scholarly journals ELECTROCHEMICAL OXIDATION OF ETHANOL USING Ni-Co-PVC COMPOSITE ELECTRODE

2011 ◽  
Vol 11 (1) ◽  
pp. 75-84 ◽  
Author(s):  
Riyanto Riyanto ◽  
Mohamed Rozali Othman ◽  
Jumat Salimon
Keyword(s):  
Polyvinyl Chloride ◽  
Electrochemical Behavior ◽  
Morphological Characteristics ◽  
Redox System ◽  
Electrochemical Technique ◽  
Metal Foil ◽  
Composite Electrodes ◽  
Nickel Metal ◽  
Nickel Cobalt

The morphological characteristics and electrochemical behavior of nickel metal foil (Ni), nickel-polyvinyl chloride (Ni-PVC) and nickel-cobalt-polyvinyl chloride (Ni-Co-PVC) electrodes in alkaline solution has been investigated. The morphological characteristics of the electrode surface were studied using SEM and EDS, while the electrochemical behavior of the electrodes was studied using cyclic voltammetry (CV). It was found that composite electrodes (Ni-PVC and Ni-Co-PVC) have a porous, irregular and rough surface. In situ studies using electrochemical technique using those three electrodes exhibited electrochemical activity for redox system, as well as selectivity in the electrooxidation of ethanol to acetic acid. The studies also found that an electrokinetics and electrocatalytic activity behaviors of the electrodes prepared were Ni metal foil

scholarly journals In situ synthesis of methane using Ag–GDC composite electrodes in a tubular solid oxide electrolytic cell: new insight into the role of oxide ion removal

2021 ◽  
Vol 5 (7) ◽  
pp. 2055-2064
Author(s):  
Saheli Biswas ◽  
Aniruddha P. Kulkarni ◽  
Daniel Fini ◽  
Sarbjit Giddey ◽  
Sankar Bhattacharya
Keyword(s):  
Electrolytic Cell ◽  
Composite Electrodes ◽  
Ion Removal ◽  
Single Temperature ◽  
Methanation Catalyst ◽  
Oxide Ion ◽  
Insight Into ◽  
Electrochemical Phenomenon

In situ synthesis of methane in a single-temperature zone SOEC in the absence of any methanation catalyst is a completely electrochemical phenomenon governed by the thermodynamic equilibrium of various reactions.

Rational Design and In-situ Formation of Nickel–Cobalt Nitride Multi-core/Hollow N-doped Carbon Shell Anode for Li-ion Batteries

2021 ◽  
pp. 129630
Author(s):  
Bong Kyun Kang ◽  
Yoo Jung Choi ◽  
Hyung Wook Choi ◽  
Seok Bin Kwon ◽  
Suji Kim ◽  
...  
Keyword(s):  
Rational Design ◽  
Carbon Shell ◽  
Li Ion Batteries ◽  
Nickel Cobalt ◽  
Li Ion ◽  
In Situ Formation

scholarly journals Radiomorphology of the Habib Sealer-Induced Resection Plane during Long-Time Followup:A Longitudinal Single Center Experience after 64 Radiofrequency-AssistedLiver Resections

HPB Surgery ◽  
2010 ◽  
Vol 2010 ◽  
pp. 1-7 ◽  
Author(s):  
Robert Kleinert ◽  
Roger Wahba ◽  
Christoph Bangard ◽  
Klaus Prenzel ◽  
Arnulf H. Hölscher ◽  
...  
Keyword(s):  
Liver Resection ◽  
Morphological Characteristics ◽  
Postoperative Mortality ◽  
Coagulation Necrosis ◽  
Time Interval ◽  
Safe Alternative ◽  
Time Points ◽  
Single Center Experience ◽  
Long Time

Background. Radiofrequency (RF-) assisted liver resection devices like the Habib sealer induce a necrotic resection plane from which a small margin of necrotic liver tissue remains in situ. The aim of the present paper was to report our long-time experience with the new resection method and the morphological characteristics of the remaining necrotic resection plane. Methods. 64 RF-assisted liver resections were performed using the Habib sealer. Followup was assessed at defined time points. Results. The postoperative mortality was 3,6% and morbidity was 18%. The followup revealed that the necrotic zone was detectable in all analyzed CT and MRI images as a hypodense structure without any contrast enhancement at all time points, irrespectively of the time interval between resection and examination. Conclusion. Liver resection utilizing radiofrequency-induced resection plane coagulation is a safe alternative to the established resection techniques. The residual zone of coagulation necrosis remains basically unchanged during a followup of three years. This has to be kept in mind when evaluating the follow up imaging of these patients.

scholarly journals A new method to detect apoptosis in paraffin sections: in situ end-labeling of fragmented DNA.

