An In Vitro Assessment of the Effects of Three Surface Treatments on Repair Bond Strength of Aged Composites

2011 ◽  
Vol 36 (6) ◽  
pp. 608-617 ◽  
Author(s):  
TS Jafarzadeh Kashi ◽  
M Erfan ◽  
V Rakhshan ◽  
N Aghabaigi ◽  
FS Tabatabaei

Clinical Relevance To achieve a durable composite-composite bond, it is highly recommended that besides selective grinding of the surface to be repaired, specific combinations of silane primer and bonding agent should be used, without the need for acid etching of the composite surface.

2014 ◽  
Vol 39 (6) ◽  
pp. E250-E260 ◽  
Author(s):  
TA Imbery ◽  
T Gray ◽  
F DeLatour ◽  
C Boxx ◽  
AM Best ◽  
...  

SUMMARY Objective Repairing composite restorations may be a more conservative treatment than replacing the entire restoration. The objective of this in vitro study was to determine the best repair method by measuring flexural, diametral tensile, and shear bond strength of repaired composites in which the surfaces were treated with chemical primers (Add & Bond or Silane Bond Enhancer), a bonding agent (Optibond Solo Plus [OBSP]), or mechanical retention with a bonding agent. Methods Filtek Supreme Ultra shade B1B was placed in special molds to fabricate specimens that served to test the flexural, diametral tensile, or shear strength of the inherent resin substrate. The same molds were modified to make specimens for testing repair strength of the resin. Repairs were made immediately or after aging in deionized water at 37°C for seven days. All repair sites were finished with coarse Sof-Lex discs to simulate finishing new restorations or partially removing aged restorations. Repair surfaces were treated with one of the following: 1) phosphoric-acid etching and OBSP; 2) Add & Bond; 3) phosphoric-acid etching, Silane Bond Enhancer, and OBSP; or 4) quarter round bur, phosphoric-acid etching, and OBSP. Specimens were placed back in the original molds to fabricate specimens for diametral tensile or flexural testing or in an Ultradent jig to make specimens for shear bond testing. Composite resin in shade B5B was polymerized against the treated surfaces to make repairs. Two negative control groups for the three testing methods consisted of specimens in which repairs were made immediately or after aging without any surface treatments. Controls and experimental repairs were aged (water 37°C, 24 hours) before flexural, diametral tensile, or shear testing in an Instron Universal testing machine at a crosshead speed of 0.5 mm/min. Results Experimental flexural repair strengths ranged from 26.4% to 88.6% of the inherent substrate strength. Diametral tensile repair strengths ranged from 40% to 80% of the inherent substrate strength, and shear bond strength repairs ranged from 56% to 102%. Geometric means were statistically analyzed with two-way analysis of variance on their log-transformed values. Significant differences were determined using Tukey honestly significant difference (p<0.05). Conclusions Depending on the mechanical property being tested, surface treatments produced different results. OBSP produced more consistent results than chemical primers.


Author(s):  
Sílvia Fontes Do Amaral Pereira

O objetivo do presente estudo in vitro foi verificar, através de teste de cisalhamento, a resistência de união da liga Wironia®light, à base de níquel-cromo sem berílio, sujeita a diferentes tratamentos de superfície, às cerâmicas Vita VM13 e Noritake. Foram confeccionados oitenta espécimes cilíndricos metálicos, com o auxílio de uma matriz de aço, nas dimensões de 4 mm de diâmetro por 4 mm de altura. Os espécimes foram divididos em oito grupos (n=10), de acordo com o tipo de tratamento superficial aplicado à liga metálica e com o tipo de cerâmica testada. Estes foram avaliados de acordo com os critérios de resistência ao cisalhamento e, com o auxílio de microscopia óptica, foi avaliada a área de cerâmica remanescente aderida ao metal após a fratura. Os corpos-de-prova do G6 (fabricados em Cerâmica Noritake com jateamento-26,401 ± 11,637 MPa) apresentaram maior resistência ao cisalhamento (p> 0,05) enquanto que os menores valores foram registrados no G4 (Cerâmica Vita com utilização de broca-13,440 ± 7,766 MPa). G6 (19425,4 μm2) apresentou a maior área de cerâmica aderida ao metal (p> 0,05) enquanto que o G4 (2310,2 μm2) apresentou a menor área. Concluiu-se que G6 obteve os valores mais altos de resistência ao cisalhamento e de remanescente cerâmico aderido à superfície metálica enquanto que o G4 obteve os valores mais baixos. Descritores: Restaurações metalo-cerâmicas; ligas de níquel-cromo;porcelana dentária.


