scholarly journals Microstructural Investigations of Low Temperature Joining of Q&P Steels Using Ag Nanoparticles in Combination with Sn and SnAg as Activating Material

2019 ◽  
Vol 9 (3) ◽  
pp. 539 ◽  
Author(s):  
Susann Hausner ◽  
Martin Wagner ◽  
Guntram Wagner
Keyword(s):  
Heat Treatment ◽  
Ag Nanoparticles ◽  
Low Temperatures ◽  
Retained Austenite ◽  
Steel Substrate ◽  
High Strength ◽  
The One ◽  
Treatment Step ◽  
Heat Treatment Step ◽  
Strength And Ductility

Quenching and partitioning (Q&P) steels show a good balance between strength and ductility due to a special heat treatment that allows to adjust a microstructure of martensite with a fraction of stabilized retained austenite. The final heat treatment step is performed at low temperatures. Therefore, joining of Q&P steels is a big challenge. On the one hand, a low joining temperature is necessary in order not to influence the adjusted microstructure; on the other hand, high joint strengths are required. In this study, joining of Q&P steels with Ag nanoparticles is investigated. Due to the nano-effect, high-strength and temperature-resistant joints can be produced at low temperatures with nanoparticles, which meets the contradictory requirements for joining of Q&P steels. In addition to the Ag nanoparticles, activating materials (SnAg and Sn) are used at the interface to achieve an improved bonding to the steel substrate. The results show that the activating materials play an important role in the successful formation of joints. Only with the activating materials, can joints be produced. Due to the low joining temperature (max. 237 °C), the microstructure of the Q&P steel is hardly influenced.

Effects of Heat Treatment on Microstructure of High-Strength Manganese-Silicon Steels

2017 ◽  
Vol 270 ◽  
pp. 239-245
Author(s):  
Dagmar Bublíková ◽  
Štěpán Jeníček ◽  
Kateřina Opatová ◽  
Bohuslav Mašek
Keyword(s):  
Heat Treatment ◽  
Cooling Rate ◽  
Microstructure Evolution ◽  
Retained Austenite ◽  
Volume Fraction ◽  
High Strength ◽  
Quenching And Partitioning ◽  
Alloying Additions ◽  
New Procedures ◽  
Strength And Ductility

Today’s advanced steels are required to possess high strength and ductility. This can be accomplished by producing appropriate microstructures with a certain volume fraction of retained austenite. The resulting microstructure depends on material’s heat treatment and alloying. High ultimate strengths and sufficient elongation levels can be obtained by various methods, including quenching and partitioning (Q&P process). The present paper introduces new procedures aimed at simplifying this process with the use of material-technological modelling. Three experimental steels have been made and cast for this investigation, whose main alloying additions were manganese, silicon, chromium, molybdenum and nickel. The purpose of manganese addition was to depress the Ms and Mf temperatures. The Q&P process was carried out in a thermomechanical simulator for better and easier control. The heat treatment parameters were varied between the sequences and their effect on microstructure evolution was evaluated. They included the cooling rate, partitioning temperature and time at partitioning temperature. Microstructures including martensite with strength levels of more than 2000 MPa and elongation of 10–15 % were obtained.

Effect of Alloying and Thermal Processing on Mechanical Properties of TiAl Alloys

2016 ◽  
Vol 258 ◽  
pp. 501-505
Author(s):  
Alice Chlupová ◽  
Milan Heczko ◽  
Karel Obrtlík ◽  
Přemysl Beran ◽  
Tomáš Kruml
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Thermal Processing ◽  
Lamellar Microstructure ◽  
High Strength ◽  
Fatigue Behaviour ◽  
Tial Alloys ◽  
Working Temperature ◽  
Β Phase ◽  
Strength And Ductility

Two γ-based TiAl alloys with 7 at.% of Nb, alloyed with 2 at.% Mo and 0.5 at.% C, were studied. A heat treatment leading to very fine lamellar microstructure was applied on both alloys. Microstructure after the heat treatment was described and mechanical properties including fatigue behaviour were measured. The as-received material alloyed with C possesses high strength and very limited ductility, especially at RT. After application of selected heat treatment it becomes even more brittle; therefore, this process could be considered as not appropriate for this alloy. On the contrary, in the case of Mo alloyed material, both strength and ductility are improved by the heat treatment at RT and usual working temperature (~750 °C). Presence of the β phase is responsible for this effect. The selected heat treatment thus can be an alternative for this alloy to other thermomechanical treatments as high temperature forging.

