Preparation of Hydroxyapatite Coating by Using Citric Acid Sodium Citrate Buffer System in the Biomimetic Procedure

2013 ◽  
Vol 55 (10) ◽  
pp. 782-788 ◽  
Author(s):  
Ibrahim Aydin ◽  
Hakan Cetinel ◽  
Ahmet Pasinli ◽  
Mithat Yuksel
2016 ◽  
Vol 58 (2) ◽  
pp. 140-145 ◽  
Author(s):  
İbrahim Aydin ◽  
Hakan Çetinel ◽  
Ahmet Pasinli ◽  
Mithat Yuksel

1987 ◽  
Vol 26 (7) ◽  
pp. 1291-1296 ◽  
Author(s):  
Binay K. Dutta ◽  
Ranjan K. Basu ◽  
Amit Pandit ◽  
Parthasarathi Ray

1989 ◽  
Vol 72 (2) ◽  
pp. 374-377
Author(s):  
G William Chase ◽  
William O Landen ◽  
Leslie T Gelbaum ◽  
Abdel-Gawad M Soliman

Abstract An ion-exchange chromatographic method was developed to determine hypoglycin A (HG-A) levels in canned ackee fruit by using an amino acid analyzer. HG-A was extracted by homogenizing the sample in 80% alcohol. An isocratic buffer system, consisting of 30% sodium citrate buffer (pH 3.15) and 70% sodium chloride-sodium acetate buffer (pH 7.40) was used to obtain baseline separation between HG-A and the other amino acids. The system can detect HGA levels as low as 4.8 μg/mh. HG-A levels in the edible portion of fruit in 6 cans ranged from 11.0 to 66.5 mg HG-A/can. Recoveries by standard addition averaged 102.5%.


2009 ◽  
Vol 2009 (12) ◽  
pp. pdb.rec12040-pdb.rec12040

Holzforschung ◽  
2011 ◽  
Vol 65 (4) ◽  
Author(s):  
Ilabahen Patel ◽  
Roland Ludwig ◽  
Dietmar Haltrich ◽  
Thomas Rosenau ◽  
Antje Potthast

Abstract The chemoenzymatic modification of cellulosic pulps by the laccase-mediator system (LMS) consisting of laccase (EC 1.10.3.2) and the 2,2,6,6-tetramethylpiperidine-1-oxyl radical (TEMPO) has been investigated. The reaction proceeds under mild aqueous conditions (sodium citrate buffer pH 6, 30°C) and introduces primarily aldehyde groups into cellulose so that carboxyl groups amount to one-third to one-fifth of the carbonyl groups only. LMS treatment caused uniform oxidation of the material, also in the high-molecular weight area, which is a non-typical behavior compared to other chemical oxidations of cellulose. Treatment of the pulp only with TEMPO or only with laccase caused no changes whatsoever, whereas treatment with the TEMPO-derived oxoammonium ion (in the absence of laccase) introduced carbonyl groups into the pulp, but no carboxyls. This chemoenzymatic approach was compared to the well-known chemical approach by means of TEMPO and hypohalite. Both approaches yielded comparable distributions of functional groups at the low oxidation degrees studied, indicating a similar reaction mechanism with the TEMPO-derived oxoammonium ion being the actual oxidant. The laccase is able to generate this oxoammonium ion, which in turn oxidized the 6-hydroxymethyl group into the corresponding aldehyde.


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