Demonstration of Tubercle Bacilli in Sputum Smears: Selection of Choice Particles Compared with Various Sodium Hydroxide Concentration Techniques

1949 ◽  
Vol 64 (18) ◽  
pp. 574 ◽  
Author(s):  
George A. Spendlove ◽  
Martin Cummings ◽  
Robert A. Patnode
Keyword(s):  
Sodium Hydroxide ◽  
Sodium Hydroxide Concentration ◽  
Selection Of

Study on the Chemical Modification Process of Jute Fiber

TAPPI Journal ◽  
2010 ◽  
Vol 9 (2) ◽  
pp. 23-29 ◽  
Author(s):  
Wei-ming Wang ◽  
Zai-sheng Cai ◽  
Jian-yong Yu
Keyword(s):  
Sodium Hydroxide ◽  
Sodium Silicate ◽  
Treatment Time ◽  
Jute Fiber ◽  
Process Conditions ◽  
Silicate Concentration ◽  
Sodium Hydroxide Concentration ◽  
Liquor Ratio ◽  
Degumming Process ◽  
Selection Of

Degumming of pre-chlorite treated jute fiber was studied in this paper. The effects of sodium hydroxide concentration, treatment time, temperature, sodium silicate concentration, fiber-to-liquor ratio, penetrating agent TF-107B concentration, and degumming agent TF-125A concentration were the process conditions examined. With respect to gum decomposition, fineness and mechanical properties, sodium hydroxide concentration, sodium silicate concentration, and treatment time were found to be the most important parameters. An orthogonal L9(34) experiment designed to optimize the conditions for degumming resulted in the selection of the following procedure: sodium hydroxide of 12g/L, sodium silicate of 3g/L, TF-107B of 2g/L, TF-125A of 2g/L, treatment time of 105 min, temperature of 100°C and fiber to liquor ratio of 1:20. The effect of the above degumming process on the removal of impurities was also examined and the results showed that degumming was an effective method for removing impurities, especially hemicellulose.

scholarly journals Study on the Chemical Modification Process of Jute Fiber

2008 ◽  
Vol 3 (2) ◽  
pp. 155892500800300 ◽  
Author(s):  
Wei-ming Wang ◽  
Zai-sheng Cai ◽  
Jian-yong Yu
Keyword(s):  
Sodium Hydroxide ◽  
Sodium Silicate ◽  
Treatment Time ◽  
Jute Fiber ◽  
Process Conditions ◽  
Silicate Concentration ◽  
Sodium Hydroxide Concentration ◽  
Liquor Ratio ◽  
Degumming Process ◽  
Selection Of

Degumming of pre-chlorite treated jute fiber was studied in this paper. The effects of sodium hydroxide concentration, treatment time, temperature, sodium silicate concentration, fiber-to-liquor ratio, penetrating agent TF-107B concentration and degumming agent TF-125A concentration were the process conditions examined. With respect to gum decomposition, fineness and mechanical properties, sodium hydroxide concentration, sodium silicate concentration and treatment time were found to be the most important parameters. An orthogonal L9(34) experiment designed to optimize the conditions for degumming resulted in the selection of the following procedure: sodium hydroxide of 12g/L, sodium silicate of 3g/L, TF-107B of 2g/L, TF-125A of 2g/L, treatment time of 105 min, temperature of 100°C and fiber to liquor ratio of 1:20. The effect of the above degumming process on the removal of impurities was also examined and the results showed that degumming was an effective method for removing impurities, especially hemicellulose.

scholarly journals Central Composite Design and Desirability of RSM for Optimization of Biodiesel Production from Mixture of Animal Waste Fat Oil and used Cooking Oil

2020 ◽  
Vol 9 (4) ◽  
pp. 1565-1571
Keyword(s):  
Reaction Time ◽  
Sodium Hydroxide ◽  
Maximum Yield ◽  
Animal Waste ◽  
Sodium Hydroxide Concentration ◽  
Used Cooking Oil ◽  
Input Parameters ◽  
Desirability Approach ◽  
Central Composite ◽  
Waste Fat

