scholarly journals Evaluation of Chemical Treatment on Zirconia Surface with Two Primer Agents and an Alkaline Solution on Bond Strength

2012 ◽  
Vol 37 (6) ◽  
pp. 625-633 ◽  
Author(s):  
FC Lorenzoni ◽  
VP Leme ◽  
LA Santos ◽  
PCG de Oliveira ◽  
LM Martins ◽  
...  
Keyword(s):  
Bond Strength ◽  
Alkaline Solution ◽  
Chemical Treatment ◽  
Failure Modes ◽  
Surface Group ◽  
Acrylic Resin ◽  
Resin Cement ◽  
Control Group ◽  
Dihydrogen Phosphate ◽  
Naoh Solution

SUMMARY Objectives This study evaluated the effect of an alkaline solution and two 10-methacryloyloxydecyl dihydrogen phosphate (MDP)-based primer agents on bond strength to zirconia (yttria-stabilized tetragonal zirconium polycrystal [Y-TZP]) through the shear bond strength (SBS) test. Materials and Methods Sixty square-shaped Y-TZP samples were embedded in an acrylic resin mold, polished, and randomly assigned to one of six groups (n=10) according to treatment surface: group CR, no treatment (control); group NaOH, 0.5 M NaOH; group AP, Alloy Primer; group ZP, Z-Primer Plus; group NaOH-AP, 0.5 M NaOH + Alloy Primer; and group NaOH-ZP, 0.5 M NaOH + Z-Primer Plus. The resin cement (Rely X U100) was applied inside a matrix directly onto the Y-TZP surface, and it was light-cured for 40 seconds. The samples were stored in distilled water at 37°C for 24 hours prior to the test, which was performed in a universal machine at a crosshead-speed of 0.5 mm/min. The data were analyzed by one-way analysis of variance and Tukey tests (p<0.05). Light stereomicroscopy and scanning electron microscopy were used to assess the surface topography and failure mode. Results The SBS was significantly affected by the chemical treatment (p<0.0001). The AP group displayed the best results, and the use of NaOH did not improve SBS results relative to either AP or ZP. The samples treated with Alloy Primer displayed mainly mixed failures, whereas those conditioned with Z-Primer Plus or with 0.5 M NaOH presented a balanced distribution of adhesive and mixed failure modes. Conclusions The use of a NaOH solution may have modified the reactivity of the Y-TZP surface, whereas the employment of a MDP/6-4-vinylbenzyl-n-propyl amino-1,3,5-triazine-2,4-dithione–based primer enhanced the Y-TZP bond strength.

scholarly journals Effect of Surface Treatments on the Bond Strength to Turkom-Cera All-ceramic Material

2016 ◽  
Vol 17 (11) ◽  
pp. 920-925 ◽  
Author(s):  
Bandar MA Al-Makramani ◽  
Fuad A Al-Sanabani ◽  
Abdul AA Razak ◽  
Mohamed I Abu-Hassan ◽  
Ibrahim Z AL-Shami ◽  
...  
Keyword(s):  
Bond Strength ◽  
Ceramic Material ◽  
Failure Modes ◽  
Testing Machine ◽  
Surface Treatments ◽  
Resin Cement ◽  
Control Group ◽  
Significant Difference ◽  
All Ceramic ◽  
Effect Of Surface

ABSTRACT Aim The aim of this study was to evaluate the effect of surface treatments on shear bond strength (SBS) of Turkom-Cera (Turkom-Ceramic (M) Sdn. Bhd., Puchong, Malaysia) all-ceramic material cemented with resin cement Panavia-F (Kuraray Medical Inc., Okayama, Japan). Materials and methods Forty Turkom-Cera ceramic disks (10 mm × 3 mm) were prepared and randomly divided into four groups. The disks were wet ground to 1000-grit and subjected to four surface treatments: (1) No treatment (Control), (2) sandblasting, (3) silane application, and (4) sandblasting + silane. The four groups of 10 specimens each were bonded with Panavia-F resin cement according to manufacturer's recommendations. The SBS was determined using the universal testing machine (Instron) at 0.5 mm/min crosshead speed. Failure modes were recorded and a qualitative micromorphologic examination of different surface treatments was performed. The data were analyzed using the one-way analysis of variance (ANOVA) and Tukey honestly significant difference (HSD) tests. Results The SBS of the control, sandblasting, silane, and sandblasting + silane groups were: 10.8 ± 1.5, 16.4 ± 3.4, 16.2 ± 2.5, and 19.1 ± 2.4 MPa respectively. According to the Tukey HSD test, only the mean SBS of the control group was significantly different from the other three groups. There was no significant difference between sandblasting, silane, and sandblasting + silane groups. Conclusion In this study, the three surface treatments used improved the bond strength of resin cement to Turkom-Cera disks. Clinical significance The surface treatments used in this study appeared to be suitable methods for the cementation of glass infiltrated all-ceramic restorations. How to cite this article Razak AAA, Abu-Hassan MI, AL-Makramani BMA, AL-Sanabani FA, AL-Shami IZ, Almansour HM. Effect of Surface Treatments on the Bond Strength to Turkom-Cera All-Ceramic Material. J Contemp Dent Pract 2016;17(11):920-925.

