scholarly journals Sinterability and characterization of Ag/Al2O3 metal and ceramic matrix composites processed by mechanical milling

2020 ◽  
Vol 52 (3) ◽  
pp. 245-255
Author(s):  
Ramin Davodi ◽  
Mohammad Ardestani ◽  
Arqavan Kazemi

In this research, the sinterability of Ag/Al2O3 milled powders with 10 and 90 wt%Ag were investigated. The powders were consolidated by two different processes including conventional and spark plasma sintering. The conventionally sintered composites with 90 wt%Ag were further densified by cold pressing and subsequent annealing at 700?C. The microstructural evaluations confirmed a fine dispersion of the constituents within the microstructure of the spark plasma sintered composites. Moreover, the results showed that the relative density, hardness, and flexural strength of the spark plasma sintered samples were much higher than those of the other samples. The hardness and flexural strength of Ag/10 wt%Al2O3 spark plasma sintered samples at 650?C were 146 HV and 264 MPa, respectively. However, unlike the composite with 90 wt%Ag, the applied sintering temperatures have not led to the synthesis of an Ag/90 wt% Al2O3 composite with the desired properties

2016 ◽  
Vol 56 (6) ◽  
pp. 636-640 ◽  
Author(s):  
N. A. Fedosova ◽  
É. M. Kol’tsova ◽  
N. A. Popova ◽  
E. V. Zharikov ◽  
E. S. Lukin

2016 ◽  
Vol 864 ◽  
pp. 47-51 ◽  
Author(s):  
Lydia Anggraini ◽  
Yuta Natsume ◽  
Kei Ameyama

Silicon nitride with 50 mass zirconia ceramic matrix composites were processed by mechanical milling (MM) followed by spark plasma sintering (SPS). Two different of Si3N4 particle shapes for create harmonic microstructure were investigated. The microstructure of Si3N4-ZrO2 with initial Si3N4 shape is like coin/flakes after MM for 144 ks was failed to create the harmonic microstructure after SPS. With another sphere shape of Si3N4 after MM for 144 ks, the harmonic microstructure could be formed after SPS. Thus, the initial powders shape of Si3N4 have an effect in the formation of harmonic microstructure could be fully achieved. The highest mechanical properties of Si3N4-ZrO2 are on the powders with mechanical milling time for 144 ks. The Si3N4 ceramic with homogeneous fine grains of ZrO2 dispersed on its surface was obtained, and the mechanical properties were improved. The Vickers hardness obtained on 144 ks is 1031 MPa and the bending strength is 262 MPa. The main factors explaining the improvement in the mechanical properties of Si3N4-ZrO2 are considered to be the porosity decrease caused by the particles shape and appropriate condition of powder processing i.e. MM and SPS.


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