Stainless steel imitative crack using X-ray LIGA with suspension electroplating technique

2020 ◽  
Vol 64 (1-4) ◽  
pp. 31-37
Author(s):  
Jirawan Monkrathok ◽  
Jongkol Srithorn ◽  
Isaratat Phung-On ◽  
Rungrueang Phatthanakun

In this research, the Synchrotron X-ray lithography (X-ray LIGA) was implemented to fabricate imitative Stress Corrosion Crack (SCC) for using as a reference specimen of electromagnetic NDT. A pattern of the imitative SCC was created by using X-ray LIGA with controllable shape and size in precise details. The pattern created had a high aspect ratio, which was formed on SU-8 polymer. As a preliminary experiment, the prepared pattern was inserted into a block of pure Nickel formed by an electroplating technique. To develop a reference comparable to stainless steel in terms of electromagnetic response, the technique called “Suspension Electroplating” was implemented to create a block of material from its powder form. A rough magnetic response was then measured by Eddy Current Testing (ECT). The results showed the possibility of creating the desired properties of stainless steel. The SCC pattern will be then inserted to become the reference specimen.

Author(s):  
Benli Wan ◽  
Bin Hu ◽  
Yuntao Li ◽  
Yuhong Zhu

The induced ferrite and other high magnetic microstructures content changes are studied when 304 austenitic stainless steel stripe specimens are tested under different uniaxial tension deformation, namely its deformation less than 50%. Furtherly, the correlation is plotted between the resulting magnetic permeability or coercivity caused by these microstructures and deformation. Meanwhile, the optimal eddy current excitation frequency under different deformation was obtained, which was consistent with 3-D finite element analysis (FEA). Besides, other various factors affecting the quality of eddy current testing (ECT), such as temperature and conductivity, are also considered comprehensively during the tensile test. The results of the experiment and simulation calculation show that when the deformation is within 50% that necking deformation has occurred, the magnetic permeability of specimens increases with deformation, and gradually begin to have the magnetic properties of weak ferromagnetic materials, which also changes the optimal excitation frequency, which varies from 60 kHz to 110 kHz. Because of the electromagnetic response noise increase, the impedance plane diagrams of defects distort simultaneously, which leads to the quantitative evaluation error of defects.


2020 ◽  
Vol 64 (1-4) ◽  
pp. 47-55
Author(s):  
Takuma Tomizawa ◽  
Haicheng Song ◽  
Noritaka Yusa

This study proposes a probability of detection (POD) model to quantitatively evaluate the capability of eddy current testing to detect flaws on the inner surface of pressure vessels cladded by stainless steel and in the presence of high noise level. Welded plate samples with drill holes were prepared to simulate corrosion that typically appears on the inner surface of large-scale pressure vessels. The signals generated by the drill holes and the noise caused by the weld were examined using eddy current testing. A hit/miss-based POD model with multiple flaw parameters and multiple signal features was proposed to analyze the measured signals. It is shown that the proposed model is able to more reasonably characterize the detectability of eddy current signals compared to conventional models that consider a single signal feature.


2007 ◽  
Vol 2007 (suppl_26) ◽  
pp. 61-66 ◽  
Author(s):  
B. Peplinski ◽  
B. Adamczyk ◽  
G. Kley ◽  
K. Adam ◽  
F. Emmerling ◽  
...  

2009 ◽  
Vol 59 (12) ◽  
Author(s):  
Claudia Maria Simonescu ◽  
Valentin Serban Teodorescu ◽  
Camelia Capatina

This paper presents the obtaining of copper sulfide CuS (covelite) from Cu(CH3COO)2.H2O and thioacetamide (TAA) system. The reaction was conducted in presence or absence of sodium-bis(2-ethylhexyl) sulfosuccinate (Na-AOT). The effects of various reaction parameters on the size and on the shape of nanoparticles have been examined. CuS obtained was characterized by X ray diffraction, IR spectroscopy, TEM � transmission electron microscopy and SAED selected area electron diffraction. The influence of surfactant to the shape and size of CuS (covellite) nanocrystals was established. The size of the nanocrystals varied from 10-60 nm depending on the reaction conditions such as quantity of surfactant.


Author(s):  
Ali Abboud ◽  
Ali AlHassan ◽  
Benjamin Dönges ◽  
Jean Sebastian Micha ◽  
Robert Hartmann ◽  
...  

CrystEngComm ◽  
2021 ◽  
Vol 23 (11) ◽  
pp. 2215-2221
Author(s):  
Emma Dennis ◽  
Soumya Kundu ◽  
Deepak Thrithamarassery Gangadharan ◽  
Jingjun Huang ◽  
Victor M. Burlakov ◽  
...  

Well-oriented PbBr2 microwires with a length-to-width ratio of up to 5000 were grown using a concentration gradient in co-crystallization with perovskite. Planar-integrated microwires showed a response to X-ray photons.


2020 ◽  
Vol 58 ◽  
pp. 443-457
Author(s):  
Sandeep Kuriakose ◽  
Paolo Parenti ◽  
Massimiliano Annoni

Sign in / Sign up

Export Citation Format

Share Document