241. Surface Sampling Media for Multiple Element ICP Analysis

2003 ◽  
Author(s):  
M. Simmons
Keyword(s):  
Surface Sampling ◽  
Icp Analysis

scholarly journals Neelipleona and Symphypleona (Collembola) from a Sampling in the Mesovoid Shallow Substratum of the Sierra de Guadarrama National Park (Madrid and Segovia, Spain): Taxonomy and Biogeography

Insects ◽  
2021 ◽  
Vol 12 (3) ◽  
pp. 266
Author(s):  
Enrique Baquero ◽  
Rafael Jordana ◽  
Vicente M. Ortuño
Keyword(s):  
National Park ◽  
Ecological Niche ◽  
Mediterranean Area ◽  
Abundant Species ◽  
Species Level ◽  
Surface Sampling ◽  
Mesovoid Shallow Substratum ◽  
The Mediterranean

Megalothorax minimus (Neelidae) and Sphaeridia pumilis (Sminthurididae) had already been identified in surface sampling from Sierra de Guadarrama. In Europe, Sminthurinus gisini (Katiannidae) seems to be associated with environments at specific altitudes, and has little representation in this sampling. Pygmarrhopalites custodum Baquero and Jordana sp. nov. (Arrhopalitidae) coexists with two previously identified surface occurring species of the same family (P. elegans and Arrhopalites caecus). However, P. custodum is more abundant, indicating that it occupies an ecological niche tending to troglophile in the mesovoid shallow substratum (MSS). Moreover, it is also more abundant in the MSS of higher altitude corresponding to the bioclimatic zones cryo-oro-Mediterranean and oro-Mediterranean supra forest. Allacma cryptica Baquero and Jordana sp. nov. (Sminthuridae), is another species that had not been previously detected on the surface in the study area. A. cryptica is an addition to a genus which has eight described species. Gisinurus malatestai (Sminthuridae) appears well represented in the MSS, being a species present very occasionally in the Mediterranean area. Two species of the genera Sminthurides (Sminthurididae) and Fasciosminthurus (Bourletiellidae) have been found, but they could not have been identified to the species level. Finally, a few specimens of Dicyrtomina minuta (Dicyrtomidae), an abundant species on the surface, have been captured.

scholarly journals Hydrogenation of Furfural to Furfuryl Alcohol over Ru Particles Supported on Mildly Oxidized Biochar

Catalysts ◽  
2020 ◽  
Vol 10 (8) ◽  
pp. 934 ◽  
Author(s):  
Raoof Bardestani ◽  
Rouholamin Biriaei ◽  
Serge Kaliaguine
Keyword(s):  
Surface Density ◽  
Furfuryl Alcohol ◽  
Surface Segregation ◽  
Catalyst Support ◽  
Mild Oxidation ◽  
Tem Analysis ◽  
Original Contribution ◽  
Icp Analysis ◽  
Optimized Conditions ◽  
Autoclave Reactor

Catalytic hydrogenation of aldehydes is required as the stabilizing step in bio-oils conversion. Ruthenium supported on carbon was used in the present work for hydrogenation of furfural (FF) to furfuryl alcohol (FA). Converting a biochar with no surface area and low carboxyl groups surface density to an outstanding catalyst support using a very simple mild air/steam oxidation is the original contribution of this work. The mildly oxidized biochar is impregnated with a targeted loading of 2.5 wt.% Ru via ion-exchange, using Ru(NH3)6Cl2 precursor. ICP analysis shows that the mild oxidation increases Ru adsorption capacity of untreated biochar from 1.2 to 2.2 wt.%. H2 chemisorption and TEM analysis indicate that the preliminary mild oxidation leads to higher Ru dispersion. XPS analysis also shows that the treatment prevents Ru from surface segregation. The highest value of 93% FA selectivity at 53% FF conversion was obtained in a batch autoclave reactor under optimized conditions.

scholarly journals Comparison of materials used for cleaning equipment in retail food premises, and of two methods for the enumeration of bacteria on cleaned equipment and work surfaces