scholarly journals Effect of Provisional Cements on Shear Bond Strength of Porcelain Laminate Veneers

2011 ◽  
Vol 05 (04) ◽  
pp. 373-379 ◽  
Author(s):  
Subutay Han Altintas ◽  
Onjen Tak ◽  
Asli Secilmis ◽  
Aslihan Usumez
Keyword(s):  
Bond Strength ◽  
Calcium Hydroxide ◽  
Shear Bond Strength ◽  
Testing Machine ◽  
Acrylic Resin ◽  
Resin Cement ◽  
Control Group ◽  
Molar Teeth ◽  
Laminate Veneers ◽  
Selection Of

ABSTRACTObjectives: The purpose of this study was to evaluate the effect of three provisional cements and two cleaning techniques on the final bond strength of porcelain laminate veneers. Methods: The occlusal third of the crowns of forty molar teeth were sectioned and embedded in autopolymerizing acrylic resin. Dentin surfaces were polished and specimens were randomly divided into four groups (n=10). Provisional restorations were fabricated and two provisional restorations were cemented onto each tooth. Restorations were fixed with one of three different provisional cements: eugenol-free provisional cement (Cavex), calcium hydroxide (Dycal), and light-cured provisional cement (Tempond Clear). Provisional restorations were removed with either a dental explorer and air-water spray, or a cleaning bur (Opticlean). In the control group, provisional restorations were not used on the surfaces of specimens. IPS Empress 2 ceramic discs were luted with a dual-cured resin cement (Panavia F). Shear bond strength was measured using a universal testing machine. Data were statistically analyzed by ANOVA, Tukey’s HSD and Dunnett tests. Surfaces were examined by scanning electronic microscopy. Results: Significant differences were found between the control group and both the light-cured provisional cement groups and the eugenol-free provisional cement-cleaning bur group (P<.05). Groups that had received light-cured provisional cement showed the lowest bond strength values. Conclusions: Selection of the provisional cement is an important factor in the ultimate bond strength of the final restoration. Calcium hydroxide provisional cement and cleaning with a dental explorer are advisable. (Eur J Dent 2011;5:373-379)

Bonding Polycrystalline Zirconia With 10-MDP–containing Adhesives

2017 ◽  
Vol 42 (3) ◽  
pp. 335-341 ◽  
Author(s):  
AE Llerena-Icochea ◽  
RM Costa ◽  
AFS Borges ◽  
JFS Bombonatti ◽  
AY Furuse
Keyword(s):  
Bisphenol A ◽  
Bond Strength ◽  
Shear Bond Strength ◽  
Failure Modes ◽  
Tetragonal Zirconia ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Single Bond ◽  
Glycol Dimethacrylate ◽  
Significant Difference

