scholarly journals In vitro biocompatibility of nickel-titanium esthetic orthodontic archwires

2016 ◽  
Vol 86 (5) ◽  
pp. 789-795 ◽  
Author(s):  
Roberto Rongo ◽  
Rosa Valletta ◽  
Rosaria Bucci ◽  
Virginia Rivieccio ◽  
Angela Galeotti ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Steel Wire ◽  
Nickel Titanium ◽  
Experimental Conditions ◽  
In Vitro Biocompatibility ◽  
Diphenyltetrazolium Bromide ◽  
Titanium Wire ◽  
Orthodontic Archwires ◽  
Niti Wires

ABSTRACT Objective:  To investigate the cytotoxicity of nickel-titanium (NiTi) esthetic orthodontic archwires with different surface coatings. Materials and Methods:  Three fully coated, tooth-colored NiTi wires (BioCosmetic, Titanol Cosmetic, EverWhite), two ion-implanted wires (TMA Purple, Sentalloy High Aesthetic), five uncoated NiTi wires (BioStarter, BioTorque, Titanol Superelastic, Memory Wire Superelastic, and Sentalloy), one β-titanium wire (TMA), and one stainless steel wire (Stainless Steel) were considered for this study. The wire samples were placed at 37°C in airtight test tubes containing Dulbecco’s Modified Eagle’s Medium (0.1 mg/mL) for 1, 7, 14, and 30 days. The cell viability of human gingival fibroblasts (HGFs) cultured with this medium was assessed by the 3-(4,5-dimethylthiazol-2-yl)-2,5-diphenyltetrazolium bromide (MTT) assay. Data were analyzed by a two-way analysis of variance (α  =  .05). Results:  The highest cytotoxic effect was reached on day 30 for all samples. The archwires exhibited a cytotoxicity on HGFs ranging from “none” to “slight,” with the exception of the BioTorque, which resulted in moderate cytotoxicity on day 30. Significant differences were found between esthetic archwires and their uncoated pairs only for BioCosmetic (P  =  .001) and EverWhite (P < .001). Conclusions:  Under the experimental conditions, all of the NiTi esthetic archwires resulted in slight cytotoxicity, as did the respective uncoated wires. For this reason their clinical use may be considered to have similar risks to the uncoated archwires.

Comparison of Chemical Properties and Ni Release of Stainless Steel and Nickel Titanium Wires

2014 ◽  
Vol 884-885 ◽  
pp. 560-565 ◽  
Author(s):  
Wassana Wichai ◽  
Niwat Anuwongnukroh ◽  
Surachai Dechkunakorn
Keyword(s):  
Stainless Steel ◽  
Corrosion Resistance ◽  
Artificial Saliva ◽  
Steel Wire ◽  
Nickel Titanium ◽  
The Other ◽  
Stainless Steel Wire ◽  
Niti Wire ◽  
Titanium Wire ◽  
Niti Wires

