scholarly journals The Effects of Multi-Stage Homogenizations on the Microstructures and Mechanical Properties of Al–Zn–Mg–Zr–Sc Alloys

2021 ◽  
Vol 11 (2) ◽  
pp. 470
Author(s):  
Yang-Chun Chiu ◽  
Tse-An Pan ◽  
Mien-Chung Chen ◽  
Jun-Wei Zhang ◽  
Hui-Yun Bor ◽  
...  

This study is aimed at exploring the effects of multi-stage homogenization and trace amounts of Zr and Sc on the microstructures, mechanical properties, and recrystallization of Al–4.5Zn–1.5Mg alloys. The mechanical properties of the AA7005 aluminum alloys after the T6 heat treatment were evaluated through a hardness test and tensile test. The microstructures were analyzed by an optical microscope (OM), a differential scanning calorimeter (DSC), a transmission electron microscope (TEM), a scanning electron microscope (SEM), and electron backscattered diffraction (EBSD). The results show that the grain refinement effect of the as-cast, homogenized, and recrystallized Al–4.5Zn–1.5Mg alloy containing 0.05Sc (wt%) after the T6 heat treatment was more significant than that of the alloy containing 0.1Zr (wt%). In addition, compared with the aforementioned one-stage homogenization heat treatment, the two-stage homogenization made the dispersed grain phase (Al3Zr/Al3Sc) smaller. As a result, the T6 mechanical strength of the alloy after the two-stage homogenization heat treatment was better than that of the contrastive alloy after the one-stage homogenization heat treatment. However, the two different homogenization heat treatments caused a greater divergence between the sizes of the dispersed grain phases of the Al–4.5Zn–1.5Mg alloys containing Zr than between the sizes of the dispersed grain phases of the alloys containing Sc. Therefore, after the two-stage homogenization heat treatment, the alloy with 0.1Zr (wt%) promoted the mechanical properties better than the alloy with 0.05Sc (wt%).

2007 ◽  
Vol 550 ◽  
pp. 289-294
Author(s):  
Suk Hoon Kang ◽  
Jae Hyung Cho ◽  
Joon Sub Hwang ◽  
Jong Soo Cho ◽  
Yong Jin Park ◽  
...  

Cold drawn gold wires are widely applied in electronic packaging process to interconnect micro-electronic components. They basically provides a conducting path for electronic signal transfer, and experience thermo-mechanical loads in use. The mechanical stability of drawn gold wires is a matter of practical concern in the reliable functioning of electronic devices. It is known that mechanical properties of materials are deeply related to the microstructure. With appropriate control of deformation and heat processes, the mechanical properties of final products, such as tensile strength and elongation can be improved. Severe plastic deformation by torsion usually contributes to grain refinement and increment of strength. In this study, microstructure variations with torsion strain followed by drawing and heat treatment were investigated. Analyses by focused ion beam (FIB) and electron backscattered diffraction (EBSD) were carried out to characterize the effect of deformation and heat treatment on the drawn gold wires. Pattern quality of EBSD measurements was used as a quantitative measure for plastic deformation.


2014 ◽  
Vol 989-994 ◽  
pp. 212-215
Author(s):  
J. Liu ◽  
G. Zhu ◽  
W. Mao

The effect of volume fraction of ferrite on the mechanical properties including strength, plasticity and wok hardening was systematically investigated in X80 pipeline steel in order to improve the plasticity. The microstructures with different volume fraction of ferrite and bainite were obtained by heat-treatment processing and the mechanical properties were tested. The work hardening behavior was analyzed by C-J method. The results show that the small amount of ferrite could effectively improve the plasticity. The work hardening ability and the ratio of yield/tensile strength with two phases of ferrite/bainite would be obviously better than that with single phase of bainite. The improvement of plasticity could be attributed to the ferrite in which more plastic deformation was afforded.


2019 ◽  
Vol 38 (2019) ◽  
pp. 892-896 ◽  
Author(s):  
Süleyman Tekeli ◽  
Ijlal Simsek ◽  
Dogan Simsek ◽  
Dursun Ozyurek

AbstractIn this study, the effect of solid solution temperature on microstructure and mechanical properties of the AA7075 alloy after T6 heat treatment was investigated. Following solid solution at five different temperatures for 2 hours, the AA7075 alloy was quenched and then artificially aged at 120∘C for 24 hours. Hardness measurements, microstructure examinations (SEM+EDS, XRD) and tensile tests were carried out for the alloys. The results showed that the increased solid solution temperature led to formation of precipitates in the microstructures and thus caused higher hardness and tensile strength.


