scholarly journals Preparation of Nano-silica Fume Coating Rubber Composite Particle and Its Application in Toughening the Oil Well Cement Stone

2018 ◽  
Author(s):  
Chengbao Wu ◽  
Guosheng Gai ◽  
Ju Tian ◽  
Yufen Yang ◽  
Chuansheng Liu ◽  
...  
Keyword(s):  
Silica Fume ◽  
Composite Particle ◽  
Cement Stone ◽  
Oil Well ◽  
Nano Silica ◽  
Rubber Composite ◽  
Oil Well Cement ◽  
Well Cement

Influence of sulfuric and hydrochloric acid on the resistance of geopolymer cement with nano-silica additive for oil well cement application

2018 ◽  
Vol 9 (5) ◽  
pp. 616-624 ◽  
Author(s):  
Syahrir Ridha ◽  
Afif Izwan Abd Hamid ◽  
Riau Andriana Setiawan ◽  
Ahmad Radzi Shahari
Keyword(s):  
Fly Ash ◽  
Hydrochloric Acid ◽  
Strength Increase ◽  
Oil Well ◽  
Nano Silica ◽  
Content Type ◽  
Oil Well Cement ◽  
Geopolymer Cement ◽  
Well Cement ◽  
Silica Additive

PurposeThe purpose of this paper is to investigate the resistivity of geopolymer cement with nano-silica additive toward acid exposure for oil well cement application.Design/methodology/approachAn experimental study was conducted to assess the acid resistance of fly ash-based geopolymer cement with nano-silica additive at a concentration of 0 and 1 wt.% to understand its effect on the strength and microstructural development. Geopolymer cement of Class C fly ash and API Class G cement were used. The alkaline activator was prepared by mixing the proportion of sodium hydroxide (NaOH) solutions of 8 M and sodium silicate (Na2SiO3) using ratio of 1:2.5 by weight. After casting, the specimens were subjected to elevated curing condition at 3,500 psi and 130°C for 24 h. Durability of cement samples was assessed by immersing them in 15 wt.% of hydrochloric acid and 15 wt.% sulfuric acid for a period of 14 days. Evaluation of its resistance in terms of compressive strength and microstructural behavior were carried out by using ELE ADR 3000 and SEM, respectively.FindingsThe paper shows that geopolymer cement with 1 wt.% addition of nano-silica were highly resistant to sulfuric and hydrochloric acid. The strength increase was contributed by the densification of the microstructure with the addition of nano-silica.Originality/valueThis paper investigates the mechanical property and microstructure behavior of emerging geopolymer cement due to hydrochloric and sulfuric acids exposure. The results provide potential application of fly ash-based geopolymer cement as oil well cementing.

Mechanical Properties and Microstructure of Epoxy Resin Enhanced Oil-Well Cement Stone

2019 ◽  
Vol 944 ◽  
pp. 1103-1107
Author(s):  
Ming Dan He ◽  
Ming Li ◽  
Yong Jin Yu ◽  
Hao Wang ◽  
Wei Yuan Xiao ◽  
...  
Keyword(s):  
Tensile Strength ◽  
Compressive Strength ◽  
Epoxy Resin ◽  
Performance Testing ◽  
Cement Stone ◽  
Oil Well ◽  
Oil Well Cement ◽  
Waterborne Epoxy ◽  
Waterborne Epoxy Resin ◽  
Well Cement

To adequately understand the waterborne epoxy resin and enhance the compressive, tensile strength of oil-well cement stone, the cement composite materials were prepared with different addition of waterborne epoxy resin, and the specimens were cured for 3days, 7 days, 14days, 28days at 50°C thermostatic water bath to test the compressive strength and tensile strength, respectively. The results showed when the content of resin emulsion is 30%, the compressive strength and tensile strength of the cement are increased by 303.09% and 306.04% compared with pure cement, respectively. Obviously, in the mechanical performance testing, oil-well cement stone modified by waterborne epoxy resin have been significantly improved compared with the pure cement. To explore the enhanced microstructure of oil-well cement modified with waterborne epoxy resin, the cement specimens were prepared with 30% waterborne epoxy resin analyzed by scanning electron microscopy (SEM).

