scholarly journals Supporting information on “2H chemical-shift resolution and dipolar 2H-1H,2H-15N correlations in solid-state MAS NMR spectroscopy for structure determination and distance measurements in hydrogen-bonded systems”

2005 ◽  
Vol 3 (2) ◽  
pp. SI1-SI12
Author(s):  
Martin Schulz-Dobrick ◽  
Ingo Schnell
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Structure Determination ◽  
Mas Nmr ◽  
Distance Measurements ◽  
Hydrogen Bonded Systems ◽  
Hydrogen Bonded

scholarly journals 2H Chemical-shift resolution and dipolar2H-1H,2H-15N correlations in solid-state MAS NMR spectroscopy for structure determination and distance measurements in hydrogen-bonded systems

2005 ◽  
Vol 3 (2) ◽  
pp. 245-251 ◽  
Author(s):  
Martin Schulz-Dobrick ◽  
Ingo Schnell
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Magic Angle Spinning ◽  
Magic Angle ◽  
Distance Measurements ◽  
Biomolecular Systems ◽  
Angle Spinning ◽  
Hydrogen Bonded Systems ◽  
Fast Magic Angle Spinning

AbstractIn solid-state NMR, deuteron (2H) spectroscopy can be performed in full analogy to1H spectroscopy, including2H chemical-shift resolution and2H-X dipolar correlation schemes, when the NMR experiments are conducted in a “rotor-synchronized” fashion under fast magic-angle spinning. Here, 2H-X NMR experiments of this type, including2H-15N and2H-1H chemical-shift correlations and distance measurements, are introduced and demonstrated on cytosine monohydrate, whose acidic protons can readily be replaced by deuterons by recrystallization from D2O. In this way,2H NMR spectroscopy provides information complementary to1H NMR data, which is particularly useful for studying hydrogen bonds in supra- or biomolecular systems.

De Novo 3D Structure Determination from Sub-milligram Protein Samples by Solid-State 100 kHz MAS NMR Spectroscopy

2014 ◽  
Vol 53 (45) ◽  
pp. 12253-12256 ◽  
Author(s):  
Vipin Agarwal ◽  
Susanne Penzel ◽  
Kathrin Szekely ◽  
Riccardo Cadalbert ◽  
Emilie Testori ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Structure Determination ◽  
De Novo ◽  
3D Structure ◽  
Mas Nmr ◽  
3D Structure Determination

scholarly journals Investigations of Uranyl Fluoride Sesquihydrate (UO2F2·1.57H2O): Combining 19F Solid-State MAS NMR Spectroscopy and GIPAW Chemical Shift Calculations

2018 ◽  
Vol 122 (34) ◽  
pp. 6873-6878 ◽  
Author(s):  
Michael A. DeVore ◽  
Christopher A. Klug ◽  
Maria R. Kriz ◽  
Lindsay E. Roy ◽  
Matthew S. Wellons
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Chemical Shift ◽  
Mas Nmr ◽  
Chemical Shift Calculations

Investigating Sorption on Iron−Oxyhydroxide Soil Minerals by Solid-State NMR Spectroscopy:  A6Li MAS NMR Study of Adsorption and Absorption on Goethite

2005 ◽  
Vol 109 (39) ◽  
pp. 18310-18315 ◽  
Author(s):  
Ulla Gro Nielsen ◽  
Younkee Paik ◽  
Keinia Julmis ◽  
Martin A. A. Schoonen ◽  
Richard J. Reeder ◽  
...  
Keyword(s):  
Solid State ◽  
Nmr Spectroscopy ◽  
Solid State Nmr ◽  
Mas Nmr ◽  
Iron Oxyhydroxide ◽  
Soil Minerals ◽  
Solid State Nmr Spectroscopy ◽  
Nmr Study

Hydrogen Elimination and Solid-State Reaction in Hydrogen-Bonded Systems under Pressure:  The Case of HBr

2000 ◽  
Vol 104 (49) ◽  
pp. 11801-11804 ◽  
Author(s):  
Takashi Ikeda ◽  
Michiel Sprik ◽  
Kiyoyuki Terakura ◽  
Michele Parrinello
Keyword(s):  
Solid State ◽  
Solid State Reaction ◽  
Hydrogen Elimination ◽  
Hydrogen Bonded Systems ◽  
Hydrogen Bonded
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