scholarly journals SPERT I DESTRUCTIVE TEST PROGRAM SAFETY ANALYSIS REPORT

1962 ◽  
Author(s):  
A.H. Spano ◽  
R.W. Miller
Keyword(s):  
Safety Analysis ◽  
Test Program ◽  
Destructive Test ◽  
Program Safety

The Didanosine Expanded Access Program: Safety Analysis

1993 ◽  
Vol 16 (Supplement_1) ◽  
pp. S63-S68 ◽  
Author(s):  
Isadore M. Pike ◽  
Claude Nicaise
Keyword(s):  
Safety Analysis ◽  
Expanded Access ◽  
Expanded Access Program ◽  
Access Program ◽  
Program Safety

Precision and bias in quantitative EDS: ASTM results

1992 ◽  
Vol 50 (2) ◽  
pp. 1654-1655
Author(s):  
John J. Friel
Keyword(s):  
Stainless Steel ◽  
Quantitative Analysis ◽  
Mechanical Alloy ◽  
Dead Time ◽  
Test Program ◽  
Round Robin Test ◽  
Wide Range ◽  
American Society ◽  
Takeoff Angle ◽  
Standardless Analysis

Committee E-04 on Metallography of the American Society for Testing and Materials (ASTM) conducted an interlaboratory round robin test program on quantitative energy dispersive spectroscopy (EDS). The test program was designed to produce data on which to base a precision and bias statement for quantitative analysis by EDS. Nine laboratories were sent specimens of two well characterized materials, a type 308 stainless steel, and a complex mechanical alloy from Inco Alloys International, Inconel® MA 6000. The stainless steel was chosen as an example of a straightforward analysis with no special problems. The mechanical alloy was selected because elements were present in a wide range of concentrations; K, L, and M lines were involved; and Ta was severely overlapped with W. The test aimed to establish limits of precision that could be routinely achieved by capable laboratories operating under real world conditions. The participants were first allowed to use their own best procedures, but later were instructed to repeat the analysis using specified conditions: 20 kV accelerating voltage, 200s live time, ∼25% dead time and ∼40° takeoff angle. They were also asked to run a standardless analysis.

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