In this work, central composite design(CCD) and desirability approach of Response surface methodology (RSM) has been used for optimization of biodiesel yield produced from mixture of animal waste fat oil and used cooking oil (AWO) in the ratio of 1:1through alkaline transesterification process. In this work, methanol quantity, reaction time and sodium hydroxide concentration are selected as input parameters and yield selected as response. The combined effect of methanol quantity, reaction time and sodium hydroxide concentration were investigated and optimized by using RSM. The second order model is generated to predict yield as a function of methanol quantity, reaction time and sodium hydroxide concentration. A statistical model predicted the maximum yield of 96.9779% at 35ml methanol quantity (% v/v of oil), 75 min. reaction time and 0.6g (% wt./v of oil) of sodium hydroxide. Experimentally, the maximum yield of 97% was obtained at the above optimized input parameters. The variation of 0.02% was observed between experimental and predicted values. In this work, an attempt has also made to use desirability approach of RSM to optimize the input parameters to predict maximum yield. Desirability approach predicts maximum yield (97.075%) at CH3OH (35.832% vol. /vol. of oil), NaOH (0.604 % wt./vol. of oil) and reaction time (79.054min.) was found for the AWO.

Stress Corrosion Cracking of Steam Generator Tube Materials in Sodium Hydroxide Solutions

CORROSION ◽  
1978 ◽  
Vol 34 (11) ◽  
pp. 369-378 ◽  
Author(s):  
R. S. PATHANIA ◽  
J. A. CHITTY
Keyword(s):  
Stress Corrosion ◽  
Sodium Hydroxide ◽  
Applied Stress ◽  
Steam Generator ◽  
Stress Corrosion Cracking ◽  
Corrosion Cracking ◽  
Sodium Hydroxide Concentration ◽  
Inconel 600 ◽  
Steam Generator Tubing ◽  
Monel 400

Abstract Stress corrosion cracking (SCC) tests were carried out on specimens of Monel 400, Inconel 600, and Sanicro 30 steam generator tubing in solutions containing 10 to 500 g NaOH/kg H2O at 300 C for times up to 600 days. Applied stress and sodium hydroxide concentration had a significant effect on the (SCC) resistance of the three materials.

scholarly journals Studies on the modification of fly ash structure with alkaline pre-treatment as a green composite flame retardant filler

2021 ◽  
Vol 1195 (1) ◽  
pp. 012015
Author(s):  
N A M Radzi ◽  
A H Sofian ◽  
S S Jamari
Keyword(s):  
Fly Ash ◽  
Pore Size ◽  
Sodium Hydroxide ◽  
Sodium Hydroxide Solution ◽  
Morphological Structure ◽  
Green Composite ◽  
Sodium Hydroxide Concentration ◽  
Physiochemical Properties ◽  
Hydrophobic Polymer ◽  
Pre Treatment

Abstract A green composite made up of renewable and recyclable materials has become one of the advanced material’s attractive topics. The smooth fly ash surface used in the green composite for flame retardancy enhancement are hard to bind with hydrophobic polymer. Thus, the surface modification of this filler is needed to increase its surface roughness and pore size to be more compatible with its polymer matrix. In this research study, the alkaline pre-treatment of fly ash has been performed by using sodium hydroxide solution (NaOH) with various concentrations (5 w/w%, 10 w/w%, 15 w/w%, 20 w/w%). For pore size and morphological of the filler’s evaluation, few analyses such as Scanning Electron Microscopy-Energy Dispersive X-Ray (SEM-EDX), Barret-Joyner-Halenda (BJH) and Brunauer-Emmett-Teller (BET) pore size and volume analysis were conducted. Treated fly ash with 20 w/w% sodium hydroxide concentration gives the better morphological structure in terms of pore diameter, volume, area and high composition of aluminium, silicon with lower calcium and sulphur contents compared to others. Hence, the potential of the physiochemical properties of the green composite produced by using this modified filler will be improved as the adhesiveness of the filler with its matrix increased.

scholarly journals Bleaching Flax Roving With Poly(Acrylic Acid) Magnesium Salt As Oxygen Bleaching Stabilizer For Hydrogen Peroxide