Objective: This study aimed to determine the composition and corrosion resistance of stainless steel and nickel titanium (NiTi) archwires and to compare Ni released from simulated standard fixed orthodontic appliances ligated with stainless steel and NiTi wires in artificial saliva at pH 5.14 and pH 6.69. in 4 weeks at 37oC. Materials and Method: Two commercial rectangular wires, 0.016 x 0.022 in size were studied, one Ormco stainless steel wire and another Ormco nickel titanium wire. Their composition was analyzed by an energy disporsive X-ray spectrometer (ESC) and their corrosion resistance was evaluated by a potentiodynamic polarization technique. For Ni release, the twenty-eight simulated fixed appliance sample sets were used, each corresponding to one half-maxillary arch. The samples were divided in 2 groups (14 sets per group). The first one was ligated to Ormco stainless steel archwires and the other one to Ormco NiTi archwires with elastomeric ligatures. Half sets of each group were immersed in 50 ml artificial saliva at pH 5.14 and the other half were immersed at pH 6.69. Ni release was quantified using flame atomic absorption spectrophotometry. Statistical analysis of variance (t-test) was determined on days 1, 4, 7, 9, 14, 21 and 28 comparing the amount of Ni released between groups. Results: Stainless steel wire was composed of Ni, Cr, Si, Mn and Fe while the nickel titanium wire was composed of Ti, Ni and Cr. NiTi wire has more percentage of Ni and therefore has less corrosion resistance than stainless steel wire. For Ni release, stainless steel and NiTi continuously increased at the time intervals for both pH levels. For group one, stainless steel wire had more Ni release at pH 5.14 and for the other group, NiTi wire had more Ni-release at pH 6.69. At 4 weeks, the Ni release of one half-maxillary arch was 1.383 ppm (1383 μg/l) at pH 5.14 and 1.079 ppm (1078 μg/l) at pH 6.69 for stainless steel wire while it was 1.221 ppm (1221 μg/l) at pH 5.14 and 1.267 ppm (1267μg/l) at pH 6.69 for NiTi wire. No significant difference was found in the amount of Ni release from stainless steel and NiTi wires at pH 5.14 and pH 6.69 in the different time intervals except on day 1 wherein the stainless steel archwire was significantly different (p<0.05) at pH 5.14 and pH 6.69. Conclusions: The NiTi wire had more Ni contain and less corrosion resistance than stainless steel wire. Stainless steel had more Ni release at pH 5.14 than pH 6.69 but NiTi had greater Ni release at pH 6.69 than pH 5.14.

scholarly journals In Vitro Corrosion Behavior of Lingual Orthodontic Archwires

2011 ◽  
Vol 2011 ◽  
pp. 1-9 ◽  
Author(s):  
Carlos Suárez ◽  
Teresa Vilar ◽  
Pablo Sevilla ◽  
Javier Gil
Keyword(s):  
Differential Scanning Calorimetry ◽  
Stainless Steel ◽  
Rhombohedral Phase ◽  
Nickel Titanium ◽  
Scanning Calorimetry ◽  
Lingual Orthodontics ◽  
Phase Transition Temperatures ◽  
Different Types ◽  
Orthodontic Archwires

Objectives. To investigate the in vitro electrochemical corrosive behavior of archwires used in lingual orthodontics and the effects on the phase transition temperatures.Materials and Methods. Six different types of archwires of stainless steel, titanium-molybdenum, nickel-titanium and nickel-titanium-copper were used. Corrosion tests were performed following ISO-standard 10993-15:2000. Differential scanning calorimetry and scanning electron microscopy were used.Results. The stainless steel archwires showed anEpitaround −600 mV, and those of titanium alloys showedEpitvalues around 1000 mV. Differential scanning calorimetry detected a rhombohedral phase in nickel-titanium archwires, while it was not detected in nickel-titanium-copper wires. A difference of 2°C to 3.5°C from the manufacturer's claim was found in the as-received and polarized samples, respectively.Conclusions. The 0.016 stainless steel archwires were found to be the less resistant to corrosion. A rhombohedral phase was detected on the nickel-titanium archwires. No major differences were observed among groups concerning phase transformation temperatures.

scholarly journals Comparison of Galvanic Corrosion Potential of Metal Injection Molded Brackets to that of Conventional Metal Brackets with Nickel-Titanium and Copper Nickel-Titanium Archwire Combinations

2013 ◽  
Vol 14 (3) ◽  
pp. 488-495 ◽  
Author(s):  
S Chidambaram ◽  
M Vijay ◽  
D Praveen Kumar Varma ◽  
K Baburam Reddy ◽  
D Ravindranath ◽  
...  
Keyword(s):  
Stainless Steel ◽  
Corrosion Potential ◽  
Galvanic Corrosion ◽  
Nickel Titanium ◽  
Copper Nickel ◽  
Conventional Brackets ◽  
Titanium Wire ◽  
Conventional Bracket ◽  
Conventional Stainless Steel

