Bond Strength of Adhesive Luting Agents to Caries-affected Dentin

2014 ◽  
Vol 39 (4) ◽  
pp. 383-388 ◽  
Author(s):  
CT Rocha ◽  
AL Faria-e-Silva ◽  
AC Peixoto
Keyword(s):  
Bond Strength ◽  
Resin Cement ◽  
Resin Cements ◽  
Tukey Test ◽  
Luting Agents ◽  
Adhesive Luting ◽  
Before And After ◽  
Ph Cycling ◽  
Relationship Of ◽  
The Relationship

SUMMARY Introduction: The aim of this study was to evaluate the bond strength of adhesive luting agents to caries-affected dentin (CAD). Methods: Forty human molars were sectioned to create dental slices presenting exposed occlusal dentin. Half of the samples were submitted to eight caries-induction demineralizing/mineralizing cycles. The pH-cycling model consisted of three hours in a demineralizing solution followed by 45 hours of immersion in a mineralizing solution. Dentin hardness was measured before and after the pH cycling. Resin cement cylinders were built up over the dentin surface using RelyX Unicem or RelyX ARC/Scotchbond Multipurpose Plus. The cement cylinders were submitted to shear load, and the data were analyzed using two-way analysis of variance (ANOVA) and Tukey test (p<0.05). Hardness data were also submitted to two-way ANOVA and Tukey test (p<0.05). The relationship of hardness vs bond strength was assessed via nonlinear regression analysis. Results: Sound dentin (tested and used in caries induction) showed similar values of hardness and were superior to CAD. Both resin cements showed higher bond strength to sound dentin than to CAD. Independent of substrate, RelyX ARC showed the highest values of bond strength. A positive linear relationship between dentin hardness and bond strength was observed for both cements evaluated. Conclusions: The adhesive luting agents evaluated showed lower bond strength to CAD.

Effects of Immediate Dentin Sealing and Pulpal Pressure on Resin Cement Bond Strength and Nanoleakage

2016 ◽  
Vol 41 (2) ◽  
pp. 189-199 ◽  
Author(s):  
VB Santana ◽  
RS de Alexandre ◽  
JA Rodrigues ◽  
C Ely ◽  
AF Reis
Keyword(s):  
Bond Strength ◽  
Negative Influence ◽  
Resin Cement ◽  
Microtensile Bond Strength ◽  
Resin Cements ◽  
Strength Data ◽  
Tukey Test ◽  
Luting Agents ◽  
Adhesive Luting ◽  
Scanning Electron

SUMMARY Objective: The object of this study was to evaluate the simulated pulpal pressure (SPP) and immediate dentin sealing technique (IDS) effects on the microtensile bond strength (μTBS) and nanoleakage of interfaces produced by different luting agents. Methods and Materials: Two self-adhesive luting agents (RelyX Unicem [UC] and Clearfil SA Luting [SA]) and two conventional luting agents (Rely X ARC [RX] and Panavia F [PF]) were evaluated. Eighty human molars were divided in four groups according to luting agents. Each group was subdivided according to SPP (with or without) and dentin sealing (immediate or delayed) using Clearfil SE Bond (n=5). After IDS was performed, specimens were stored in water for seven days before luting procedures. Composite blocks were luted according to the manufacturers' instructions. One half of the specimens were subjected to 15 cm H2O of hydrostatic pressure for 24 hours before cementation procedures and continued for 24 hours afterward. Then, restored teeth were sectioned into beams and tested in tension. Two additional teeth per group were prepared for nanoleakage evaluation with scanning electron microscopy. Bond strength data were statistically analyzed by three-way analysis of variance and Tukey test. Results: μTBS of RX decreased when it was subjected to SPP without IDS. However, in the same conditions, μTBS of UC increased. The IDS prevented negative influence of SPP on μTBS of RX and PF; however, a decrease in μTBS of SA and UC was observed. Except for RX, IDS increased μTBS for all resin cements. Conclusion: Independent of SPP, the IDS technique obtained higher μTBS for PF, SA, and UC and did not influence RX μTBS.