SUMMARY Objective: The objective of this study was to evaluate the influence of adhesives with different 10-MDP concentrations on the shear bond strength of a resin cement to zirconia. Methods and Materials: Six experimental adhesives were prepared with the following composition: camphorquinone, 1,2-diaminobenzene, butylhydroxytoluene, diphenyliodonium hexafluorophosphate, 2-hydroxyethyl methacrylate triethylene glycol dimethacrylate, ethoxylated bisphenol A glycol dimethacrylate, urethane dimethacrylate, bisphenol A diglycidyl methacrylate, and ethanol. The 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) monomer was added at 0wt%, 3wt%, 6wt%, 9wt%, 12wt%, or 15wt%. Three commercially available adhesives were evaluated: Single Bond Universal, Single Bond 2, and Signum Zirconia Bond. Resin cement cylinders made with RelyX Ultimate were bonded to yttria-stabilized tetragonal zirconia polycrystal with one of the evaluated adhesives and were subjected to the shear bond strength evaluation. Failure modes were analyzed with a stereoscopic loupe. Statistical analyses were performed with one-way analysis of variance and the Tukey's Honestly Significant Difference test (α=0.05). Pearson's was used to correlate the percentage of 10-MDP in the experimental adhesives and shear bond strength. Results: There were significant differences between adhesives (p&lt;0.00001). The highest shear bond strength values were obtained with the Signum Zirconia Bond and Single Bond Universal. Single Bond 2 showed the lowest values. There were no differences between experimental adhesives. All groups showed adhesives failures. A nonlinear correlation was found between bond strength and percentage of 10-MDP in experimental adhesives (r=0.872). Conclusions: The commercially available adhesives indicated for bonding to zirconia showed the highest bonding values.

scholarly journals Impact of simplified chemical treatment of semi-direct restorations cemented with self-adhesive resin cement on dentin bond durability and nanoleakage

2020 ◽  
Vol 9 (11) ◽  
pp. e619119525
Author(s):  
Joselúcia da Nóbrega Dias ◽  
Andressa Eveline de Lima Ribeiro ◽  
Ana Margarida dos Santos Melo ◽  
Boniek Castillo Dutra Borges ◽  
Isauremi Assunção
Keyword(s):  
Bond Strength ◽  
Chemical Treatment ◽  
Failure Modes ◽  
Surface Treatments ◽  
Resin Cement ◽  
Universal Adhesive ◽  
Adhesive Resin ◽  
Chemical Surface ◽  
Adhesive Resin Cement ◽  
Bond Durability

The present study aimed to evaluate the impact of different chemical surface treatments and aging on dentin bond strength and nanoleakage of semi-direct restorations cemented with self-adhesive resin cement. One hundred and sixty semi-direct composite restorations (4.8 x 2.8 x 4.0 mm) were produced to fill dentin preparations in bovine tooth, and the specimens were divided into 8 groups according to chemical treatment [No treatment, Silane (S), Scotchbond™ Universal adhesive (SBU), and S+SBU], and aging time in water [24 h and 6 months]. Push-out bond strength (PBS) was measured through a universal testing machine (1.0 mm/min), failure modes by a dissecting microscope, and nanoleakage by scanning electron microscopy. Two-way ANOVA and Tukey's post-hoc (p<0.05) test were used to analyze PBS data, whilst failure modes and nanoleakage were analyzed descriptively. The bond durability was influenced by different chemical surface treatments after 6 months of aging in distilled water, with the best performance for the group that uses silane associated with the universal adhesive. Nanoleakage was greater at the dentin-cement interface, from the base of the restorations. However, the infiltration of silver crystals at the cement-resin interface was not influenced by the different chemical treatments applied. The results of the study suggest that self-adhesive cement promotes efficient adhesion to the interface that improves over time without the need for chemical surface treatment or when using SBU, with or without silane.

Effect of Surface Treatment and Resin Cement on Microtensile Bond Strength of Zirconia to Dentin

2014 ◽  
Vol 602-603 ◽  
pp. 602-605
Author(s):  
Xiao Li Feng ◽  
Ruo Yu Liu ◽  
Yan Li Zhang ◽  
Liang Jiao Chen ◽  
Yao Kun Zhang ◽  
...  
Keyword(s):  
Bond Strength ◽  
Surface Treatment ◽  
Acrylic Resin ◽  
Silica Coating ◽  
Surface Treatments ◽  
Resin Cement ◽  
Occlusal Plane ◽  
Control Group ◽  
Microtensile Bond Strength ◽  
Relyx Unicem

To evaluate the effect of three surface treatments and two resin cements on microtensile bond strength of zirconia to dentin. Sixty human molars were embedded in acrylic resin and sectioned 3 mm below the occlusal plane. Teeth specimens and sixty zirconia specimens were randomized into 3 groups according to the following surface treatments (n=20): no treatment (control), sandblasting and silane application (SB+SI), sandblasting then silica coating and silane application (SB+SC+SI). In each group, half of the ceramic-tooth assemblies were cemented with PanaviaTM F (Kurary Dental), the rest with RelyX Unicem (3M ESPE). All specimens were cut into microtensile sticks that were loaded in tension until failure. Data were analyzed using two-way ANOVA and Tukey’s HSD test (α=0.05). The SB+SC+SC group presented higher values than SB+SI and the control group (P<0.05). Bond strength in PanaviaTM F groups were significantly higher than those in RelyX Unicem regardless of the surface treatment (P<0.05). Data indicated that both surface treatment and resin cement have significant effects on bond strength of zirconia to dentin.