ABSTRACT Aim The aim of the study is to investigate the galvanic corrosion potential of metal injection molding (MIM) brackets to that of conventional brackets under similar in vitro conditions with nickel-titanium and copper nickel-titanium archwires. Materials and methods Twenty-five maxillary premolar MIM stainless steel brackets and 25 conventional stainless steel brackets and archwires, 0.16 inch, each 10 mm length, 25 nickeltitanium wires, 25 copper nickel-titanium wires were used. They were divided into four groups which had five samples each. Combination of MIM bracket with copper nickel-titanium wire, MIM bracket with nickel-titanium wire and conventional stainless steel brackets with copper nickel-titanium wire and conventional stainless steel brackets with nickel-titanium wires which later were suspended in 350 ml of 1 M lactic acid solution media. Galvanic corrosion potential of four groups were analyzed under similar in vitro conditions. Precorrosion and postcorrosion elemental composition of MIM and conventional stainless steel bracket by scanning electron microscope (SEM) with energy dispersive spectroscope (EDS) was done. Results MIM bracket showed decreased corrosion susceptibility than conventional bracket with copper nickeltitanium wire. Both MIM and conventional bracket showed similar corrosion resistance potential in association with nickel-titanium archwires. It seems that both brackets are more compatible with copper nickel-titanium archwires regarding the decrease in the consequences of galvanic reaction. The EDS analysis showed that the MIM brackets with copper nickel-titanium wires released less metal ions than conventional bracket with copper nickeltitanium wires. Conclusion MIM brackets showed decreased corrosion susceptibility, copper nickel-titanium archwires are compatible with both the brackets than nickel-titanium archwires. Clinical significance Clinically MIM and conventional brackets behaved more or less similarly in terms of corrosion resistance. In order to decrease the corrosion potential of MIM brackets, more precise manufacturing technique should be improved to get a more smoother surface finish. How to cite this article Varma DPK, Chidambaram S, Reddy KB, Vijay M, Ravindranath D, Prasad MR. Comparison of Galvanic Corrosion Potential of Metal Injection Molded Brackets to that of Conventional Metal Brackets with Nickel-Titanium and Copper Nickel-Titanium Archwire Combinations. J Contemp Dent Pract 2013;14(3):488-495.

scholarly journals Clinicians' Choices in Selecting Orthodontic Archwires

2013 ◽  
Vol 59 (4) ◽  
pp. 212-218
Author(s):  
Pop Silvia-Izabella ◽  
Păcurar Mariana ◽  
Bratu Dana Cristina ◽  
Pop Rv ◽  
Chibelean Manuela
Keyword(s):  
Stainless Steel ◽  
Titanium Alloy ◽  
Orthodontic Treatment ◽  
Nickel Titanium ◽  
Beta Titanium ◽  
Personal Opinion ◽  
Fixed Appliances ◽  
Round Section ◽  
Orthodontic Archwires ◽  
Niti Wires

Abstract Objective: The aim of this study was to assess the choices made by clinicians in selecting archwires during the initial, intermediate and final stages of orthodontic treatment with fixed appliances. Methods: We carried out a questionnaire-based study at the Orthodontics and Pedodontics Clinic Târgu Mureș, between March 2012 and September 2012. The questionnaires consisted of two parts: the first included questions related to the dimension, alloy used in fabrication, section (round or rectangular) and manufacturer of the archwires used by the orthodontists in their orthodontic practice, the second part was concerned with their personal opinion about the physical properties and disadvantages of the archwires. Results: From a total number of 90 distributed questionnaires, 62 were returned. The majority of clinicians are using stainless steel (SS) and nickel-titanium alloy (NiTi) wires in their fixed orthodontic treatments, very few are using beta-titanium (Beta Ti), copper nickel-titanium (Co- NiTi) and esthetic archwires. The preferred dimension seem to be 0.022 inches in the appliance system. Regarding the wire dimensions, 0.014, 0.016 inch wires are mostly used from the round section group and 0.016 × 0.022 inch, 0.017 × 0.025 inch from the rectangular ones. Conclusions: There is a general lack of agreement between the clinicians surveyed regarding the properties of an ideal archwire and the disadvantages of the used wires. The most frequently used alloys seemed to be the SS and NiTi

scholarly journals Comparative Evaluation of Frictional forces between different Archwire-bracket Combinations