scholarly journals Bond Strength of Overdenture Locator Posts Cemented with Seven Luting Agents

2013 ◽  
Vol 14 (4) ◽  
pp. 675-680
Author(s):  
Khalil Aleisa
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Mean Value ◽  
Resin Cement ◽  
Control Group ◽  
Resin Cements ◽  
Human Teeth ◽  
Luting Agents ◽  
Relyx Unicem ◽  
Significant Difference

ABSTRACT Statement of the problem Post retention is crucial factor in restoration survival. Posts are commonly failed due to loss of retention. It is unknown which luting agents would provide the maximum bond strength for Locator overdenture posts. Aim The aim of this study was to evaluate the bond retentive strengths of Locator overdenture posts cemented with 7 luting agents. Materials and methods One hundred and five single rooted human teeth were decoronated and randomly assigned to 7 groups (n = 15). Post spaces were prepared with Locator post drills to the depth of 6 mm. The Locator posts were cemented with Variolink II, RelyX ARC, Multilink N, RelyX Unicem, ParaCore, or MultiCore Flow resin luting agents. Zinc phosphate cement was served as control group. Specimens were stored in water at 37°C for 24 hours. Each specimen was loaded in tension in an Instron universal testing machine. The maximum force required to dislodge each Locator post was recorded. Means and standard deviations were calculated and data were statistically analyzed with one-way analysis of variance (ANOVA). Results The highest mean bond strength value for Locator posts was recorded for MultiCore® Flow group (mean = 550.1 N), while the lowest mean value was for RelyX Unicem™ resin cement group (mean = 216.8 N). A statistically significant difference in mean locator overdenture post bond strength was observed between the 7 cement types (p < 0.0001). ParaCore™ and MultiCore® Flow groups had significantly higher bond strength than all other groups, but they were not differed from each other. Conclusion Bond strength of Locator overdenture posts were influenced by the type of luting agents. MultiCore Flow and ParaCore resin cements offered the greatest retention. Clinical significance The type of luting agents had a significant effect on the retention of Locator posts. The use of Core buildup resin cements as luting agent with Locator post demonstrated the greatest retention. How to cite this article Aleisa K. Bond Strength of Overdenture Locator Posts Cemented with Seven Luting Agents. J Contemp Dent Pract 2013;14(4):675-680.

Evaluation of the Microshear Bond Strength of MDP-containing and Non–MDP-containing Self-adhesive Resin Cement on Zirconia Restoration

2019 ◽  
Vol 44 (4) ◽  
pp. 379-385 ◽  
Author(s):  
EJ Go ◽  
Y Shin ◽  
JW Park
Keyword(s):  
Bond Strength ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Exact Test ◽  
Tukey Test ◽  
Significant Difference ◽  
Post Hoc ◽  
Microshear Bond Strength

SUMMARY Objectives: The purpose of this study was to measure the microshear bond strength (μSBS) of four different self-adhesive resin cements with/without 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-containing primer to zirconium ceramics and to evaluate the effect of zirconia primers on these self-adhesive resin cements (SARCs). Methods and Materials: Zirconia blocks (20 × 20 × 8 mm3) were prepared and divided into eight groups (n=20). They were sandblasted (50 μm Al2O3) and treated as follows: no primer or primer (Z-Primer Plus). Four self-adhesive resin cements (MDP-containing: Permacem 2.0 [PC], Clearfil SA luting [CS]; non–MDP-containing: Rely-X U200 [RU], Maxcem Elite [ME]) were bonded to the zirconia surface. After thermocycling, a μSBS test was performed. The failure mode was analyzed using light microscopy. Statistical analysis of μSBS was performed using one-way analysis of variance and two-sample t-test with post hoc Tukey test. The loss rate was evaluated using the Fisher's exact test and χ2 test with post hoc Tukey test (p&lt;0.05). Results: Within the no primer groups, the PC and CS groups showed higher bond strength than the RU and ME groups. Comparing the μSBS of the no primer and primer groups in the same SARCs, the RU/P group was higher than the RU group, and the ME/P group was higher than the ME group. No significant difference was observed between the PC and PC/P groups and between the CS and CS/P groups. Conclusions: Non–MDP-containing SARC showed the increased bonding value with MDP-containing primer to zirconia ceramics. The bond strength of MDP-containing SARCs was not affected significantly by the use of zirconia primer.

