed on specially designed samples and scanning-electron micrographs were taken at regular applied strain intervals. Patterns defined by the microstructural features of the material have been used for the correlation carried out using LAVision software. The full field strain maps produced by DIC show a progressive localisation of deformation into bands at about 45o with respect to the loading direction. Plastic strains as high as 130% have been measured within the ferrite phase.

In-situ TEM Study of Thermally Induced Voids in 180 nm Cu Interconnects

2005 ◽  
Vol 907 ◽  
Author(s):  
Jin Ho An ◽  
P.J. Ferreira
Keyword(s):  
Crystal Orientation ◽  
Void Nucleation ◽  
Void Formation ◽  
Grain Morphology ◽  
In Situ Tem ◽  
Thermally Induced ◽  
Cu Interconnects ◽  
Formation Behavior ◽  
Reliability Issue

AbstractCu interconnects have decreased in width and are at around 100 nm. A decrease in interconnect width have led to a predominately bamboo structured Cu lines. In Cu interconnects, void formation during high temperature is a reliability issue, and this study looks at the void formation behavior in damascene Cu interconnects with a predominately bamboo microstructure. First, the crystal texture and grain morphology of the Cu interconnects was observed. Then to determine the void formation behavior, in-situ Transmission Electron Microscopy (TEM) was performed. Voids that formed as a result of in-situ heating were analyzed in terms of preferential void formation sites and crystal orientation where voids formed. In bamboo structured lines, voids formed at the triple junction of grain boundary and Cu/diffusion barrier interface. The crystal orientation where voids nucleated was studied to identify diffusion paths during void nucleation and growth.

scholarly journals Mechanical response of a Laser Cladding repaired structure: localization of plastic strain due to microstructure gradient

2019 ◽  
Vol 300 ◽  
pp. 03003
Author(s):  
Camille Guévenoux ◽  
Simon Hallais ◽  
Alexandre Charles ◽  
Eric Charkaluk ◽  
Andrei Constantinescu
Keyword(s):  
Laser Cladding ◽  
Mechanical Response ◽  
Base Material ◽  
Correlation Method ◽  
Tensile Tests ◽  
Image Correlation ◽  
Thin Walls ◽  
Gauge Section ◽  
Initial Geometry

Laser Cladding is an additive manufacturing technology enabling to repair complex metallic components by removing the worn region and reconstructing locally the initial geometry. The aim of this work is to study the mechanical response of Inconel 718 repaired thin walls. More precisely, we perform an EBSD imaging and in-situ SEM tensile tests on specimen whose gauge section contains the interface between base material and repaired area. We observe the multiaxial strain patterns until failure at the grain level using a Digital Image Correlation method and superpose this pattern with the microstructure gradient induced by repair. The observations highlight a strain localization phenomenon in repaired structures mainly due to grain size effect.

In situ observations of electromigration induced void behavior

1995 ◽  
Vol 53 ◽  
pp. 244-245
Author(s):  
T. Marieb ◽  
J. C. Bravman ◽  
P. Flinn ◽  
D. Gardner ◽  
M. Madden
Keyword(s):  
Electron Microscopy ◽  
Void Nucleation ◽  
Plan View ◽  
Transmission Electron ◽  
Nucleation Sites ◽  
Microelectronics Industry ◽  
In Situ Observations ◽  
Backscatter Electron Detector ◽  
Voltage Scanning

Electromigration and stress voiding have been active areas of research in the microelectronics industry for many years. While accelerated testing of these phenomena has been performed for the last 25 years[1-2], only recently has the introduction of high voltage scanning electron microscopy (HVSEM) made possible in situ testing of realistic, passivated, full thickness samples at high resolution.With a combination of in situ HVSEM and post-testing transmission electron microscopy (TEM) , electromigration void nucleation sites in both normal polycrystalline and near-bamboo pure Al were investigated. The effect of the microstructure of the lines on the void motion was also studied.The HVSEM used was a slightly modified JEOL 1200 EX II scanning TEM with a backscatter electron detector placed above the sample[3]. To observe electromigration in situ the sample was heated and the line had current supplied to it to accelerate the voiding process. After testing lines were prepared for TEM by employing the plan-view wedge technique [6].

scholarly journals Effect of Crystallographic Orientation and Grain Boundaries on Martensitic Transformation and Superelastic Response of Oligocrystalline Fe–Mn–Al–Ni Shape Memory Alloys

2021 ◽  
Author(s):  
A. Bauer ◽  
M. Vollmer ◽  
T. Niendorf
Keyword(s):  
Martensitic Transformation ◽  
Grain Boundary ◽  
Shape Memory Alloys ◽  
Shape Memory ◽  
Grain Boundaries ◽  
Tensile Tests ◽  
Image Correlation ◽  
Stress Concentrations ◽  
Grain Orientations ◽  
High Degree

AbstractIn situ tensile tests employing digital image correlation were conducted to study the martensitic transformation of oligocrystalline Fe–Mn–Al–Ni shape memory alloys in depth. The influence of different grain orientations, i.e., near-〈001〉 and near-〈101〉, as well as the influence of different grain boundary misorientations are in focus of the present work. The results reveal that the reversibility of the martensite strongly depends on the type of martensitic evolving, i.e., twinned or detwinned. Furthermore, it is shown that grain boundaries lead to stress concentrations and, thus, to formation of unfavored martensite variants. Moreover, some martensite plates seem to penetrate the grain boundaries resulting in a high degree of irreversibility in this area. However, after a stable microstructural configuration is established in direct vicinity of the grain boundary, the transformation begins inside the neighboring grains eventually leading to a sequential transformation of all grains involved.

scholarly journals Digital Image Correlation for Evaluation of Cracks in Reinforced Concrete Bridge Slabs

2021 ◽  
Vol 6 (7) ◽  
pp. 99
Author(s):  
Christian Overgaard Christensen ◽  
Jacob Wittrup Schmidt ◽  
Philip Skov Halding ◽  
Medha Kapoor ◽  
Per Goltermann
Keyword(s):  
Reinforced Concrete ◽  
Digital Image Correlation ◽  
Crack Initiation ◽  
Laboratory Test ◽  
Digital Image ◽  
Crack Detection ◽  
Image Correlation ◽  
In Situ Tests ◽  
Stop Criterion

In proof-loading of concrete slab bridges, advanced monitoring methods are required for identification of stop criteria. In this study, Two-Dimensional Digital Image Correlation (2D DIC) is investigated as one of the governing measurement methods for crack detection and evaluation. The investigations are deemed to provide valuable information about DIC capabilities under different environmental conditions and to evaluate the capabilities in relation to stop criterion verifications. Three Overturned T-beam (OT) Reinforced Concrete (RC) slabs are used for the assessment. Of these, two are in situ strips (0.55 × 3.6 × 9.0 m) cut from a full-scale OT-slab bridge with a span of 9 m and one is a downscaled slab tested under laboratory conditions (0.37 × 1.7 × 8.4 m). The 2D DIC results includes full-field plots, investigation of the time of crack detection and monitoring of crack widths. Grey-level transformation was used for the in situ tests to ensure sufficient readability and results comparable to the laboratory test. Crack initiation for the laboratory test (with speckle pattern) and in situ tests (plain concrete surface) were detected at intervals of approximately 0.1 mm to 0.3 mm and 0.2 mm to 0.3 mm, respectively. Consequently, the paper evaluates a more qualitative approach to DIC test results, where crack indications and crack detection can be used as a stop criterion. It was furthermore identified that crack initiation was reached at high load levels, implying the importance of a target load.

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