2014 ◽  
Vol 4 (1) ◽  
pp. 22-28 ◽  
Author(s):  
Vinit Singh ◽  
Swati Acharya ◽  
Satyabrata Patnaik ◽  
Smruti Bhusan Nanda
Keyword(s):  
Stainless Steel ◽  
Tooth Movement ◽  
Testing Machine ◽  
Frictional Resistance ◽  
Nickel Titanium ◽  
Orthodontic Bracket ◽  
Fixed Appliance ◽  
Beta Titanium ◽  
Frictional Forces

Introduction: During sliding mechanics, frictional resistance is an important counterforce to orthodontic tooth movement; whichmust be controlled to allow application of light continuous forces.Objective: To investigate static and kinetic frictional resistance between three orthodontic brackets: ceramic, self-ligating, andstainless steel, and three 0.019×0.025” archwires: stainless steel, nickel-titanium, titanium-molybdenum.Materials & Method: The in vitro study compared the effects of stainless steel, nickel-titanium, and beta-titanium archwires onfrictional forces of three orthodontic bracket systems: ceramic, self-ligating, and stainless steel brackets. All brackets had 0.022”slots, and the wires were 0.019×0.025”. Friction was evaluated in a simulated half-arch fixed appliance on a testing machine. Thestatic and kinetic friction data were analyzed with 1-way analysis of variance (ANOVA) and post-hoc Duncan multiple rangetest.Result: Self-ligating (Damon) brackets generated significantly lower static and kinetic frictional forces than stainless steel (Gemini)and ceramic brackets (Clarity). Among the archwire materials, Beta-titanium showed the maximum amount of frictional forceand stainless steel archwires had the lowest frictional force.Conclusion: The static and kinetic frictional force for stainless steel bracket was lowest in every combination of wire.

scholarly journals Orthodontic Aligner Incorporating Eucommia ulmoides Exerts Low Continuous Force: In Vitro Study

Materials ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 4085
Author(s):  
Sayuri Inoue ◽  
Satoshi Yamaguchi ◽  
Hiroshi Uyama ◽  
Takashi Yamashiro ◽  
Satoshi Imazato
Keyword(s):  
Water Immersion ◽  
In Vitro Study ◽  
Nickel Titanium ◽  
Orthodontic Appliances ◽  
Orthodontic Appliance ◽  
Measuring Device ◽  
Orthodontic Force ◽  
Custom Made ◽  
Titanium Wire

The aim of this study was to investigate the orthodontic force exerted by thermoplastic orthodontic appliances incorporating Eucommiaulmoides in terms of usefulness as the aligner-type orthodontic device. Erkodur, Essix C+®, Eucommia elastomer, and edgewise brackets were used (n = 3, each; thickness = 1.0 mm, each). The orthodontic force on the upper right incisor was measured every 24 h for two weeks using a custom-made measuring device. The force of the Eucommia elastomer (4.25 ± 0.274 N) and multi bracket system (5.32 ± 0.338 N) did not change from the beginning to the end (p > 0.01). The orthodontic force exerted by the Eucommia elastomer was lower than that of the multi-bracket orthodontic appliance from the beginning to the end. The force of Erkodur significantly decreased from the beginning to 24 h (6.47 ± 1.40 N) and 48 h (3.30 ± 0.536 N) (p < 0.01). The force of Essix C+® significantly decreased from the beginning (13.2 ± 0.845 N) to 24 h (8.77 ± 0.231 N) (p < 0.01). The thermoplastic orthodontic appliance made of Eucommia elastomer continuously exerted a constant orthodontic force for two weeks under water immersion conditions. The orthodontic force of Eucommia elastomer was found to be similar to the orthodontic force exerted by the multi-bracket orthodontic appliance with 0.019 × 0.025 in nickel–titanium wire. These results suggest that the Eucommia elastomer has possibly become one of the more useful materials to form thermoplastic orthodontic appliance exerting low continues orthodontic force.