scholarly journals Adhesion of Indirect MOD Resin Composite Inlays Luted With Self-adhesive and Self-etching Resin Cements

2012 ◽  
Vol 37 (5) ◽  
pp. 474-484 ◽  
Author(s):  
T Inukai ◽  
T Abe ◽  
Y Ito ◽  
P Pilecki ◽  
RF Wilson ◽  
...  
Keyword(s):  
Bond Strength ◽  
Resin Composite ◽  
Resin Cement ◽  
Acid Etching ◽  
Resin Cements ◽  
Significant Difference ◽  
Before And After ◽  
Indirect Composite ◽  
Bond Strengths ◽  
Composite Inlays

SUMMARY This study investigated the effect of loading on the bond strength to dentin and microleakage of MOD indirect composite restorations bonded with self-adhesive and self-etching resin cements with or without acid etching of the proximal enamel margins. Class II MOD cavities were prepared in 48 molar teeth into dentin and divided into three groups of 16 teeth. Impressions were taken and indirect composite inlays fabricated (Estenia C & B). The enamel margins of the proximal boxes of half the specimens were phosphoric acid etched, and the inlays were cemented with one of three cements (Panavia F 2.0, SA Cement, or Rely X Unicem). After luting, eight teeth in each cement group were mechanically loaded at 2.5 cycles/s for 250,000 cycles. Unloaded teeth acted as controls. Teeth were stored in Rhodamine B solution for 24 hours, sectioned buccolingually at the proximal boxes to examine microleakage using confocal microscopy, and further sectioned for μTBS testing of the resin-dentin interface. Analysis of variance was performed to assess the effect of loading and acid etching on microleakage and bond strength. Acid etching had no effect on microleakage. No significant difference in the dentin bond strengths between the three cements existed after loading. Panavia F 2.0 exhibited a significant reduction in bond strength. With regard to microleakage at the proximal boxes, loading had no effect on dye penetration at the cavity floor. However, at the axial walls, loading had a significant deleterious effect on Panavia F 2.0. No difference in microleakage existed between the three cements at both sites before and after loading. In conclusion, the two tested self-adhesive cements exhibited similar bond strengths before and after loading to the self-etching resin cement. Loading reduced dentin bond strengths and increased microleakage at the resin-dentin interface. However, acid etching of the enamel margins had no significant effect on microleakage in the approximal regions of the bonded inlays.

scholarly journals Can the silane heat treatment influence the bond durability between resin cements and a dental ceramic?

2020 ◽  
Vol 68 ◽  
Author(s):  
Ronaldo Luís Almeida de CARVALHO ◽  
Jean Soares MIRANDA ◽  
Rodrigo Furtado de CARVALHO ◽  
Michelly Rocha DUARTE ◽  
Estevão Tomomitsu KIMPARA ◽  
...  
Keyword(s):  
Heat Treatment ◽  
Bond Strength ◽  
Resin Cement ◽  
Microtensile Bond Strength ◽  
Resin Cements ◽  
Luting Agents ◽  
All Ceramic ◽  
Cad Cam ◽  
Ceramic Blocks ◽  
Bond Durability