1993 ◽  
Vol 41 (1) ◽  
pp. 7-12 ◽  
Author(s):  
J H Wijsman ◽  
R R Jonker ◽  
R Keijzer ◽  
C J van de Velde ◽  
C J Cornelisse ◽  
...  
Keyword(s):  
Cell Death ◽  
Programmed Cell Death ◽  
Staining Method ◽  
Morphological Characteristics ◽  
Image Cytometry ◽  
Apoptotic Cells ◽  
Dna Breaks ◽  
Paraffin Sections ◽  
Tissue Sections

Apoptosis (programmed cell death) can be difficult to detect in routine histological sections. Since extensive DNA fragmentation is an important characteristic of this process, visualization of DNA breaks could greatly facilitate the identification of apoptotic cells. We describe a new staining method for formalin-fixed, paraffin-embedded tissue sections that involves an in situ end-labeling (ISEL) procedure. After protease treatment to permeate the tissue sections, biotinylated nucleotides are in situ incorporated into DNA breaks by polymerase and subsequently stained with DAB via peroxidase-conjugated avidin. Staining of cells with the morphological characteristics of apoptosis was demonstrated in tissues known to exhibit programmed cell death, i.e., prostate and uterus after castration, tumors, lymph node follicles, and embryos. Apoptotic cells could be discriminated morphologically from areas of labeled necrotic cells, in which DNA degradation also occurs. Because apoptosis is relatively easily recognized in H&E-stained sections of involuting prostates of castrated rats, we used this model system to validate the ISEL method for the quantification of apoptotic cells. A high correlation was found between the fractions of ISEL-labeled cells and the fractions of apoptotic cells that were morphologically determined in adjacent sections. We conclude that ISEL is a useful technique for quantification of apoptosis in paraffin sections, especially for those tissues in which morphological determination is difficult. Furthermore, this new staining method enables the use of automated image cytometry for evaluating apoptosis.

scholarly journals In Situ SEM Observation of Structured Si/C Anodes Reactions in an Ionic-Liquid-Based Lithium-Ion Battery

2019 ◽  
Vol 9 (5) ◽  
pp. 956 ◽  
Author(s):  
Huifeng Shi ◽  
Xianqiang Liu ◽  
Rui Wu ◽  
Yijing Zheng ◽  
Yonghe Li ◽  
...  
Keyword(s):  
Morphological Evolution ◽  
Structural Evolution ◽  
Lithium Ion ◽  
Composite Electrodes ◽  
Charge Capacity ◽  
Shed Light ◽  
3D Electrode ◽  
Large Charge ◽  
Scanning Electron

In situ scanning electron microscopy (SEM) offers a good way to investigate the structural evolution during lithiation and delithiation processes. In this paper, the dynamical morphological evolution of 3D-line-structured/unstructured Si/C composite electrodes was observed by in situ SEM. The investigation revealed the microstructural origin of large charge capacity for 3D-line-structured anodes. Based on this proposed mechanism, a coarse optimization of 3D-line-structured anodes was proposed. These results shed light on the unique advantages of using an in situ SEM technique when studying realistic bulk batteries and designing 3D electrode structures.

A Ni3N–Co3N hybrid nanowire array electrode for high-performance nonenzymatic glucose detection

2018 ◽  
Vol 10 (15) ◽  
pp. 1680-1684 ◽  
Author(s):  
Xinglu Dai ◽  
Wenqing Deng ◽  
Chao You ◽  
Zhen Shen ◽  
Xiaoli Xiong ◽  
...  
Keyword(s):  
High Performance ◽  
Active Catalyst ◽  
Nanowire Array ◽  
Alkaline Media ◽  
Nickel Cobalt ◽  
Array Electrode ◽  
New Type ◽  
Glucose Electrooxidation ◽  
Catalyst Electrode

In this communication, we report a new type of nickel cobalt nitride hybrid nanowire array in situ grown on a Ti plate (Ni3N–Co3N NW/Ti) topotactically converted from Ni–Co hydroxide as a high-active catalyst electrode for glucose electrooxidation in alkaline media.

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