scholarly journals Comparison Of Different Microwave Digestion Methods For Heavy Metals From Stream Sediment

2016 ◽  
Author(s):  
Zhenzhen Qiu ◽  
Jingdong Zhang ◽  
Chaoyang Liu ◽  
Fei Li ◽  
Zixian Wu
Keyword(s):  
Heavy Metals ◽  
Microwave Digestion ◽  
Stream Sediment ◽  
Digestion Methods

Analysis of Heavy Metals in Scalp Hair Samples of Hypertensive Patients by Conventional and Microwave Digestion Methods

2006 ◽  
Vol 39 (2) ◽  
pp. 203-214 ◽  
Author(s):  
Hassan Imran Afridi ◽  
Tasneem Gul Kazi ◽  
Mohammad Khan Jamali ◽  
Gul Hasan Kazi ◽  
Mohammad Bilal Arain ◽  
...  
Keyword(s):  
Heavy Metals ◽  
Scalp Hair ◽  
Microwave Digestion ◽  
Hypertensive Patients ◽  
Hair Samples ◽  
Digestion Methods

Determination of Residual Heavy Metals in an Incinerator Bottom Ash from Municipal Solid Waste Power Plant

2020 ◽  
Vol 901 ◽  
pp. 65-71
Author(s):  
Woravith Chansuvarn
Keyword(s):  
Heavy Metals ◽  
Power Plant ◽  
Municipal Solid Waste ◽  
Solid Waste ◽  
Microwave Digestion ◽  
Bottom Ash ◽  
Flame Atomic Absorption ◽  
Digestion Technique ◽  
Relative Standard ◽  
Copper Zinc

Bottom ash is a part of by-product from the municipal solid waste power plants which is always a wider problem for the urban and rural communities due to its disposal plants may cause serious environmental pollution. This work was focused on the residual heavy metal in an incinerator bottom ash from the municipal waste power plant placed in Nongkham district, Bangkok. Four bottom ash samples were obtained in 2017. After drying and grounding, the bottom ash samples were prepared to clear solution with the microwave digestion technique using nitric, hydrochloric and hydrofluoric acid under the heating program. The total residual heavy metals in the incinerator bottom ashes, such as lead, copper, zinc, and cadmium were determined by using flame atomic absorption spectrophotometer (FAAS) with deuterium background correction. The total concentration of lead, copper, zinc and cadmium were found in the range of 280.40-354.22mg kg-1, 365.35-524.45 mg kg-1, 1,527.25-2,074.34 mg kg-1, and 0.48-1.02 mg kg-1, respectively. The recovery of all metals was found in the range of 89.4-101.2% and the relative standard deviation (RSD) was to be 2.15-3.55 % (n=7). The concentration of zinc, copper, and lead was found high levels, while cadmium was low concentration. Heavy metals in solid waste material occur in different chemical forms and phases. The sample preparation based on the microwave digestion was successfully developed for the waste samples with a good reliability.

scholarly journals Heavy metal contamination and ecological risk assessment of the agricultural soil in Shanxi Province, China

2020 ◽  
Vol 7 (10) ◽  
pp. 200538
Author(s):  
Hongxue Qi ◽  
Bingqing Zhao ◽  
Lihong Li ◽  
Xiuling Chen ◽  
Jing An ◽  
...  
Keyword(s):  
Heavy Metals ◽  
Ecological Risk ◽  
Inductively Coupled Plasma ◽  
Agricultural Soil ◽  
Heavy Metal Contamination ◽  
Microwave Digestion ◽  
Risk Index ◽  
Shanxi Province ◽  
Ecological Risks ◽  
Geo Accumulation

To assess contamination levels and ecological risks of heavy metals in agricultural soil from Shanxi Province of China, a total of 33 samples in the surface soil were collected from 11 cities in Shanxi. The soil samples were digested by a mixed acid of nitric acid and hydrofluoric acid on a microwave digestion system, then the levels of eight heavy metals were analysed using an inductively coupled plasma mass spectrometer. The pollution levels of soil heavy metals were evaluated using a geo-accumulation index and their ecological risks were assessed using risk index calculated by Hakanson's method. As a result, the average concentrations of the heavy metals As, Cd, Cr, Cu, Hg, Ni, Pb and Zn were 12.9 ± 4.8, 0.35 ± 0.23, 43 ± 14, 27 ± 19, 0.25 ± 0.14, 21.7 ± 5.7, 17 ± 13 and 89 ± 53 mg kg −1 , respectively. By comparison to the Chinese soil environmental quality (GB15618-2018), only 9% of Cd samples and 3% of Cu samples exceeded their corresponding screening criteria. Subsequently, the results of geo-accumulation indices suggested that Shanxi's soil suffered from moderate to heavy contamination posed by Cd and Hg, and risk indices exhibited a similar trend that Cd and Hg were the main contributors for considerable to very high ecological risk. Finally, the analysis of variance indicated that the mean levels of Cd significantly occurred at Yuncheng areas among the 11 cities ( n = 3, p < 0.05), but Hg concentrations did not have significantly statistical differences. This study demonstrated that metals Cd and Hg had higher levels and ecological risks for agricultural soil in Shanxi, especially, Yuncheng City suffered from heavy Cd contamination. The findings of the present study will provide basic information on management and control of the agricultural soil contamination in Shanxi Province, China.

scholarly journals Geochemical assessment of heavy metal pollution of river basin in Nigeria using stream sediment

2020 ◽  
Vol 7 (2) ◽  
pp. 198
Author(s):  
Oluwafunso Oladipo Awosusi ◽  
Adeshina Luqman Adisa
Keyword(s):  
Heavy Metals ◽  
Heavy Metal ◽  
Enrichment Factor ◽  
River Basin ◽  
Metal Pollution ◽  
Heavy Metal Pollution ◽  
Stream Sediment ◽  
The Body ◽  
The Mean ◽  
Mean Concentration

Heavy metal pollution has been a source of health problems in humans. These metals are persistent, toxic, non-degradable and often take a long time to be eliminated from the body. This study is, therefore, designed to assess heavy metal pollution of River Basin in Nigeria. Seventy stream sediment samples were systematically collected from an area, approximately 400km2, latitude 7O 00’ and 7O 15’N and longitude 5O 11’ and 5O 19’E. The pollution status of the sediments by heavy metals were assessed by Enrichment Factor (EF), Pollution Load Index (PLI) and Geo-accumulation Index (Igeo). The concentrations of the heavy metals were also compared with United States Environmental Protection Agency (USEPA) Sediment quality guidelines (SQG). The samples were dried in the laboratory, disaggregated, sieved to minus 80 (<177 microns) mesh size using nylon sieve. The sieved samples were, then, digested and the concentrations of As, Co, Fe, Mn, Ni, Pb, V and Zn were determined by Wavelength Dispersive X-ray Fluorescence Spectrometry (WD-XRFS). Results revealed that the mean concentrations of the heavy metals are in the order V>Zn>Pb>As>Ni>Co>Fe>Mn. Furthermore, the mean concentration of lead exceeded both the average world shale and the USEPA SQG values. However, the mean concentration of cobalt, nickel, manganese and zinc were lower than the average world shale values for these elements. The Enrichment Factor (EF) revealed that cobalt was moderately enriched while arsenic and lead were significantly enriched in the sediments. On the basis of the geoaccumulation index, the stream sediments were largely uncontaminated except at some sites that were moderately to strongly contaminated by As and Pb.  

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