Optimisation of TiN thin film synthesis by a novel combined laser/sol-gel processing technique

Author(s):  
Tamer Ezz ◽  
Philip Crouse ◽  
Lin Li ◽  
Zhu Liu
2015 ◽  
Vol 74 (3) ◽  
pp. 585-593 ◽  
Author(s):  
Jan Hegmann ◽  
Rainer Jahn ◽  
Steffi Schönau ◽  
Nicolas Sommer ◽  
Peer Löbmann

2005 ◽  
Vol 37 (12) ◽  
pp. 1092-1104 ◽  
Author(s):  
Neluta Ibris ◽  
Anna Maria Salvi ◽  
Massimiliano Liberatore ◽  
Franco Decker ◽  
Angela Surca

2006 ◽  
Vol 957 ◽  
Author(s):  
Lassaad El Mir ◽  
H.Jurgen von Bardeleben ◽  
M Saadoun ◽  
Aroussi Ben Mahmoud ◽  
Jean-Louis Cantin

ABSTRACTWe report the elaboration of Ni doped ZnO nanoparticles prepared by a sol-gel processing technique. In our approach the water for hydrolyse was slowly released by esterification of the metal acetate with methanol followed by a supercritical drying in ethyl alcohol. Doping concentrations between 5 and 25 at% have been investigated. In the as-prepared state the powders with an average particle size of 30nm present ferromagnetic properties; thermal annealing in the 500°C to 700°C temperature range in air or oxygen modifies the magnetic properties. We ascribe the observed ferromagnetism to the presence and transformation of Ni based secondary phases.


1992 ◽  
Vol 147-148 ◽  
pp. 442-446 ◽  
Author(s):  
Kunihiko Kojima ◽  
Fujio Mizukami ◽  
Mitsuharu Miyazaki ◽  
Kazuyuki Maeda

1994 ◽  
Vol 361 ◽  
Author(s):  
Robert W. Schwartz ◽  
R.A. Assink ◽  
D. Dimos ◽  
M.B. Sinclair ◽  
T.J. Boyle ◽  
...  

ABSTRACTSol-gel processing methods are frequently used for the fabrication of lead zirconate titanate (PZT) thin films for many electronic applications. Our standard approach for film fabrication utilizes lead acetate and acetic acid modified metal alkoxides of zirconium and titanium in the preparation of our precursor solutions. This report highlights some of our recent results on the effects of the addition of a second chelating ligand, acetylacetone, to this process. We discuss the changes in film drying behavior, densification and ceramic microstructure which accompany acetylacetone additions to the precursor solution and relate the observed variations in processing behavior to differences in chemical precursor structure induced by the acetylacetone ligand. Improvements in thin film microstructure, ferroelectric and optical properties are observed when acetylacetone is added to the precursor solution.


1990 ◽  
Vol 5 (5) ◽  
pp. 916-918 ◽  
Author(s):  
Ren Xu ◽  
Yuhuan Xu ◽  
Ching Jih Chen ◽  
John D. Mackenzie

Ferroelectric thin film of strontium-barium niobate was successfully fabricated by the sol-gel technique. The films were made on several types of substrate, including quartz, single crystal silicon wafer, and glass slides. The processing temperature was as low as 700 °C. The film obtained with thickness of 3000 Å was dense, transparent, and showed excellent ferroelectricity.


2016 ◽  
Vol 4 (21) ◽  
pp. 8308-8315 ◽  
Author(s):  
Ross A. Kerner ◽  
Lianfeng Zhao ◽  
Zhengguo Xiao ◽  
Barry P. Rand

We show that metal halide perovskite thin film formation is a sol–gel process which allows us to improve film morphology, achieving roughness ∼1 nm via process and additive engineering.