ABSTRACT Objective Evaluate the influence of silane heat treatment in bond durability between two resin cements and CAD/CAM feldspathic ceramic. Methods 40 feldspathic ceramic blocks were obtained, and were duplicated in microhybrid composite. All ceramic blocks were etched with 10% hydrofluoric acid for 20 s and received application of silane agent. The blocks were randomizedinto eight groups (n=5) according to the surface treatments and luting agents: P- Panavia F; PAg- Panavia F + Aging; HP- Heat Treatment + Panavia F; HPAg- Heat Treatment + Panavia F + Aging; R- RelyX ARC; Rag- RelyX ARC + Aging; HR- Heat Treatment + RelyX ARC; HRAg- Heat Treatment + RelyX ARC + Aging. The heat treatment was performed in furnace at 100 °C for 2 min. All blocks were cemented and cut to obtain samples with adhesive area of 1 mm2. Aging was performed with 10000 thermal cycles. The samples were subjected to microtensile bond strength test. Results The three-way ANOVA test revealed a significant interaction between cement versus heat treatment (p=0.001) and heat treatment versus thermal cycling (p=0.001) indicating that there was a change in bond strength due to surface treatment and aging. Conclusion Therefore, the heat treatment of the silane at 100 ºC for 2 minutes obtained higher values of bond strength between the resin cement and a feldspathic ceramicafter aging.

Bonding of Adhesive Luting Agents to Caries-affected Dentin Induced by a Microcosm Biofilm Model

2015 ◽  
Vol 40 (3) ◽  
pp. E102-E111 ◽  
Author(s):  
AC Peixoto ◽  
AA Bicalho ◽  
CP Isolan ◽  
TT Maske ◽  
RR Moraes ◽  
...  
Keyword(s):  
Elastic Modulus ◽  
Stress Distribution ◽  
Bond Strength ◽  
Three Dimensional ◽  
Strength Test ◽  
Resin Cement ◽  
Experimental Conditions ◽  
Luting Agents ◽  
Biofilm Model ◽  
Adhesive Luting

SUMMARY Objectives To evaluate the bond strength of adhesive luting agents applied to caries-affected dentin (CAD). Methods Thirty-six noncarious human third molars were abraded to expose an occlusal dentin surface. Caries lesions were induced in half of the samples using a microcosm biofilm model. Biofilm was cultivated under an anaerobic atmosphere for 14 days in a medium enriched with mucin. The same medium containing 1% sucrose was alternated for 4 hours per day. Cylinders of resin cement (RelyX ARC, RelyX U200, or BisCem) were built up over the dentin substrate and submitted to shear bond load. The samples were then longitudinally sectioned. The hardness and elastic modulus of dentin were measured at different depths from the occlusal surface. A three-dimensional finite element simulation was performed to analyze the residual stress distribution during the shear bond strength test. Bond strength data were analyzed by two-way analysis of variance (ANOVA) and hardness and elastic modulus by split-plot ANOVA. Multiple comparisons were performed with the SNK test (α=0.05). Results For all cements, the highest bond strengths were observed in sound dentin. Relyx ARC bond strength was similar to that of RelyX U200 for both substrates; BisCem had the lowest values. CAD had lower hardness (above a depth of 100 μm) and elastic modulus (above a depth of 150 μm) values than sound dentin. Stress distribution during the bond strength test was similar under all experimental conditions. Conclusion Impairment of the mechanical properties of dentin promoted by carious lesions reduced the bond strength of adhesive luting agents.

scholarly journals Effect of two Resin Cements and two Fiber Post Surface Treatments on Push-out Bond Strength between Fiber Post and Root Dentin

2015 ◽  
Vol 16 (1) ◽  
pp. 7-12 ◽  
Author(s):  
Luiz Felipe Valandro ◽  
César Dalmolin Bergoli ◽  
Carolina Ceolin Druck ◽  
Gabriel Kalil Rocha Pereira
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Acrylic Resin ◽  
Surface Treatments ◽  
Resin Cement ◽  
Fiber Post ◽  
Resin Cements ◽  
Tukey Test ◽  
Root Dentin ◽  
Push Out