scholarly journals Effect of Chlorhexidine and Ethanol Application on Longterm Push-out Bond Strength of Fiber Posts to Dentin

2015 ◽  
Vol 16 (7) ◽  
pp. 547-553 ◽  
Author(s):  
Roberta Tarkany Basting ◽  
Cecília Pedroso Turssi ◽  
Flavia Lucisano Botelho do Amaral ◽  
Fabiana Mantovani Gomes França ◽  
Rafaela Crystyan Vaneli ◽  
...  
Keyword(s):  
Bond Strength ◽  
Repeated Measures ◽  
Adhesive System ◽  
Resin Cement ◽  
Control Group ◽  
Test Analysis ◽  
Significance Level ◽  
Fiber Posts ◽  
Etch And Rinse ◽  
Push Out

ABSTRACT Aim The aim of this study was to evaluate the effect of chlorhexidine and ethanol application on the push-out bond strength and bond durability of fiber posts cemented with an etch-and-rinse adhesive system/resin cement to intraradicular dentin. Materials and methods Fifty-four bovine roots were shaped for the cementation of a fiberglass post and received the application of 37% phosphoric acid. They were then randomly divided into three groups, according to the type of dentin treatment (n = 18) performed: no treatment (control group), 100% ethanol, or 2% chlorhexidine. Next, the adhesive system (Adper Scotch Bond Multipurpose Plus, 3M ESPE) was applied to the dentin, according to the manufacturer's instructions. Glass fiber posts were cemented with dual resin cement (Rely X ARC, 3M ESPE). After 48 hours, the specimens were serially sectioned for push-out test analysis, providing two slices from each root third (cervical, medium and apical), one of which was tested immediately and the other stored in distilled water for 180 days. The data were analyzed with three-way analysis of variance (ANOVA) for repeated measures and Tukey's test at a 5% significance level. Results Intraradicular treatment with chlorhexidine yielded the highest bond strength means, followed by ethanol treatment. The control group presented the lowest bond strength means. Water storage exerted no effect on bond strength values. Conclusion Both chlorhexidine and ethanol improved push-out bond strength to intraradicular dentin, with the former providing the best results, regardless of the storage time. Clinical significance The application of 2% chlorhexidine or 100% ethanol may be an important step that can be taken to enhance bond strength of fiber posts to intraradicular dentin, when dual resin cements are used. How to cite this article França FMG, Vaneli RC, de Melo Conti C, Basting RT, do Amaral FLB, Turssi CP. Effect of Chlorhexidine and Ethanol Application on Long-term Pushout Bond Strength of Fiber Posts to Dentin. J Contemp Dent Pract 2015;16(7):547-553.

scholarly journals Influence of curing mode of resin luting cements on bond strength to dentin

2017 ◽  
Vol 15 (4) ◽  
pp. 258
Author(s):  
Marcelo Giannini ◽  
Andreia Assis Carvalho ◽  
Ariovaldo Stefani ◽  
Wladimir Franco de Sá Barbosa ◽  
Lawrence Gonzaga Lopes
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Resin Cement ◽  
Control Group ◽  
Resin Cements ◽  
Luting Cements ◽  
Halogen Light ◽  
Significant Difference ◽  
Tooth Surfaces ◽  
Light Curing

Self-adhesive, dual-polymerizing resin cements require no treatment to the prepared tooth surfaces before cementation. Aim: The aim of this study was to evaluate the influence of curing mode on bond strength (BS) of three cementing systems to bovine dentin. Methods: The buccal enamel surfaces of 50 bovine incisors were removed to expose dentin and to flat the surface. The teeth were divided into five groups (n=10), which consisted of two resin cements (Multilink and Clearfil SA Cement) that were tested in dual- (halogen light for 40 s) and self-cured modes, and a control (RelyX ARC). Two cylinders of resin cements (1.0 mm X 0.75 mm) were prepared on each bonded dentin surface. After 24h at 37oC, resin cylinders were subjected to micro-shear testing in a universal testing machine (4411/Instron - 0.5 mm/min). Data were statistically analyzed by two-way ANOVA, Tukey and Dunnett`s test (5%). Results: Multilink showed higher BS than those observed on Clearfil SA. Light-curing resulted in higher BS for both Multilink and Clearfil SA. When Multilink was light-cured, no significant difference on BS was demonstrated between it and RelyX ARC. Conclusions: The highest BS values were obtained in control group and light-cured Multilink resin cement.

