scholarly journals Fluence Dependence of Surface Morphology and Deuterium Retention in W Bulks and Nanocrystalline W Films Exposed to Deuterium Plasma

2021 ◽  
Vol 11 (4) ◽  
pp. 1619
Author(s):  
Jing Yan ◽  
Xia Li ◽  
Kaigui Zhu

The surface morphology of pure W bulks and nanocrystalline tungsten films was investigated after exposure to a low-energy (100 eV/D), high-flux (1.8 × 1021 D·m−2s−1) deuterium plasma. Nanocrystalline tungsten films of 6 μm thickness were deposited on tungsten bulks and exposed to deuterium plasma at various fluences ranging from 1.30 × 1025 to 5.18 × 1025 D·m−2. Changes in surface morphology from before to after irradiation were studied with scanning electron microscopy (SEM). The W bulk exposed to low-fluence plasma (1.30 × 1025 D·m−2) shows blisters. The blisters on the W bulk irradiated to higher-fluence plasma are much larger (~2 µm). The blisters on the surface of W films are smaller in size and lower in density than those of the W bulks. In addition, the modifications exhibit the appearance of cracks below the surface after deuterium plasma irradiation. It is suggested that the blisters are caused by the diffusion and aggregation of the deuterium-vacancy clusters. The deuterium retention of the W bulks and nanocrystalline tungsten films was studied using thermal desorption spectroscopy (TDS). The retention of deuterium in W bulks and W films increases with increasing deuterium plasma fluence when irradiated at 500 K.

2008 ◽  
Vol 59 ◽  
pp. 42-45
Author(s):  
Vladimir K. Alimov ◽  
Wataru M. Shu ◽  
J. Roth ◽  
D.A. Komarov ◽  
Stefan Lindig ◽  
...  

Deuterium retention in single crystal and polycrystalline tungsten and molybdenum exposed to low-energy (38200 eV/D), high ion flux (10211022 D/m2s) deuterium plasmas at various temperatures were examined with the D(3He,p)4He nuclear reaction at a 3He energy varied from 0.69 to 4.0 MeV, and with thermal desorption spectroscopy. The surface morphology was examined by scanning electron microscope. Blisters formed on the Mo surfaces under plasma exposure are significantly larger in size than those for W. The D retention in the W and Mo samples increases with the exposure temperature, reaching its maximum at about 500 and 530 K (for ion fluxes of 1021 and 1022 D/m2/s), respectively, and then decreases as the temperature grows further. For polycrystalline W and Mo exposed at temperatures above 400 K, the D retention in the bulk (far beyond the ion implanted zone) is dominant. Plastic deformation caused by deuterium super-saturation within the near-surface layer is suggested as a mechanism for blister formation and creation of defects responsible for deuterium trapping at depths up to several micrometers.


2014 ◽  
Vol 454 (1-3) ◽  
pp. 136-141 ◽  
Author(s):  
V.Kh. Alimov ◽  
Y. Hatano ◽  
K. Sugiyama ◽  
M. Balden ◽  
M. Oyaidzu ◽  
...  

2014 ◽  
Vol 54 (8) ◽  
pp. 083014 ◽  
Author(s):  
M.H.J. 't Hoen ◽  
M. Balden ◽  
A. Manhard ◽  
M. Mayer ◽  
S. Elgeti ◽  
...  

2012 ◽  
Vol 420 (1-3) ◽  
pp. 519-524 ◽  
Author(s):  
V.Kh. Alimov ◽  
B. Tyburska-Püschel ◽  
S. Lindig ◽  
Y. Hatano ◽  
M. Balden ◽  
...  

2011 ◽  
Vol 409 (1) ◽  
pp. 27-32 ◽  
Author(s):  
V.K. Alimov ◽  
B. Tyburska ◽  
M. Balden ◽  
S. Lindig ◽  
J. Roth ◽  
...  

2009 ◽  
Vol T138 ◽  
pp. 014048 ◽  
Author(s):  
V Kh Alimov ◽  
W M Shu ◽  
J Roth ◽  
K Sugiyama ◽  
S Lindig ◽  
...  

2021 ◽  
pp. 153168
Author(s):  
Hanjun Tu ◽  
Shiwei Wang ◽  
Liangcheng Cui ◽  
Long Cheng ◽  
Guang-Hong Lu ◽  
...  

Sign in / Sign up

Export Citation Format

Share Document