ABSTRACT Aim To evaluate the effect of fiber post surface treatments on push-out bond strength between fiber post and root dentin. Materials and methods Sixty bovine mandibular teeth (N = 60) were sectioned (16 mm), prepared (12 mm), embedded with acrylic resin and then allocated into six groups (n = 10): Gr1- Silane coupling agent (Sil) + Conventional resin cement AllCem (AlC); Gr2- Sil + Conventional resin cement RelyX ARC (ARC); Gr3- tribochemical silica coating (TBS) + AlC; Gr4– TBS + ARC; Gr5- No treatment (NT) + AlC; Gr6– NT+ ARC. Specimens were sectioned in four slices (2 mm) and submitted to push-out test. Fracture analyses were executed at x200. The values of the push-out bond strength were submitted to two-way ANOVA and Tukey test (á = 0.05). Results Resin cement did not affect the bond strength values (p = 0.9674), fiber post surface treatment affected the push-out bond strength (p = 0.0353), interaction between factors did not affected the values (p = 0.338). Tukey test did not show differences between the groups. Adhesive failure between cement and dentin was predominantly. Conclusion The fiber post surface treatment appears have no influence on bond strength between fiber post and root dentin. Clinical significance The tested fiber posts surface treatment appears do not influence the fiber post bond behavior. How to cite this article Druck CC, Bergoli CD, Pereira GKR, Valandro LF. Effect of two Resin Cements and two Fiber Post Surface Treatments on Push-out Bond Strength between Fiber Post and Root Dentin. J Contemp Dent Pract 2015;16(1):7-12.

scholarly journals Comparative Evaluation of Tensile Bond Strength of Nickel-Chromium Alloy to Dental Enamel Using Different Resin Cements – An In Vitro Study.

2016 ◽  
Vol 04 (03) ◽  
pp. 170-176
Author(s):  
Manjit Kumar ◽  
Abhishek Gupta ◽  
Vandana Chabhra ◽  
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Dental Enamel ◽  
Tensile Bond Strength ◽  
Chromium Alloy ◽  
Resin Cements ◽  
Luting Agents ◽  
Nickel Chromium ◽  
Adhesive Luting ◽  
Self Etch

Abstract Aim: The aim of this study was to evaluate and compare the tensile bond strength of nickel-chromium alloy to dental enamel by using four different resin cements. Materials and Methods: 40 extracted central incisor teeth embedded in acrylic blocks were flattened not to expose dentin. Wax rectangular blocks of 5 mm length, 5 mm width and 1 mm height with a loop were invested and casted using Nickel-Chromium alloy by conventional induction casting method and sandblasted. Then casted rectangular blocks and 40 tooth embedded acrylic samples were divided into four groups (10 each) and cemented to tooth enamel following manufacturer's instructions as; GroupAcemented using RelyX U200, Group B cemented using Smartcem 2, Group C cemented using Multilink Speed and Group D cemented using Multilink N and then stored in artificial saliva for 24 hours. The direct pull tensile test was carried out on Universal Testing Machine at cross head speed of 0.5mm/min. Results: One way ANOVA showed a highly statistically significant (p<.01) difference between all the four resin cements. Post Hoc Tests- Multiple comparisons showed highly statistically significant (p< 0.01) difference between RelyX U200: Multilink N, Smartcem 2: Multilink Speed, Smartcem 2: Multilink N, Multilink Speed: Multilink N. Difference between RelyX U200 : Smartcem 2 and RelyX U200 : Multilink Speed was statistically significant(p< 0.05). Conclusion: Self etch resin cement (Multilink N) showed maximum mean tensile bond strength as compared to self-adhesive resin cements (Smartcem 2, RelyX U200 and Multilink Speed). Clinically the greatest advantage of self-adhesive cements is the easy and fast application technique. But this time saving technique is not as effective as self-etch resin luting agents. The presumed benefit of saving time with self-adhesive luting agents may only be realized at the expense of compromising bond strength.