Research Status of Synthetic Oil Well Cement Retarder

2020 ◽  
Vol 14 ◽  
Author(s):  
Guo Zihan ◽  
Liu Ziyang ◽  
Liao Kai ◽  
Yang Xianghui
Keyword(s):  
Great Influence ◽  
Large Temperature ◽  
Strength Development ◽  
Cement Stone ◽  
Oil Well ◽  
Research Status ◽  
Synthetic Oil ◽  
Oil Well Cement ◽  
Cement Retarder ◽  
Well Cement

: Oil well cement retarder is an additive that can extend time for thickening cement slurry, which can ensure the safety of cement. At present, the oil well cement retarder is mainly composed of synthetic materials, which are mainly divided into three major categories: compound polymer, AMPS polymer and non-AMPS. In this paper, the research status of synthetic oil well cement retarder in recent years is reviewed, and its shortcomings and development trends are analyzed. It is pointed out that the shortage of synthetic retarder mainly lies in problems, including large temperature sensitivity, small temperature application range, abnormal thickening curve, great influence on high temperature settlement stability and cement stone strength development. The development direction of oil well cement retarder is mainly focused on developing intelligent retarder and degradable retarder to meet the cementing needs of oilfields and ensure cementing effect increasing steadily.

Compressive Strength Changing Law of Oil Well Cement Paste under Corporate Corrosion of HCO3- and SO42-

2012 ◽  
Vol 229-231 ◽  
pp. 95-99 ◽  
Author(s):  
Yu Wang ◽  
Yu Feng Chen ◽  
Yan Lu ◽  
Hui Fang Zhang ◽  
Zhi Guo Sun
Keyword(s):  
Compressive Strength ◽  
Influence Factors ◽  
Ion Concentration ◽  
Solution Temperature ◽  
Cement Stone ◽  
Corrosion Mechanism ◽  
Oil Well ◽  
Experimental Conditions ◽  
Oil Well Cement ◽  
Well Cement

On the basis of analyzing the oil well cement corrosion mechanism by SO42- and HCO3-, the corrosion products, microstructure and compressive strength of cement stone were measured and the changing regularity and influence factors of compressive strength were analyzed under different experimental conditions. The following conclusions can be drawn. Under the interactive corrosion effect of SO42- and HCO3-, Ca(OH)2 in cement stone was dissolved out and consumed, the calcium silicate hydrate was decomposed, ettringite, gypsum, calcite and thaumasite were produced which destroyed the structure and components of cement stone primary products and led the compressive strength of corrosion cement stone decline. With the increases of ion concentration of corrosive solution, temperature and corrosive time, the compressive strength was decreased gradually, even collapsed completely.

scholarly journals Synergistic Effect of Latex Powder and Rubber on the Properties of Oil Well Cement-Based Composites

2018 ◽  
Vol 2018 ◽  
pp. 1-9 ◽  
Author(s):  
Jianjian Song ◽  
Mingbiao Xu ◽  
Weihong Liu ◽  
Xiaoliang Wang ◽  
Yumeng Wu
Keyword(s):  
Synergistic Effect ◽  
External Load ◽  
Oil And Gas ◽  
Fluid Loss ◽  
Cement Stone ◽  
Oil Well ◽  
Cement Slurry ◽  
Sem Images ◽  
Oil Well Cement ◽  
Well Cement

The brittleness and the poor resistance to external load of oil well cement impede the development of oil and gas wells. To overcome these deficiencies, latex powder or rubber and their hybrid combinations were used to modify the oil well cement. The conventional properties, mechanical properties, and scanning electron microscopy (SEM) images of the modified cement were analyzed. In comparison with latex powder-incorporated cement and rubber-incorporated cement, a significant improvement of fluid loss, flexural strength, impact strength, and elasticity of the cement slurry was observed when using the hybrid combinations of 3 wt.% latex powder and 2 wt.% rubber, although this synergistic effect was not remarkable on the compressive strength and the thickening time. These evidences arose from the synergism between latex powder and rubber leading to the formation of a three-dimensional network structure and a flexible structure which subsequently improved the elasticity and toughness of cement stone. The improved elastic matrix has a buffering effect on external impact when the cement stone is subjected to an external load.

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