2021 ◽  
Vol 2021 ◽  
pp. 1-6
Author(s):  
Zohreh Moradi ◽  
Farnoosh Akbari ◽  
Sara Valizadeh

Aim. This study aimed to assess shear bond strength (SBS) of resin cement to zirconia ceramic with different surface treatments by using Single Bond Universal. Methods. In this in vitro study, 50 zirconia discs (2 × 6 mm) were divided into 5 groups of (I) sandblasting with silica-coated alumina (CoJet)  + silane + Single Bond 2, (II) sandblasting with CoJet + Single Bond Universal, (III) sandblasting with alumina + Single Bond Universal, (IV) sandblasting with alumina + Z-Prime Plus, and (V) Single Bond Universal with no surface treatment. Resin cement was applied in plastic tubes (3 × 5 mm2), and after 10,000 thermal cycles, the SBS was measured by a universal testing machine. The mode of failure was determined under a stereomicroscope at × 40 magnification. Data were analyzed using one-way ANOVA. Results. The maximum (6.56 ± 4.29 MPa) and minimum (1.94 ± 1.96 MPa) SBS values were noted in groups III and I, respectively. Group III had the highest frequency of mixed failure (60%). Group V had the maximum frequency of adhesive failure (100%). Conclusion. Single Bond Universal + sandblasting with alumina or silica-coated alumina particles is an acceptable method to provide a strong SBS between resin cement and zirconia.


2020 ◽  
Vol 19 ◽  
pp. e206155
Author(s):  
Yançanã Luizy Gruber ◽  
Thaís Emanuelle Bakaus ◽  
Bruna Fortes Bittencourt ◽  
João Carlos Gomes ◽  
Alessandra Reis ◽  
...  

Aim: The roughness and micromorphology of various surface treatments in aged metal-free crowns and the bond strength of these crowns repaired with composite resin (CR) was evaluated in vitro. Methods: A CR core build-up was confectioned in 60 premolars and prepared for metal-free crowns. Prepared teeth were molded with the addition of silicone, and the laboratory ceromer/fiber-reinforced crowns (SR Adoro/Fibrex Lab) were fabricated. Subsequently, the crowns were cemented and artificially aged in a mechanical fatigue device (1.2 X 106 cycles), then divided into 4 groups (n = 15) according to the surface treatment: 1) phosphoric acid etching (PA); 2) PA + silane application; 3) roughening with a diamond bur + PA; and 4) sandblasting with Al2O3 + PA. After the treatments, the crowns (n = 2) were qualitatively analyzed by scanning electron microscope (SEM) and surface roughness (n = 5) was analyzed before and after the surface treatment (Ra parameter). The remaining crowns (n = 8) received standard repair with an adhesive system (Tetric N-Bond) and a nanohybrid CR (Tetric N-Ceram), and the microshear bond strength (SBS) test was performed (0.5 mm/min). Roughness and SBS data were analyzed by one- and two-way ANOVA, respectively, as well as Tukey’s post-test (α = 0.05). Results: Sandblasting with Al2O3 + PA resulted in the highest final roughness and SBS values. The lowest results were observed in the PA group, whereas the silane and diamond bur groups showed intermediate values. Conclusion: It may be concluded that indirect ceromer crowns sandblasted with aluminum oxide prior to PA etching promote increased roughness surface and bond strength values.


2006 ◽  
Vol 17 (4) ◽  
pp. 290-295 ◽  
Author(s):  
Marcos Paulo Nagayassu ◽  
Luciana Keiko Shintome ◽  
Eduardo Shigueyuki Uemura ◽  
José Eduardo Junho de Araújo

The purpose of this in vitro study was to evaluate the effect of different surface treatments on the shear bond strength of a resin-based cement to porcelain. Sixty pairs of 50% aluminous porcelain discs were fabricated. In each pair, one disc measured 6 mm in diameter X 3 mm thickness (A) and the other measured 3 mm in diameter X 3mm thickness (B). The specimens were randomly assigned to 6 groups (n=10 pairs of discs), according to the surface treatment: etching with 10% hydrofluoric acid for 2 or 4min (G1 and G2); 50-µm particle aluminum oxide sandblasting for 5 s (G3); sandblasting followed by etching for 2 or 4min (G4 and G5) and control - no treatment (G6). A silane agent was applied to the treated surface of both discs of each pair. Bistite II DC dual-cure resin cement was applied and the B discs were bonded to their respective A discs. Specimens were stored in distilled water at 37ºC for 24 h and were tested in shear strength at a crosshead speed of 2 mm/min. Means in MPa were: G1: 14.21 ± 4.68; G2: 8.92 ± 3.02; G3: 10.04 ± 2.37; G4: 12.74 ± 5.15; G5: 10.99 ± 3.35; G6: 6.09 ± 1.84. Data were compared by one-way ANOVA and Tukey's test at 5% significance level. Bond strength recorded after 2-min acid etching was significantly higher than 4-min etching (p<0.05) and control (p<0.05), but did not differ significantlyfrom sandblasting alone (p>0.05) or followed by etching for 2 or 4 min (p>0.05). Within the limitations of an in vitro study, it may be concluded that 2-min hydrofluoric acid etching produced a favorable micromechanical retention that enhanced resin cement bond strength to porcelain.


2009 ◽  
Vol 34 (5) ◽  
pp. 558-564 ◽  
Author(s):  
F. Shafiei ◽  
I. Safarpoor ◽  
M. Moradmand ◽  
A. A. Alavi

Clinical Relevance Low dentin bond strength has been previously documented when one-bottle adhesives are used with self-cured resin-based composites. Low dentin bond strength may also occur when one-bottle adhesives are used with light-cured resin-based composites that are activated by soft-start or pulse-delay curing strategies.


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