scholarly journals Determination of selenium in infant foods using electrothermal atomic absorption spectrometry with direct slurry sample introduction

2004 ◽  
Vol 2 (2) ◽  
pp. 334-346 ◽  
Author(s):  
Danuta Baralkiewicz ◽  
Usama El-Sayed ◽  
Marian Filipiak ◽  
Hanka Gramowska ◽  
Miroslaw Mleczek

AbstractSlurry sampling electrothermal atomic absorption (SS ETAAS) was applied to the development of a sensitive and precise method for selenium determination in infant foods without sample pretreatment. Suspensions prepared in a medium containing 0.1% Triton X-100, 0.5 or 5% v/v concentrated HNO3 were directly introduced into the furnace. The accuracy of the procedure was confirmed by analysis of a standard reference material and comparison with hydride generation atomic absorption spectrometric (HGAAS) procedure. The characteristic mass is 44 pg and detection limit 0.43 μg·l−1.

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