Lack of Neutralization of 10-MDP Primers by Zirconia May Affect the Degree of Conversion of Dual-cure Resin Cement

2021 ◽  
Vol 46 (1) ◽  
pp. 107-115
Author(s):  
DM De Paula ◽  
AD Loguercio ◽  
A Reis ◽  
S Sauro ◽  
AH Alves ◽  
...  
Keyword(s):  
Bond Strength ◽  
Testing Machine ◽  
Monomer Concentration ◽  
Positive Control ◽  
Degree Of Conversion ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Resin Cements ◽  
Low Concentrations ◽  
Microshear Bond Strength

Clinical Relevance Use of zirconia primers with a low pH and a high acidic monomer concentration should be employed in combination with dual-cure resin cements that are less sensitive to an acidic environment. Primers with lower 10-MDP concentrations attain better outcomes. SUMMARY Objective: To assess the effects of different concentrations of 10-methacryloyloxydecyl dihydrogen phosphate (10-MDP) included in experimental ceramic primers on the degree of conversion (DC) and microshear bond strength (μSBS) of a dual-cure resin cement, and on the acidity neutralization potential of zirconia (ZrO2) in comparison to hydroxyapatite (HAp). Methods: Experimental ceramic primers were formulated using 5 wt%, 10 wt%, 20 wt%, or 40 wt% 10-MDP as an acidic functional monomer and camphorquinone (CQ)/amine or 1-phenyl-1,2-propanedione (PPD) as a photoinitiator system. Clearfil Ceramic Primer (Kuraray Dental, Tokyo, Japan) was used as the commercial control. Micro-Raman spectroscopy was used to assess the DC of uncured and light-cured resin cements applied onto primer-treated ZrO2 surfaces. The μSBS and pH of primers were assayed in a universal testing machine and by a digital pH meter (Tec-3MP; Tecnal, Piracicaba, Brazil), respectively. Statistical analysis was performed by one-way analysis of variance (ANOVA) and Tukey’s test (p&lt;0.05). Results: DC was not affected until a concentration of 10% 10-MDP in CQ primer and 5% 10-MDP in PPD primer was reached, when compared with the positive control (p&gt;0.05). Groups 10-MDP 5% in CQ and PPD primers showed the highest μSBS compared with the positive control (p&gt;0.05); however, higher concentrations of 10-MDP induced significant DC and μSBS reduction (p&lt;0.05). HAp neutralized 10-MDP primers, but ZrO2 provided higher acidity to the primers’ pH. Conclusion: 10-MDP monomer should be used in low concentrations in ZrO2 primers to avoid reduction of the polymerization and bond strength of resin cement.

scholarly journals Effect of Replacing a Component of a Self-Etch Adhesive by Chlorhexidine on Bonding to Dentin

2013 ◽  
Vol 24 (4) ◽  
pp. 335-339 ◽  
Author(s):  
Cesar Pomacondor-Hernandez ◽  
Alberto Nogueira de Gama Antunes ◽  
Vinicius di Hipolito ◽  
Mario Fernando de Goes
Keyword(s):  
Bond Strength ◽  
Repeated Measures ◽  
Failure Modes ◽  
Resin Composite ◽  
Water Storage ◽  
Control Group ◽  
Morphological Aspect ◽  
Human Teeth ◽  
Self Etch ◽  
Experimental Group