Improvement of Strength and Ductility by Combining Static Recrystallization and Unique Heat Treatment in Co-20Cr-15W-10Ni Alloy for Stent Application

2021 ◽  
Vol 1016 ◽  
pp. 1503-1509
Author(s):  
Kosuke Ueki ◽  
Soh Yanagihara ◽  
Kyosuke Ueda ◽  
Masaaki Nakai ◽  
Takayoshi Nakano ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Grain Size ◽  
Static Recrystallization ◽  
High Strength ◽  
Small Variation ◽  
Grain Structure ◽  
Fine Grain ◽  
High Temperature Short Time ◽  
Average Grain Size ◽  
Strength And Ductility

The Co-20Cr-15W-10Ni (CCWN, mass%) alloy has excellent corrosion resistance and strength-ductility balance and is applied in almost all balloon-expandable stent platforms. To further reduce the invasiveness of stent placement, it is necessary to reduce the diameter of the stent. That is, both high strength and high ductility should be achieved while maintaining a low yield stress. In our previous studies, it was discovered that low-temperature heat-treatment (LTHT) at 873 K improves the elongation of the CCWN alloy. In this study, we focused on the grain refinement by swaging and static recrystallization to improve the strength of the alloy. The as-swaged alloy was recrystallized at 1373–1473 K for 100–300 s, followed by LTHT. A fine grain structure with an average grain size of 3–17 μm was obtained by static recrystallization. The η-phase (M12X-M6X type precipitates, M: metallic elements, X: C and/or N) formed during the recrystallization at 1373–1448 K. The alloys recrystallized at 1448 and 1473 K had a homogeneous structure with a small variation in the grain size. On the other hand, the alloys recrystallized at 1373 and 1423 K had an inhomogeneous structure in which fine and coarse grains were mixed. Both the strength and ductility of the CCWN alloy were improved by combining high-temperature short-time recrystallization and LTHT.

Microstructure and Tensile Properties of TRIP-Aided Steel Sheet Subjected to Hot-Rolling and Austempering

2021 ◽  
Vol 1016 ◽  
pp. 732-737
Author(s):  
Junya Kobayashi ◽  
Hiroto Sawayama ◽  
Naoya Kakefuda ◽  
Goroh Itoh ◽  
Shigeru Kuraoto ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Hot Rolling ◽  
Manufacturing Process ◽  
Retained Austenite ◽  
Volume Fraction ◽  
Isothermal Holding ◽  
High Strength ◽  
Isothermal Transformation ◽  
Transformation Process ◽  
Steel Sheets

Various high strength steel sheets for weight reduction and safety improvement of vehicles have been developed. TRIP-aided steel with transformation induced plasticity of the retained austenite has high strength and ductility. Conventional TRIP-aided steels are subjected to austempering process after austenitizing. Generally, elongation and formability of TRIP-aided steel are improved by finely dispersed retained austenite in BCC phase matrix. The finely dispersed retained austenite and grain refinement of TRIP-aided steel can be achieved by hot rolling with heat treatment. Therefore, the improvement of mechanical properties of TRIP-aided steel is expected from the manufacturing process with hot rolling and then isothermal transformation process. In this study, thermomechanical heat treatment is performed by combining hot rolling and isothermal holding as the manufacturing process of TRIP-aided steel sheets. The complex phase matrix is obtained by hot rolling and then isothermal holding. Although the hardness of the hot rolled and isothermal held TRIP-aided steel is decreased, the volume fraction of retained austenite is increased.