2021 ◽  
Author(s):  
Jie Liu ◽  
Wenqi Jiang ◽  
Ling Sun ◽  
Chun Lv
Keyword(s):  
Hydrogen Peroxide ◽  
Acrylic Acid ◽  
Sodium Hydroxide ◽  
Sodium Silicate ◽  
Magnesium Salt ◽  
Capillary Effect ◽  
Sodium Hydroxide Concentration ◽  
Silicon Oxygen ◽  
Oxygen Bleaching ◽  
Poly Acrylic Acid

Abstract Alkali-oxygen one-bath scouring and bleaching process of the flax roving was studied by using a new type of synthesized non-silicon oxygen bleaching stabilizer Poly(acrylic acid) magnesium instead of sodium silicate. Based on the analysis of the effects of single factors such as sodium hydroxide concentration, hydrogen peroxide concentration, temperature, time and the amount of the synthesized non-silicon oxygen bleaching stabilizer poly(acrylic acid) magnesium salt on the performance of the bleached flax roving, including the whiteness, the breaking tenacity, the capillary effect and the weight loss ratio. The optimal process for the application of the stabilizer was determined by orthogonal test, namely, hydrogen peroxide concentration 8.5 g/L, sodium hydroxide concentration 5 g/L, sodium bisulfite 3 g/L, sodium carbonate 3 g/L, the synthesized non-silicon oxygen bleaching stabilizer poly(acrylic acid) magnesium 5.5 g/L, scoured and bleached at 90 ℃ for 60 min, and the bath ratio was 25:1. Compared with the traditional oxygen bleaching stabilizer sodium silicate, it not only has good ability to inhibit the rapid decomposition of hydrogen peroxide, but also has the advantages of higher whiteness, higher capillary effect, good feel and breaking tenacity, and can effectively solve the "silicon scale" problem and improve the quality of flax products.

Kinetics and Mechanism of the Formation and Decomposition of Imidazolin-4-ones from 2-(N-Benzoylamino)alkanamides in Aqueous Medium

1999 ◽  
Vol 64 (10) ◽  
pp. 1629-1640 ◽  
Author(s):  
Miloš Sedlák ◽  
Jiří Hanusek ◽  
Radim Bína ◽  
Jaromír Kaválek ◽  
Vladimír Macháček
Keyword(s):  
Sodium Hydroxide ◽  
Aqueous Medium ◽  
Sodium Hydroxide Solution ◽  
Base Catalysis ◽  
Cyclization Reactions ◽  
Sodium Hydroxide Concentration ◽  
Rate Limiting Step ◽  
Limiting Step ◽  
Reaction Constant ◽  
Rate Limiting

The cyclization reactions of substituted 2-(N-benzoyl-N-methyl)aminoalkanamides 1a-1g have been studied in aqueous medium. The Hammett reaction constant is ρ = 1.4 for the cyclization reactions of compounds 1a-1e in sodium hydroxide solutions. 2-[N-Methyl- N-(4-nitrobenzoyl)amino]-2-(4-nitrophenyl)propanamide (1g) is cyclized to imidazolinone 2g in aqueous amine buffers of pH 9-11.5; the reaction is subject to specific base catalysis in these media, and the rate-limiting step is the formation of a tetrahedral intermediate. In sodium hydroxide solution, the primary cyclization product is hydrolyzed to give an intermediate M which is subsequently decomposed to sodium 4-nitrobenzoate and 2-methylamino- 2-(4-nitrophenyl)propanamide. At low sodium hydroxide concentration, the rate-limiting step of the opening of imidazoline ring of compound 2g is non-catalyzed decomposition of the intermediate. At higher sodium hydroxide concentrations, the other reaction path begins to make itself felt: hydroxide-ion-catalyzed decomposition of the intermediate. The dependence of observed rate constant of cyclization of compound 1f on sodium hydroxide concentration was used to determine kinetically the value of pKa = 13.5 ± 0.1. The kinetic deuterium isotope effect of cyclization of compounds 1f giving 2f (kCH/kCD = 1.7) was determined in solutions of NaOD in D2O.

Sign in / Sign up

Export Citation Format

Share Document