Characterization of Adhesion Interlayer between Rubber and Brass by a Novel Method of Sample Preparation, Part.2. SEM-EDX Analysis of Adhesion Interlayer by Exposing Reaction Layer Using Filter

2004 ◽  
Vol 77 (7) ◽  
pp. 244-249 ◽  
Author(s):  
Takeshi HOTAKA ◽  
Yasuhiro ISHIKAWA ◽  
Kunio MORI
Keyword(s):  
Sample Preparation ◽  
Reaction Layer ◽  
Edx Analysis ◽  
Novel Method

TEM Sample Prep Tool Matching—DualBeam FIB Cut Look and Measure Monitoring for Process Control and Development in a 300 mm IC Fab

2016 ◽  
Author(s):  
Jangbae Jeon
Keyword(s):  
Process Control ◽  
Sample Preparation ◽  
Continuous Improvement ◽  
Process Time ◽  
Operational Monitoring ◽  
Thickness Control ◽  
Running Time ◽  
End Products ◽  
Novel Method

Abstract This work presents a novel method of continuous improvement for faster, better and cheaper TEM sample preparation using Cut Look and Measure (CLM). The improvement of the process is executed by operational monitoring of daily beam conditions, end products, bulk thickness control, recipe usage and tool running time. This process produces a consequent decrease in rework rate and process time. In addition, it also increases throughput with better quality TEM samples.

scholarly journals Creation of Ionically Crosslinked Tri-Layered Chitosan Membranes to Simulate Different Human Skin Properties

Materials ◽  
2021 ◽  
Vol 14 (7) ◽  
pp. 1807
Author(s):  
Rocío Guerle-Cavero ◽  
Blanca Lleal-Fontàs ◽  
Albert Balfagón-Costa
Keyword(s):  
Elastic Modulus ◽  
Human Skin ◽  
Sodium Tripolyphosphate ◽  
Snow Crab ◽  
Suitable Material ◽  
Cosmetic Industry ◽  
Novel Method ◽  
Current Article ◽  
Chitosan Membranes

In 2023, new legislation will ban the use of animals in the cosmetic industry worldwide. This fact, together with ethical considerations concerning the use of animals or humans in scientific research, highlights the need to propose new alternatives for replacing their use. The aim of this study is to create a tri-layered chitosan membrane ionically crosslinked with sodium tripolyphosphate (TPP) in order to simulate the number of layers in human skin. The current article highlights the creation of a membrane where pores were induced by a novel method. Swelling index, pore creation, and mechanical property measurements revealed that the swelling index of chitosan membranes decreased and, their pore formation and elasticity increased with an increase in the Deacetylation Grade (DDA). Additionally, the results demonstrate that chitosan’s origin can influence the elastic modulus value and reproducibility, with higher values being obtained with seashell than snow crab or shrimp shells. Furthermore, the data show that the addition of each layer, until reaching three layers, increases the elastic modulus. Moreover, if layers are crosslinked, the elastic modulus increases to a much greater extent. The characterization of three kinds of chitosan membranes was performed to find the most suitable material for studying different human skin properties.

Synthesis and characterization of a new magnetic restricted access molecularly imprinted polymer for biological sample preparation

2020 ◽  
Vol 24 ◽  
pp. 101002 ◽  
Author(s):  
Tássia Venga Mendes ◽  
Lidiane Silva Franqui ◽  
Mariane Gonçalves Santos ◽  
Célio Wisniewski ◽  
Eduardo Costa Figueiredo
Keyword(s):  
Sample Preparation ◽  
Molecularly Imprinted Polymer ◽  
Biological Sample ◽  
Synthesis And Characterization ◽  
Imprinted Polymer ◽  
Molecularly Imprinted ◽  
Restricted Access

Polycrystalline Silicon Gettering Layers with Controlled Residual Stress

2013 ◽  
Vol 205-206 ◽  
pp. 284-289 ◽  
Author(s):  
David Lysáček ◽  
Petr Kostelník ◽  
Petr Pánek
Keyword(s):  
Residual Stress ◽  
Vapor Deposition ◽  
Polycrystalline Silicon ◽  
Opposite Sign ◽  
Chemical Vapor ◽  
Pressure Chemical ◽  
Novel Method ◽  
The Individual ◽  
Scanning Electron

We report on a novel method of low pressure chemical vapor deposition of polycrystalline silicon layers used for external gettering in silicon substrate for semiconductor applications. The proposed method allowed us to produce layers of polycrystalline silicon with pre-determined residual stress. The method is based on the deposition of a multilayer system formed by two layers. The first layer is intentionally designed to have tensile stress while the second layer has compressive stress. Opposite sign of the residual stresses of the individual layers enables to pre-determine the residual stress of the gettering stack. We used scanning electron microscopy for structural characterization of the layers and intentional contamination for demonstration of the gettering properties. Residual stress of the layers was calculated from the wafer curvature.