Toward the Development of AHSS for Wear Resistant Applications

2018 ◽  
Vol 941 ◽  
pp. 568-573 ◽  
Author(s):  
Preston Wolfram ◽  
Christina Hensley ◽  
Ronald Youngblood ◽  
Rachael Stewart ◽  
Emmanuel de Moor ◽  
...  
Keyword(s):  
Wear Resistance ◽  
Retained Austenite ◽  
Process Development ◽  
High Strength ◽  
Advanced High Strength Steel ◽  
Wear Resistant ◽  
Transformation Induced Plasticity ◽  
Enhance Wear Resistance ◽  
Improve Wear Resistance ◽  
Strength And Ductility

Advanced High Strength Steel (AHSS) developments have largely focused on automotive applications using metallurgical approaches to develop retained austenite-containing microstructures in a variety of new steels, using the transformation-induced plasticity (TRIP) effect to achieve better combinations of strength and ductility. These efforts have been extended in recent studies to explore the potential to improve wear resistance, using metastable retained austenite to enhance wear resistance for earth-moving and other applications. This paper provides selected highlights of the authors’ efforts to develop wear resistant steels using AHSS processing approaches. Some attractive product/process development opportunities are identified, and it appears that martensite-austenite microstructures produced using “quenching and partitioning” exhibit increased wear resistance.

scholarly journals Microstructure and Mechanical Properties of High Vacuum Die-Cast AlSiMgMn Alloys at as-Cast and T6-Treated Conditions

Materials ◽  
2019 ◽  
Vol 12 (13) ◽  
pp. 2065
Author(s):  
Fei Liu ◽  
Haidong Zhao ◽  
Runsheng Yang ◽  
Fengzhen Sun
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Failure Modes ◽  
High Vacuum ◽  
High Strength ◽  
Thin Wall ◽  
T6 Heat Treatment ◽  
Die Cast ◽  
Strength And Ductility

Al–Si–Mg based alloys can provide high strength and ductility to satisfy the increasing demands of thin wall castings for automotive applications. This study has investigated the effects of T6 heat-treatment on the microstructures, the local mechanical properties of alloy phases and the fracture behavior of high vacuum die-cast AlSiMgMn alloys using in-situ scanning electron microscopy (SEM) in combination with nano-indentation testing. The microstructures of the alloys at as-cast and T6 treated conditions were compared and analyzed. It is found that the T6 heat treatment plays different roles in affecting the hardness and the Young’s modulus of alloy phases. This study also found that the T6 heat treatment would influence the failure modes of the alloys. The mechanisms of crack propagation in the as-cast and T6 treated alloys were also analyzed and discussed.

Microstructure and Mechanical Properties of a Nb-Microalloyed Medium Carbon Steel Treated by Quenching-Partitioning Process

2012 ◽  
Vol 531-532 ◽  
pp. 596-599
Author(s):  
Kai Zhang ◽  
Shang Wen Lu ◽  
Yao Hui Ou ◽  
Xiao Dong Wang ◽  
Ning Zhong
Keyword(s):  
Mechanical Properties ◽  
Heat Treatment ◽  
Electron Microscope ◽  
Carbon Steel ◽  
Retained Austenite ◽  
High Strength ◽  
Medium Carbon Steel ◽  
Orientation Relationships ◽  
Medium Carbon ◽  
Microstructure And Mechanical Properties

The recently developed “quenching and partitioning” heat treatment and “quenching-partitioning-tempering” heat treatment are novel processing technologies, which are designed for achieving advanced high strength steels (AHSS) with combination of high strength and adequate ductility. In present study, a medium carbon steel containing Nb was subjected to the Q-P-T process, and both the microstructure and mechanical properties was studied. The experimental results show that the Nb-microalloyed steel demonstrates high tensile strength and relatively high elongation. The microstructure of the steel was investigated in terms of scanning electron microscope and transmission electron microscope, and the results indicate that the Q-P-T steel consist of fine martensite laths with dispersive carbide precipitates and the film-like interlath retained austenite. The orientation relationships between martensite and retained austenite is as well-known Kurdjurmov-Sachs relationship and Nishiyama-Wasserman relationship.

Microstructure and Mechanical Propertiesof Ti/Cu-Cr/S20C and Ti/Cu-Ag/S20C Clad Composites

2013 ◽  
Vol 376 ◽  
pp. 153-157 ◽  
Author(s):  
Jong Su Ha ◽  
Sun Ig Hong
Keyword(s):  
Heat Treatment ◽  
High Pressure ◽  
Strain Hardening ◽  
Intermetallic Compounds ◽  
Mechanical Performance ◽  
High Strength ◽  
Strengthening Mechanism ◽  
Reaction Products ◽  
Heat Treated ◽  
Strength And Ductility

