Selection of operating conditions for multiple-element analysis by inductively coupled plasma-atomic emission spectrometry; an application of optimization methodology in analytical chemistry

1981 ◽  
Author(s):  
A.E. Brookes ◽  
J.J. Leary ◽  
D.W. Golightly
2000 ◽  
Vol 95 ◽  
pp. 219-238 ◽  
Author(s):  
Efi Karantzali ◽  
Matthew J. Ponting

This paper presents the results of the chemical analyses by inductively coupled plasma atomic emission spectrometry (ICP-AES) of a selection of vases from the recent excavations of Mycenaean tombs at Pylona, Rhodes. The data are used to support and confirm the stylistic attributions of the vases as either local Rhodian products or mainland imports. It is suggested that the majority of the imports are from the Argolid, but that at least one other origin is likely as well. Two distinct compositional groups of ‘local’ pottery are also identified. Comparison is made with the data from the analyses of pottery from Ialysos and the veracity of the conclusions drawn from the earlier optical emission data is confirmed.


2021 ◽  
pp. 108-116
Author(s):  
F.N. Karachevtsev ◽  
◽  
R.M. Dvoretskov ◽  
T.N. Zagvozdkina ◽  
А.V. Slavin ◽  
...  

A method is proposed for the determination of titanium and zirconium by inductively coupled plasma atomic emission spectrometry in aluminum alloys. Analytical lines of titanium and zirconium free from other elements significant spectral overlaps are selected. The selection of the sample preparation method was carried out, namely – dissolution in concentrated nitric acid. Studies of the metrological characteristics of the technique were carried out: for titanium and zirconium contents from 0.05 to 0.3 % of the mass. the accuracy index is no more than 5 % rel., which fully ensures the possibility of analytical control of the content of titanium and zirconium in products from aluminum alloys.


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