Graphite/UPE Nanocomposite: Transport, Thermal, Mechanical and Viscoelastic Properties

2019 ◽  
Vol 23 ◽  
pp. 201-212
Author(s):  
Shivkumari Panda ◽  
Dibakar Behera ◽  
Tapan Kumar Bastia
Keyword(s):  
Transport Properties ◽  
Unsaturated Polyester ◽  
Homogeneous Distribution ◽  
Thermo Gravimetric ◽  
New Class ◽  
The Matrix ◽  
Novel Method ◽  
Water Transport Properties ◽  
First Time

This chapter presents the preparation and characterization of some unique properties of nanocomposites by dispersing graphite flakes in commercial unsaturated polyester (UPE) matrix. The composite was prepared by a novel method with the use of solvent swelling technique. Three different specimens of UPE/graphite nanocomposites were fabricated with addition of 1, 2 and 3 wt% of graphite flakes. Except mechanical, viscoelastic and thermo gravimetric properties, transport properties like electrical conductivity, thermal conductivity and water transport properties were studied for the first time. Graphite flakes propose enhanced properties to the composites suggesting homogeneous distribution of the nanofiller in the matrix and strong interaction with the matrix. 2wt% nanofiller loading showed superior essential characteristics and after that the properties reduced may be due to the nucleating tendency of the nanofiller particles. The XRD pattern showed the compatibility of the graphite flakes by introducing a peak around 26.550 in the nanocomposites. SEM Properties are also in agreement with the compatibility. Nanocomposite with 2wt% graphite also showed remarkable enhancement in transport, mechanical, viscoelastic and thermo gravimetric properties. So by introduction of a small quantity of graphite endow the new class of multiphase nanocomposites with inimitable structure and tremendous application.

scholarly journals Visual Biochemistry: modular microfluidics enables kinetic insight from time-resolved cryo-EM

2020 ◽  
Author(s):  
Märt-Erik Mäeots ◽  
Byungjin Lee ◽  
Andrea Nans ◽  
Seung-Geun Jeong ◽  
Mohammad M. N. Esfahani ◽  
...  
Keyword(s):  
Sample Preparation ◽  
Reaction Intermediates ◽  
Protein Distribution ◽  
Time Resolved ◽  
Biochemical Processes ◽  
Molecular Events ◽  
Biophysical Analysis ◽  
Common Strategy ◽  
Set Up

AbstractMechanistic understanding of biochemical reactions requires structural and kinetic characterization of the underlying chemical processes. However, no single experimental technique can provide this information in a broadly applicable manner and thus structural studies of static macromolecules are often complemented by biophysical analysis. Moreover, the common strategy of utilizing mutants or crosslinking probes to stabilize otherwise short-lived reaction intermediates is prone to trapping off-pathway artefacts and precludes determining the order of molecular events. To overcome these limitations and allow visualisation of biochemical processes at near-atomic spatial resolution and millisecond time scales, we developed a time-resolved sample preparation method for cryo-electron microscopy (trEM). We integrated a modular microfluidic device, featuring a 3D-mixing unit and a delay line of variable length, with a gas-assisted nozzle and motorised plunge-freeze set-up that enables automated, fast, and blot-free sample vitrification. This sample preparation not only preserves high-resolution structural detail but also substantially improves protein distribution across the vitreous ice. We validated the method by examining the formation of RecA filaments on single-stranded DNA. We could reliably visualise reaction intermediates of early filament growth across three orders of magnitude on sub-second timescales. Quantification of the trEM data allowed us to characterize the kinetics of RecA filament growth. The trEM method reported here is versatile, easy to reproduce and thus readily adaptable to a broad spectrum of fundamental questions in biology.

scholarly journals Characterization of Glass Delamination by TEM: Results from a New Sample Preparation Technique

2017 ◽  
Vol 25 (1) ◽  
pp. 36-41
Author(s):  
Elaine F. Schumacher ◽  
Heidi M. Talesky ◽  
Kristie J. Diebold
Keyword(s):  
Sample Preparation ◽  
Preparation Technique ◽  
Sample Preparation Technique
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