In this study Cu-Ag or Cu-Cr layer was sandwiched by Ti and Fe plates and the three layers of Ti/Cu-8Ag/S20C were clad by High Pressure Torsioning(HPT). The effect of post-HPT heat treatment on the interfacial reaction products and the mechanical performance in Ti/Cu-Ag/S20C and Ti/Cu-Cr/S20C clad material were studied. Cu4Ti3 and Cu4Ti Intremetallic compound layers were observed at the Ti/Cu-Ag and Ti/Cu-Cr interfaces in the clad heat-treated at 500°C where as no intermetallic compounds were observed at the Cu-Ag/S20C and Cu-Cr/S20C interfaces. The strength of as-HPTed Ti/Cu-8Ag/S20C is much higher than that of Ti/Cu-1Cr/S20C. The strengthening mechanism of Cu-Ag deformed severely is the interface and strain hardening in which dislocations are deposited at the Cu/Ag interfaces and can contribute to the strengthening of the clad composite just after HPT processing, rendering the high strength just after processing. In both clad composites, the strength and ductility increased after heat treatment at 350°C, which are likely caused by the enhanced bonding at the interfaces.

scholarly journals EFFECTS OF Q&P PROCESS PARAMETERS ON PROPERTIES OF 42SiCr STEEL

2018 ◽  
Vol 24 (2) ◽  
pp. 126
Author(s):  
Kateřina Rubešová ◽  
Ivan Vorel ◽  
Hana Jirková ◽  
Štěpán Jeníček
Keyword(s):  
Heat Treatment ◽  
Ultimate Strength ◽  
Retained Austenite ◽  
High Strength ◽  
Carbon Diffusion ◽  
Salt Bath ◽  
Treatment Techniques ◽  
Microstructure Effects ◽  
The Impact ◽  
Quenching And Tempering

<p class="AMSmaintext"><span lang="EN-GB">The requirement for high strength and good ductility poses problems in today’s advanced steels. This problem can be tackled by appropriate heat treatment which produces suitable microstructures. By this means, ultimate strengths of about 2000 MPa and elongations of more than 10% can be obtained. One of such advanced heat treatment techniques is the Q&amp;P (Quenching and Partitioning) process. It produces a mixture of martensite and retained austenite, where the latter is an important agent in raising the ductility of steel. </span></p><p class="AMSmaintext"><span lang="EN-GB">In this experiment, a low-alloy steel with 0.41% carbon and manganese, silicon and chromium was used. An air furnace and a salt bath were employed for heat treatment and quenching, respectively. In order to obtain the best ultimate strength and elongation levels, partitioning temperatures of 250°C and 300°C were applied. Partitioning involves carbon diffusion from super-saturated martensite into retained austenite, and tempering of hardening microstructure. Effects of the quenching temperatures of 200°C and 150°C were studied as well. To map the impact of the Q&amp;P process on mechanical properties, an additional schedule with conventional quenching and tempering was carried out. Upon optimization of the parameters, the process produced martensite with a small amount of bainite and retained austenite. The ultimate strength was between 1930 and 2080 MPa and the elongation levels were from 9 to 16%.</span></p><p class="AMSmaintext"><span lang="EN-GB"> </span></p>

scholarly journals Low temperature tensile properties of line pipe steels

2015 ◽  
Vol 6 (3) ◽  
pp. 8
Author(s):  
Harold Tubex ◽  
Koen Van Minnebruggen ◽  
Wim De Waele
Keyword(s):  
Tensile Properties ◽  
Low Temperatures ◽  
Oil And Gas ◽  
High Strength ◽  
The Arctic ◽  
Test Results ◽  
Pipe Steels ◽  
Line Pipe ◽  
Expected Increase ◽  
Strength And Ductility

Given the expected increase in Arctic oil and gas exploitation, there is a demand for high-strength line pipe steels able to cope with the Arctic climate. The state-of-the-art of the tensile properties of API 5L steels at low temperatures is reviewed and discussed. Well-known characteristics such as an increase in strength and Young’s modulus with decreasing temperatures are confirmed. The Y/T ratio is fairly unaffected by changes in temperature. Lüders elongation manifests itself at low temperatures where the Lüders plateau tends to increase. Conflicting statements about the relation between ductility and temperature were found. Altogether, quantifiable test results are scarce, especially for the high strength grades from API 5L X90 grade onwards. The urgent need for more tensile strength and ductility data of these steels at low temperatures is stated and defended.

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