scholarly journals Surface Properties and Biocompatibility of Anodized Titanium with a Potential Pretreatment for Biomedical Applications

Metals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 1090
Author(s):  
Bai-Hung Huang ◽  
Yi-Jung Lu ◽  
Wen-Chien Lan ◽  
Muhammad Ruslin ◽  
Hung-Yang Lin ◽  
...  
Keyword(s):  
Porous Structure ◽  
Biomedical Applications ◽  
Grazing Incidence ◽  
Acid Pretreatment ◽  
Osteoblast Cells ◽  
In Vitro Biocompatibility ◽  
Porous Ti ◽  
Diphenyltetrazolium Bromide ◽  
Anodized Titanium

The effects of anodized titanium (Ti) with a potential hydrogen fluoride (HF) acid pretreatment through cathodization on the formation of nano-porous Ti dioxide (TiO2) layer were characterized using field-emission scanning electron microscopy, grazing incidence X-ray diffractometer, and contact angle goniometer. The biocompatibility was determined by 3-[4,5-dimethylthiazol-2-yl]-2,5-diphenyltetrazolium bromide (MTT) test. Analytical results found that a well-aligned nano-porous structure was formed on the anodized Ti surface with HF pretreatment concentration above 0.5%. Microstructure of the nano-porous Ti dioxide surface generated by anodization with HF pretreatment was composed of anatase and rutile phases, while the anodized Ti sample with HF pretreatment concentration of 0.5% presented excellent hydrophilicity surface. An in-vitro biocompatibility also indicated that osteoblast cells grown on the surface of the anodized Ti sample with HF pretreatment increased with the increase of culture time. The filopodia of osteoblast cells not only adhered flat, but also tightly grabbed the nano-porous structure for promoting cell adhesion and proliferation. Therefore, the anodized Ti with HF pretreatment can form a functionalized surface with great biocompatibility for biomedical applications, particularly for dental implants.

scholarly journals In Vitro Frictional Forces Generated by Three Different Ligation Methods

2008 ◽  
Vol 78 (5) ◽  
pp. 917-921 ◽  
Author(s):  
Paola Gandini ◽  
Linda Orsi ◽  
Chiara Bertoncini ◽  
Sarah Massironi ◽  
Lorenzo Franchi
Keyword(s):  
Steel Wire ◽  
Testing Machine ◽  
Low Friction ◽  
Instron Testing Machine ◽  
Resistance To Sliding ◽  
Titanium Wire ◽  
Frictional Forces ◽  
Conventional Bracket ◽  
Wire Resistance

Abstract Objective: To test the hypothesis that there is no difference between the frictional forces produced by a passive self-ligating bracket (SLB) in vitro and a conventional bracket (CB) used with two types of elastomeric ligatures. Materials and Method: The brackets, wires and ligation methods used in vitro were a passive SLB and a CB used with two types of elastomeric ligatures (conventional elastomeric ligature [CEL] and unconventional elastomeric ligatures [UEL]). The bracket ligation systems were tested with two types of wires (0.014″ super elastic nickel titanium wire and 0.019″ × 0.025″ stainless steel wire). Resistance to sliding of the bracket/wire/ligature systems was measured with an experimental model mounted on the crosshead of an Instron testing machine with a 10 N load cell. Each sample was tested 10 consecutive times under a dry state. Results: Frictional forces close to 0 g were recorded in all tests with SLB and in all tests with UEL on CB with both wire types. Resistance to sliding increased significantly (87–177 g) (P &lt; .05) when CEL on CB was used with both wires. Conclusion: UELs may represent a valid alternative to passive SLBs for low-friction biomechanics.

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