1968 ◽  
Vol 40 (2) ◽  
pp. 175-188 ◽  
Author(s):  
J. B. BROWN ◽  
CAROLINE MACNAUGHTAN ◽  
MARGERY A. SMITH ◽  
BARBARA SMYTH

SUMMARY Higher temperatures allow lower sulphuric acid concentrations and shorter heating times to be used in the Kober colour reaction for oestrogens. A one-stage reaction which is completed in 5 min. at 120° is described for oestrone and oestradiol, and a two-stage reaction which requires two periods of heating for 5 min. at 120° is described for oestriol. The conditions were applied to the Ittrich fluorescence procedure. A spectrophotofluorimetric correction was developed in which fluorescence was measured at wavelengths for excitation and emitted light near the optima for the oestrogens and at another combination at which the oestrogens produced virtually no fluorescence whereas that of impurities was not diminished. Extraction, centrifugation and fluorimetry were performed in specially designed cells. The sensitivity is 0·05–0·1 ng./sample with a linear response up to 300 ng. and a precision better than 4% in the range 1·0–100 ng.


2019 ◽  
Vol 944 ◽  
pp. 64-72
Author(s):  
Qing Feng Yang ◽  
Cun Juan Xia ◽  
Ya Qi Deng

Bulky sample was made by using TIG wire and arc additive manufacturing (WAAM) technology, in which Ф1.6 mm filler wire of in-situ TiB2/Al-Si composites was selected as deposition metal, following by T6 heat treatment. The microstructure and mechanical properties of the bulky sample before and after heat treatment were analyzed. Experimental results showed that the texture of the original samples parallel to the weld direction and perpendicular to the weld direction was similar consisting of columnar dendrites and equiaxed crystals. After T6 heat treatment, the hardness of the sample was increased to 115.85 HV from 62.83 HV, the yield strength of the sample was 273.33 MPa, the average tensile strength was 347.33 MPa, and the average elongation after fracture was 7.96%. Although pore defects existed in the fracture, yet the fracture of the sample was ductile fracture.


Materials ◽  
2019 ◽  
Vol 12 (13) ◽  
pp. 2065
Author(s):  
Fei Liu ◽  
Haidong Zhao ◽  
Runsheng Yang ◽  
Fengzhen Sun

Al–Si–Mg based alloys can provide high strength and ductility to satisfy the increasing demands of thin wall castings for automotive applications. This study has investigated the effects of T6 heat-treatment on the microstructures, the local mechanical properties of alloy phases and the fracture behavior of high vacuum die-cast AlSiMgMn alloys using in-situ scanning electron microscopy (SEM) in combination with nano-indentation testing. The microstructures of the alloys at as-cast and T6 treated conditions were compared and analyzed. It is found that the T6 heat treatment plays different roles in affecting the hardness and the Young’s modulus of alloy phases. This study also found that the T6 heat treatment would influence the failure modes of the alloys. The mechanisms of crack propagation in the as-cast and T6 treated alloys were also analyzed and discussed.


2012 ◽  
Vol 531-532 ◽  
pp. 596-599
Author(s):  
Kai Zhang ◽  
Shang Wen Lu ◽  
Yao Hui Ou ◽  
Xiao Dong Wang ◽  
Ning Zhong

The recently developed “quenching and partitioning” heat treatment and “quenching-partitioning-tempering” heat treatment are novel processing technologies, which are designed for achieving advanced high strength steels (AHSS) with combination of high strength and adequate ductility. In present study, a medium carbon steel containing Nb was subjected to the Q-P-T process, and both the microstructure and mechanical properties was studied. The experimental results show that the Nb-microalloyed steel demonstrates high tensile strength and relatively high elongation. The microstructure of the steel was investigated in terms of scanning electron microscope and transmission electron microscope, and the results indicate that the Q-P-T steel consist of fine martensite laths with dispersive carbide precipitates and the film-like interlath retained austenite. The orientation relationships between martensite and retained austenite is as well-known Kurdjurmov-Sachs relationship and Nishiyama-Wasserman relationship.


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