scholarly journals The fabrication of particulate composite by in situ oxidation process.

1992 ◽  
Vol 42 (3) ◽  
pp. 138-142 ◽  
Author(s):  
Makoto KOBASHI ◽  
Takao CHOH
Author(s):  
K. R. Lawless ◽  
J. V. Cathcart ◽  
E. A. Kenik

Ni3Al is subject to dynamic embrittlement when tested in an oxidizing environment; whereas pre-oxidation under stress does not embrittle the alloy. In situ HVEM oxidation studies of several ordered intermetallic (LI2 structure) Ni3Al alloys with small additions of boron and hafnium are reported. AEM studies of the oxidized specimens were also made to fully characterize the microstructure. Specimens were annealed and then electropolished to penetration just prior to insertion in the hot stage of the HVEM. Oxidations were carried out at an oxygen pressure of 13-60 mPa at 750°C. Gas pressure and composition were monitored with a residual gas analyzer. Specimens raised to the operating temperature in the base vacuum (∼0.2 mPa) showed no indication of oxide in the diffraction pattern and were almost entirely free of dislocations.Many of the features of different stages of the oxidation process are shown in Fig. 1. After two minutes exposure to oxygen, a thin, fine-grained, oriented, polycrystalline region of primarily γ-Al2O3 developed at the thinnest regions of the foil (Region A in Fig. 1 and Fig. 2).


2017 ◽  
Vol 5 (13) ◽  
pp. 6052-6059 ◽  
Author(s):  
Qian Wang ◽  
Zhen-Bo Wang ◽  
Chao Li ◽  
Da-Ming Gu

Microporous carbon coated sulfur composites with a double-hollow-sphere structure are prepared through anin situoxidation process.


2011 ◽  
Vol 3 (3) ◽  
pp. 789-794 ◽  
Author(s):  
Guanghui Cui ◽  
Dezhen Wu ◽  
Shengli Qi ◽  
Shao Jin ◽  
Zhanpeng Wu ◽  
...  

1999 ◽  
Author(s):  
VIRGINIA UNIV CHARLOTTESVILLE
Keyword(s):  

2021 ◽  
Vol 22 (1) ◽  
pp. 141-148
Author(s):  
Weini Jia ◽  
Shirong Li ◽  
Zhengxin Luo ◽  
Hainan Yu ◽  
Wenjun Zhu ◽  
...  
Keyword(s):  

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