2012 ◽  
Author(s):  
Ahmad Sharmi Abdullah ◽  
Amirjan Nawabjan ◽  
Norazan Mohd Kassim ◽  
Mohd Haniff Ibrahim ◽  
Mohamad Zahid Abdul Malek

Pandu gelombang optik jalur berasaskan bahan–bahan sol–gel organik–bukan organic (hybrid) direka, disimulasi dan dibentuk. Bahan–bahan sol–gel hybrid tersebut disediakan daripada vinyltriethoxysilane (VTES), tetraethoxysilane (TEOS) dan tetrabutoxytitanate (TTBu) malalui kaedah pemprosesan sol–gel. Pandu gelombang optik tersebut telah dibentuk di atas lapisan quartz menggunakan kaedah penyalutan berputar, lithografi langsung, dan goresan kimia basah. Beberapa lapisan sol telah dibentuk demi mendapatkan struktur pandu gelombang dengan ketebalan yang sesuai untuk laluan mod cahaya sebagaimana diperolehi daripada simulasi. Kebolehan pandu gelombang untuk memandu cahaya pada panjang gelombang 1550 nm telah dicirikan mengunakan kaedah direct end–face fiber butt–coupling. Struktur fizikal pandu gelombang tersebut telah diperhatikan melalui mikroskop berkuasa tinggi. Keputusan yang diperolehi menunjukkan bahawa bahan yang dicadangkan boleh digunakan dalam aplikasi pemanduan gelombang optik pada panjang gelombang 1550 nm. Simulasi menunjukkan bahawa pandu gelombang jalur satu mod dapat direalisasikan jika ketebalan dan kelebaran pandu gelombang tersebut berada pada suatu julat nilai tertentu. Julat nilai tersebut dapat diperolehi melalui pengawalan parameter–parameter penyalutan berputar dan pembentukan mikro. Kualiti keratan rentas yang baik juga diperhatikan telah diperolehi melalui kaedah pembelahan semulajadi. Kata kunci: Pemprosesan sol–gel; bahan organik–bukan organic; pandu gelombang jalur Ridge optical waveguides based on organic–inorganic (hybrid) sol–gel materials were designed, simulated and fabricated. The hybrid sol–gel materials were synthesized from vinyltriethoxysilane (VTES), tetraethoxysilane (TEOS) and tetrabutoxytitanate (TTBu) precursors by means of sol–gel processing technique. The optical waveguides were fabricated on quartz substrate using spin coating, direct photolithography, and wet chemical etching techniques. Multiple layers of sol were deposited so as to obtain waveguide structure with suitable thickness for mode propagation such as acquired from the simulation. Waveguiding ability of the ridge optical waveguides at 1550 nm wavelength was characterized using direct end–face fiber butt–coupling method. Physical structure of the waveguides was observed through high power microscope. Observation showed that the proposed material possesses the ability for waveguiding application at the wavelength of 1550 nm. Simulation showed that a single mode ridge optical waveguide could be realized provided that the structure thickness and width are within certain range. The range is attainable through proper control of spin coating and micropatterning parameters. Acceptable end–face quality resulted from natural cleaving process was also discovered. Key words: Sol–gel processing; organic–inorganic material; ridge optical waveguide


2013 ◽  
Vol 320 ◽  
pp. 202-207 ◽  
Author(s):  
Lian Wei Shan ◽  
Lai Guo Wang ◽  
Wei Li ◽  
Li Min Dong ◽  
Zhi Dong Han ◽  
...  

Sr0.5Ba0.5-xBixTiO3 (SBT) thin films were fabricated on a Pt/SiO2/Si substrate by sol-gel method. The effects of chelating agent acetylacetone (HAcHAc) on the formation temperature and the microstructure of Sr0.5Ba0.5-xBixTiO3 (SBT) thin films were investigated in this paper. The microstructure of BST thin films was examined by XRD and TEM. It is found that Bi3+ doping decreases dielectric loss, improves frequency dispersion for BST thin films. The peak of temperature-dependence of dielectric constant of Bi3+-doped BST thin films is compressed and moves to a low-temperature region. An inclined angle of approximately 1.8o between the two different polarization vectors was observed for BST thin film from the results of high-resolution transmission electron microscopy (HRTEM). The Pr, Ps and Ec was 0.22μC/cm2, 0.72μC/cm2 and 60Kv/cm respectively for Sr0.5Ba0.485Bi0.015TiO3 thin film at 100Hz, 20V.


1995 ◽  
Vol 76 (1-2) ◽  
pp. 143-154 ◽  
Author(s):  
A Ahmad
Keyword(s):  
Sol Gel ◽  

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