scholarly journals In situ observation with x-ray for tentative exploration of laser beam welding processes for aluminum-based alloys

2021 ◽  
Vol 33 (1) ◽  
pp. 012026
Author(s):  
Stephan Börner ◽  
Dirk Dittrich ◽  
Philipp Mohlau ◽  
Christoph Leyens ◽  
Francisco García-Moreno ◽  
...  
2021 ◽  
Vol 33 (4) ◽  
pp. 042043
Author(s):  
Yuji Sato ◽  
Naoki Shinohara ◽  
Tomoki Arita ◽  
Masami Mizutani ◽  
Tomomasa Ohkubo ◽  
...  

1993 ◽  
Vol 308 ◽  
Author(s):  
Paul R. Besser ◽  
Thomas N. Marieb ◽  
John C. Bravman

ABSTRACTStrain relaxation in passivated Al-0.5% Cu lines was measured using X-ray diffraction coupled with in-situ observation of the formation and growth of stress induced voids. Samples of 1 μm thick Al-0.5% Cu lines passivated with Si3N4 were heated to 380ºC, then cooled and held at 150ºC. During the test, principal strains along the length, width, and height of the line were determined using a grazing incidence x-ray geometry. From these measurements the hydrostatic strain in the metal was calculated and strain relaxation was observed. The thermal cycle was duplicated in a high voltage scanning transmission electron microscope equipped with a backscattered electron detector. The 1.25 μm wide lines were seen to have initial stress voids. Upon heating these voids reduced in size until no longer observable. Once the samples were cooled to 150ºC, voids reappeared and grew. The measured strain relaxation is discussed in terms of void and θ-phase (Al2Cu) formation.


2020 ◽  
Vol 326 ◽  
pp. 08005
Author(s):  
Mete Demirorer ◽  
Wojciech Suder ◽  
Supriyo Ganguly ◽  
Simon Hogg ◽  
Hassam Naeem

An innovative process design, to avoid thermal degradation during autogenous fusion welding of high strength AA 2024-T4 alloy, based on laser beam welding, is being developed. A series of instrumented laser welds in 2 mm thick AA 2024-T4 alloys were made with different processing conditions resulting in different thermal profiles and cooling rates. The welds were examined under SEM, TEM and LOM, and subjected to micro-hardness examination. This allowed us to understand the influence of cooling rate, peak temperature, and thermal cycle on the growth of precipitates, and related degradation in the weld and heat affected area, evident as softening. Although laser beam welding allows significant reduction of heat input, and higher cooling rates, as compared to other high heat input welding processes, this was found insufficient to completely supress coarsening of precipitate in HAZ. To understand the required range of thermal cycles, additional dilatometry tests were carried out using the same base material to understand the time-temperature relationship of precipitate formation. The results were used to design a novel laser welding process with enhanced cooling, such as with copper backing bar and cryogenic cooling.


ChemInform ◽  
2006 ◽  
Vol 37 (12) ◽  
Author(s):  
Katsuhiro Kobayashi ◽  
Tadashi Hata ◽  
Hiroshi Fukuhara ◽  
Yuji Ohashi
Keyword(s):  

2011 ◽  
Vol 59 (5) ◽  
pp. 1995-2008 ◽  
Author(s):  
H. Toda ◽  
E. Maire ◽  
S. Yamauchi ◽  
H. Tsuruta ◽  
T. Hiramatsu ◽  
...  

Nanoscale ◽  
2016 ◽  
Vol 8 (4) ◽  
pp. 1849-1853 ◽  
Author(s):  
S. E. R. Tay ◽  
A. E. Goode ◽  
J. Nelson Weker ◽  
A. A. Cruickshank ◽  
S. Heutz ◽  
...  

The nucleation and growth of a nanostructure controls its size and morphology, and ultimately its functional properties.


2018 ◽  
Vol 25 (6) ◽  
pp. 1673-1682 ◽  
Author(s):  
Adam S. Hoffman ◽  
Joseph A. Singh ◽  
Stacey F. Bent ◽  
Simon R. Bare

In situ characterization of catalysts gives direct insight into the working state of the material. Here, the design and performance characteristics of a universal in situ synchrotron-compatible X-ray diffraction cell capable of operation at high temperature and high pressure, 1373 K, and 35 bar, respectively, are reported. Its performance is demonstrated by characterizing a cobalt-based catalyst used in a prototypical high-pressure catalytic reaction, the Fischer–Tropsch synthesis, using X-ray diffraction. Cobalt nanoparticles supported on silica were studied in situ during Fischer–Tropsch catalysis using syngas, H2 and CO, at 723 K and 20 bar. Post reaction, the Co nanoparticles were carburized at elevated pressure, demonstrating an increased rate of carburization compared with atmospheric studies.


Sign in / Sign up

Export Citation Format

Share Document