The purpose of this study was to evaluate the effect of replacing a component of the self-etch adhesive Adper Scotchbond SE (liquid A + liquid B) by 2% chlorhexidine (CHX) on bond strength to dentin after 1 day, 3 months or 6 months of water storage. Eight human teeth were sectioned to expose a flat dentin surface and were then randomly assigned to 2 groups. In the control group, the dentin surfaces were treated with the adhesive according to the manufacturer's instructions. In the experimental group, liquid A was replaced by 2% CHX. Next, a 6-mm-high resin composite block was incrementally built on the bonded surfaces. The restored teeth were then sectioned to produce stick-shaped specimens (cross-sectional area - 0.8 mm2). The microtensile bond strength (µTBS) was recorded, and the failure modes were assessed. Data were analyzed by two-way repeated measures ANOVA (α=0.05). Four additional teeth were processed in order to conduct a micromorphological analysis of the resin-dentin interface. The µTBS values did not significantly decrease after water storage in either the control or the experimental group, whose values did not differ significantly irrespective of storage time. The morphological aspect of the bonding interface appears not to have been affected by CHX. A higher incidence of cohesive failures within the adhesive and mixed failures (cohesive within adhesive and resin composite) was observed for both groups. It may be concluded that dentin pre-treatment with 2% CHX did not influence significantly the bonding performance of the evaluated adhesive.

Effect of Methacryloyloxydecyl Dihydrogen Phosphate–Containing Silane and Adhesive Used Alone or in Combination on the Bond Strength and Chemical Interaction With Zirconia Ceramics Under Thermal Aging

2020 ◽  
Vol 45 (5) ◽  
pp. 516-527 ◽  
Author(s):  
MF Gutierrez ◽  
J Perdigão ◽  
P Malaquias ◽  
AM Cardenas ◽  
F Siqueira ◽  
...  
Keyword(s):  
Bond Strength ◽  
Computer Aided Design ◽  
Chemical Interaction ◽  
Interaction Analysis ◽  
Resin Cement ◽  
Dihydrogen Phosphate ◽  
Universal Adhesive ◽  
Adhesive Application ◽  
Aided Design ◽  
Silane Solution

Clinical Relevance Achieving durable bonding to zirconia is fundamental for the application of a methacryloyloxydecyl dihydrogen phosphate (MDP)–containing silane solution or an MDP-containing silane solution associated with an MDP-containing universal adhesive. SUMMARY Objectives: To evaluate the effect of a methacryloyloxydecyl dihydrogen phosphate (MDP)–containing silane coupling agent and universal adhesive, used alone or in combination, on the microshear bond strength (μSBS) to zirconia after 24 hours of water storage (24h) and after 10,000 thermocycles (TC), complemented with chemical analysis of the surface to establish the presence of MDP on the surface of the zirconia after bonding procedures. Methods and Materials: Thirty computer-aided design/computed-aided manufacturing blocks of zirconia were cut into four sections (6×6×6 mm) and sintered. Zirconia sections (n=96) were assigned to 24 groups according to three factors: 1) silane (no silane, Monobond S [MBS], Monobond P [MB+]), 2) adhesive + resin cement (no adhesive + Enforce [ENF], no adhesive + RelyX Ultimate [REX], Prime&Bond Elect + Enforce [PBE/ENF], Scotchbond Universal + RelyX Ultimate [SBU/REX]), and 3) thermocycling (no thermocycling [24h], 10,000 thermocycles [TC]). Upon silane/adhesive application, cylinder-shaped matrices were filled with resin cement and light cured. Specimens were tested in μSBS (1.0 mm/min) after 24h or TC. The μSBS data were analyzed using twoway ANOVA and Tukey’s post hoc test (α=0.05). In addition, micro-Raman spectroscopy was used to analyze the zirconia surface for immediate chemical interaction analysis (n=24). Results: For the 24h condition, PBE/ENF resulted in lower mean μSBS than both groups with silane without PBE (MBS and MB+ groups; p&lt;0.001). SBU alone or MB+ alone and MB+ associated with SBU showed the highest mean μSBS (p&lt;0.001). For the TC condition, all groups showed a significant decrease in mean μSBS compared with those of 24h (p&lt;0.001), with the exception of MB+ associated to SBU (p&gt;0.05). However, the application of MB+ alone or MB+ associated to SBU resulted in higher mean μSBS (p&lt;0.001) after TC than the remaining TC groups. In terms of chemical interaction, only the SBU groups, alone or combined with both of the silane agents, were associated with the methacrylate groups after rinsing. Conclusions: The results of the current study support the use of an MDP-containing silane solution or an MDP-containing silane solution associated with an MDP-containing universal adhesive for bonding to air-abraded zirconia, as a more stable bonding after thermocycling.

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