scholarly journals Effect of Cr Diffused Layer Formed by AIH-FPP Treatment on Adhesion of DLC Films to a Carbon Steel Substrate

2018 ◽  
Vol 59 (4) ◽  
pp. 642-647 ◽  
Author(s):  
Shogo Takesue ◽  
Hiroyuki Akebono ◽  
Mizuki Furukawa ◽  
Shoichi Kikuchi ◽  
Jun Komotori ◽  
...  
Keyword(s):  
2019 ◽  
Vol 24 (4) ◽  
pp. 51-58
Author(s):  
Le Hong Quan ◽  
Nguyen Van Chi ◽  
Mai Van Minh ◽  
Nong Quoc Quang ◽  
Dong Van Kien

The study examines the electrochemical properties of a coating based on water sodium silicate and pure zinc dust (ZSC, working title - TTL-VN) using the Electrochemical Impedance Spectra (EIS) with AutoLAB PGSTAT204N. The system consists of three electrodes: Ag/AgCl (SCE) reference electrode in 3 M solution of KCl, auxiliary electrode Pt (8x8 mm) and working electrodes (carbon steel with surface treatment up to Sa 2.5) for determination of corrosion potential (Ecorr) and calculation of equivalent electric circuits used for explanation of impedance measurement results. It was shown that electrochemical method is effective for study of corrosion characteristics of ZSC on steel. We proposed an interpretation of the deterioration over time of the ability of zinc particles in paint to provide cathodic protection for carbon steel. The results show that the value of Ecorr is between -0,9 and -1,1 V / SCE for ten days of diving. This means that there is an electrical contact between the zinc particles, which provides good cathodic protection for the steel substrate and most of the zinc particles were involved in the osmosis process. The good characteristics of the TTL-VN coating during immersion in a 3,5% NaCl solution can also be explained by the preservation of corrosive zinc products in the coating, which allows the creation of random barrier properties.


2011 ◽  
Vol 686 ◽  
pp. 569-573 ◽  
Author(s):  
Ming Feng Tan ◽  
Wan Chang Sun ◽  
Lei Zhang ◽  
Quan Zhou ◽  
Jin Ding

Electroless Ni-P coating containing ZrO2particles was successfully co-deposited on low carbon steel substrate. The surface and cross-sectional micrographs of the composite coatings were observed with scanning electron microscopy (SEM). And the chemical composition of the coating was analyzed with energy dispersive spectroscopy (EDS). The oxidation resistance was evaluated by weight gains during high temperature oxidation test. The results showed that the embedded ZrO2particles with irregular shape uniformly distributed in the entire Ni-P matrix, and the coating showed a good adhesion to the substrate. The weight gain curves of Ni-P-ZrO2composite coatings and Ni-P coating at 923K oxidation experiments were in accordance with . The ZrO2particles in Ni-P matrix could significantly enhance the high temperature oxidation resistance of the carbon steel substrate as compared to pure Ni-P coating.


2013 ◽  
Vol 734-737 ◽  
pp. 2269-2272
Author(s):  
Hong Mei Zhu ◽  
Shu Mei Lei ◽  
Tong Chun Kuang

In this paper, a low carbon steel was used as the substrate to prepare the carbon nanostructural materials by the oxygen-acetylene flame method. The experimental results show that the composite products including nodular carbon nanoparticles and amorphous carbon were obtained on the substrate after a mechanical polishing pretreatment. Comparatively, the short tubular carbon nanofibers with the diameter of around 100 nm were deposited on the substrate pretreated by dipping in the concentrated nitric acid solution. The possible mechanism for the growth of such carbon nanofibers was discussed.


2007 ◽  
Vol 190 (1-3) ◽  
pp. 204-210 ◽  
Author(s):  
B. Uyulgan ◽  
E. Dokumaci ◽  
E. Celik ◽  
I. Kayatekin ◽  
N.F. Ak Azem ◽  
...  

2006 ◽  
Vol 201 (6) ◽  
pp. 3116-3122 ◽  
Author(s):  
K. Raeissi ◽  
M.R. Bateni ◽  
A. Saatchi ◽  
M.A. Golozar ◽  
J.A. Szpunar

2012 ◽  
Vol 57 (2) ◽  
pp. 517 ◽  
Author(s):  
M. Żelechower ◽  
J. Kliś ◽  
E. Augustyn ◽  
J. Grzonka ◽  
D. Stróż ◽  
...  

The Microstructure of AnnealedGalfanCoating on Steel SubstrateThe commercially availableGalfancoating containing 5-7wt.% of Al deposited on the low carbon steel substrate by hot dipping has been examined with respect to the microstructure of the coating/substrate interface area. The application of several experimental techniques (SEM/EDS, XRD, TEM/AEM/EDS/ED) allowed demonstrating the two-phase structure of the alloy coating in non-treated, commercially availableGalfansamples: Zn-rich pre-eutectoidηphase grains are surrounded by lamellar eutectics ofβ-Al andη-Zn. The transition layer between the alloy coating and steel substrate with the considerably higher Al content (SEM/EDS, TEM/EDS) has been found in both non-treated and annealed samples (600°C/5 minutes). Only the monoclinic FeAl3Znxphase however was revealed in the annealed sample (TEM/electron diffraction) remaining uncertain the presence of the orthorhombic Fe2Al5Znxphase, reported by several authors.


Materials ◽  
2019 ◽  
Vol 12 (12) ◽  
pp. 1960 ◽  
Author(s):  
Yue Li ◽  
Chunchun Wu ◽  
Ming Xue ◽  
Jiawen Cai ◽  
Yi Huang ◽  
...  

Anticorrosive coatings prepared by sol-gel derived approaches have become an emergent research area in the field of corrosion prevention materials. Furthermore, enhanced coating thickness can greatly improve the barrier effect of the sol-gel coatings, thus influencing their service life in industrial applications. Here, we propose the preparation of a two-layer coating system using a low-cost sol-gel derived method. The coating structure was composed of first an underlying layer incorporated with silica and titania powder as filler and pigment materials, and a second translucent topcoat containing a colloidal silica sol-gel matrix crosslinked by methyltrimethoxysilane (MTMS). This coating system was applied on Q235 carbon steel substrate by a two-step spray deposition method, resulting in an enhanced coating thickness of around 35 μm. The physical and morphological properties of the coatings were characterized using multiple techniques, including scanning electron microscopy (SEM), energy dispersive spectroscopy (EDS) and atomic force microscopy (AFM). The anticorrosion performance of the sol-gel coatings was studied by a salt spray test, outdoor exposure test and electrochemical impedance spectroscopy (EIS). Results revealed that this two-layer coating system exhibited excellent physical and anticorrosion properties, and that the topcoat played a crucial role in maintaining the barrier effect and preventing water leakage.


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