Development of a Cavity Disinfectant Containing Antibacterial Monomer MDPB

2016 ◽  
Vol 95 (13) ◽  
pp. 1487-1493 ◽  
Author(s):  
N. Hirose ◽  
R. Kitagawa ◽  
H. Kitagawa ◽  
H. Maezono ◽  
A. Mine ◽  
...  
Keyword(s):  
Antibacterial Activity ◽  
Bond Strength ◽  
Bacterial Species ◽  
Oral Bacteria ◽  
Resin Cement ◽  
Resin Cements ◽  
Adhesive Resin ◽  
Significant Difference ◽  
Adhesive Resin Cement

An experimental cavity disinfectant (ACC) that is intended to be used for various direct and indirect restorations was prepared by adding an antibacterial monomer 12-methacryloyloxydodecylpyridinum bromide (MDPB) at 5% into 80% ethanol. The antibacterial effectiveness of ACC and its influences on the bonding abilities of resin cements were investigated. To examine the antibacterial activity of unpolymerized MDPB, the minimum inhibitory and bactericidal concentrations (MIC and MBC) were determined for Streptococcus mutans, Lactobacillus casei, Actinomyces naeslundii, Parvimonas micra, Enterococcus faecalis, Fusobacterium nucleatum, and Porphyromonas gingivalis. Antibacterial activities of ACC and the commercial cavity disinfectant containing 2% chlorhexidine and ethanol (CPS) were evaluated by agar disk diffusion tests through 7 bacterial species and by MIC and MBC measurement for S. mutans. The effects of ACC and CPS to kill bacteria in dentinal tubules were compared with an S. mutans–infected dentin model. Shear bond strength tests were used to examine the influences of ACC on the dentin-bonding abilities of a self-adhesive resin cement and a dual-cure resin cement used with a primer. Unpolymerized MDPB showed strong antibacterial activity against 7 oral bacteria. ACC produced inhibition zones against all bacterial species similar to CPS. For ACC and CPS, the MIC value for S. mutans was identical, and the MBC was similar with only a 1-step dilution difference (1:2). Treatment of infected dentin with ACC resulted in significantly greater bactericidal effects than CPS ( P < 0.05, analysis of variance and Tukey’s honest significant difference test). ACC showed no negative influences on the bonding abilities to dentin for both resin cements, while CPS reduced the bond strength of the self-adhesive resin cement ( P < 0.05). This study clarified that the experimental cavity disinfectant containing 5% MDPB is more effective in vitro than the commercially available chlorhexidine solution to eradicate bacteria in dentin, without causing any adverse influences on the bonding abilities of resinous luting cements.

Richard Scheringer, the KPD and the Politics of Class and Nation in Germany, 1922–1969

2005 ◽  
Vol 14 (3) ◽  
pp. 317-346 ◽  
Author(s):  
TIMOTHY S. BROWN
Keyword(s):  
Interwar Period ◽  
Third Reich ◽  
Radical Right ◽  
High Profile ◽  
Army Officer ◽  
Modern Germany ◽  
Before And After ◽  
The Third Reich ◽  
Relationship Of ◽  
The Relationship

This article examines the life and times of Richard Scheringer, an army officer and supporter of Adolf Hitler who became famous during the early 1930s for his high-profile conversion to communism. Known in the closing years of the Weimar Republic as a point-man for Communist efforts to win support from the radical right, Scheringer survived the Third Reich to become a leading figure in the postwar Communist Party. His well-documented but little-studied career, bridging critical caesurae of modern Germany history, highlights the unique political constellation of the interwar period, demonstrating fundamental continuities in the relationship of German communism to the nation before and after 1945.

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