1970 ◽  
Vol 68 (2) ◽  
pp. 221-232 ◽  
Author(s):  
R. J. Gilbert
Keyword(s):  
Control Method ◽  
Field Trials ◽  
Surface Sampling ◽  
Step Procedure ◽  
Cleaning Equipment ◽  
Before And After ◽  
Plate Counts ◽  
Self Service ◽  
Materials Used ◽  
Retail Food

SUMMARYThere is no official scheme for testing disinfectants and detergent/disinfectants for use in the retail food trade and few recommended procedures have been given for the cleaning of equipment with these agents. Therefore, field trials were carried out in a large self-service store. Comparisons were made of the various cleaning efficiencies, as determined by bacterial plate counts, of detergent and disinfectant solutions and machine cleaning oils applied with either clean cloths or disposable paper towels to items of equipment. The most satisfactory results were always obtained when anionic detergent (0·75 % w/v) and hypochlorite (200 p.p.m. available chlorine) solutions were applied in a ‘two-step’ procedure.Tests were made to compare the calcium alginate swab-rinse and the agar sausage (Agaroid) techniques for the enumeration of bacteria on stainless steel, plastic, formica and wooden surfaces before and after a cleaning process. Although recovery rates were always greater by the swab-rinse technique, the agar sausage technique was considered to be a useful routine control method for surface sampling.

Concentration Depth Profiles of Microplastic Particles in River Flow and Implications for Surface Sampling

2021 ◽  
Vol 55 (9) ◽  
pp. 6032-6041
Author(s):  
Win Cowger ◽  
Andrew B. Gray ◽  
James J. Guilinger ◽  
Brandon Fong ◽  
Kryss Waldschläger
Keyword(s):  
River Flow ◽  
Surface Sampling ◽  
Depth Profiles ◽  
Concentration Depth Profiles

Directed sampling using remote sensing with a response surface sampling design for site-specific agriculture

2006 ◽  
Vol 53 (2) ◽  
pp. 98-112 ◽  
Author(s):  
Glenn J. Fitzgerald ◽  
Scott M. Lesch ◽  
Edward M. Barnes ◽  
William E. Luckett
Keyword(s):  
Remote Sensing ◽  
Response Surface ◽  
Sampling Design ◽  
Surface Sampling ◽  
Site Specific

scholarly journals Evaluation of Two Surface Sampling Methods for Detection of Erwinia herbicola on a Variety of Materials by Culture and Quantitative PCR

2007 ◽  
Vol 73 (11) ◽  
pp. 3505-3510 ◽  
Author(s):  
Mark P. Buttner ◽  
Patricia Cruz ◽  
Linda D. Stetzenbach ◽  
Tracy Cronin
Keyword(s):  
Quantitative Pcr ◽  
Sampling Methods ◽  
Collection Efficiency ◽  
Test Chamber ◽  
Surface Sampling ◽  
Laminate Glass ◽  
Erwinia Herbicola ◽  
Surface Samples ◽  
Sampling Protocols ◽  
Surface Materials

ABSTRACT This research was designed to evaluate surface sampling protocols for use with culture and quantitative PCR (QPCR) amplification assay for detection of the gram-negative bacterial biothreat simulant Erwinia herbicola on a variety of surface materials. Surfaces selected for evaluation were wood laminate, glass and computer monitor screens, metal file cabinets, plastic arena seats, nylon seat cushions, finished concrete flooring, and vinyl tile flooring. Laboratory and test chamber studies were performed to evaluate two sampling methods, a sponge and a macrofoam swab, for detection of E. herbicola on surface materials. In laboratory trials, seven materials were inoculated with a known concentration of E. herbicola cells and samples were collected from the surfaces of the materials to determine sampling efficiencies. Culture analysis was ineffective for assessing E. herbicola collection efficiency because very few culturable cells were obtained from surface samples. QPCR demonstrated that E. herbicola DNA was present in high concentrations on all of the surface samples, and sampling efficiencies ranged from 0.7 to 52.2%, depending on the sampling method and the surface material. The swab was generally more efficient than the sponge for collection of E. herbicola from surfaces. Test chamber trials were also performed in which E. herbicola was aerosolized into the chamber and allowed to settle onto test materials. Surface sampling results supported those obtained in laboratory trials. The results of this study demonstrate the capabilities of QPCR to enhance the detection and enumeration of biocontaminants on surface materials and provide information on the comparability of sampling methods.

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