scholarly journals In-Situ Neutron Diffraction Studies of Complex Hydrogen Storage Materials

2013 ◽  
Author(s):  
William B. Yelon
Keyword(s):  
Neutron Diffraction ◽  
Hydrogen Storage ◽  
Hydrogen Storage Materials ◽  
Storage Materials ◽  
In Situ Neutron Diffraction

scholarly journals Desorption reaction in MgH2 studied with in situ μ+SR

2019 ◽  
Vol 3 (4) ◽  
pp. 956-964 ◽  
Author(s):  
Jun Sugiyama ◽  
Izumi Umegaki ◽  
Mitsuru Matsumoto ◽  
Kazutoshi Miwa ◽  
Hiroshi Nozaki ◽  
...  
Keyword(s):  
Hydrogen Storage ◽  
Muon Spin ◽  
Spin Rotation ◽  
Sample Space ◽  
Muon Spin Rotation ◽  
Hydrogen Storage Materials ◽  
Storage Materials ◽  
Desorption Temperature ◽  
Desorption Reaction

To study the mechanism determining the desorption temperature of hydrogen storage materials, we have measured muon spin rotation and relaxation (μ+SR) in MgH2 together with the pressure in the sample space.

Performance of Cu-coated vanadium cans forin situneutron powder diffraction experiments on hydrogen storage materials

2012 ◽  
Vol 45 (5) ◽  
pp. 902-905 ◽  
Author(s):  
Roxana Flacau ◽  
Jim Bolduc ◽  
Thomas Bibienne ◽  
Jacques Huot ◽  
Helmut Fritzsche
Keyword(s):  
Hydrogen Storage ◽  
High Temperatures ◽  
Powder Diffraction ◽  
Neutron Powder Diffraction ◽  
Simple Design ◽  
Hydrogen Storage Materials ◽  
High Quality ◽  
Handling System ◽  
Storage Materials

In situneutron powder diffraction (NPD) measurements of hydrogenation processes taking place at high temperatures pose difficulties related to the choice of sample can material. This article describes a simple design for a copper-coated vanadium can and its connection to the gas-handling system, tested up to 523 K. High-quality NPD patterns of TiV1.2Mn0.8body-centred cubic alloy, as-cast and partially hydrogenated, were collected at 373 K and deuterium pressures up to 2 bar (200 kPa).

Metallic Ni nanocatalyst in situ formed from a metal–organic-framework by mechanochemical reaction for hydrogen storage in magnesium

2015 ◽  
Vol 3 (16) ◽  
pp. 8294-8299 ◽  
Author(s):  
Yi Jia ◽  
Chenghua Sun ◽  
Ye Peng ◽  
Wenqi Fang ◽  
Xuecheng Yan ◽  
...  
Keyword(s):  
Hydrogen Storage ◽  
Metal Organic Framework ◽  
Mechanochemical Reaction ◽  
Hydrogen Storage Materials ◽  
Storage Materials ◽  
Metal Organic ◽  
Kinetics Of ◽  
Organic Framework

The facile and scalable fabrication of ultrafine (<5 nm) nanoparticles (NPs) as effective catalysts is the key for enhancing the kinetics of most hydrogen storage materials (HSMs).

scholarly journals In-situ TEM Observation with Environmental Cell for Hydrogen Storage Materials

Materia Japan ◽  
2009 ◽  
Vol 48 (12) ◽  
pp. 616-616
Author(s):  
Shigehito Isobe ◽  
Yongming Wang ◽  
Koya Okudera ◽  
Hiroko Hirasawa ◽  
Naoyuki Hashimoto ◽  
...  
Keyword(s):  
Hydrogen Storage ◽  
In Situ Tem ◽  
Hydrogen Storage Materials ◽  
Storage Materials ◽  
Environmental Cell

In situ measurement technologies on solid-state hydrogen storage materials: a review

2020 ◽  
Vol 17 ◽  
pp. 100463 ◽  
Author(s):  
Huai-Jun Lin ◽  
Hai-Wen Li ◽  
Huaiyu Shao ◽  
Yanshan Lu ◽  
Kohta Asano
Keyword(s):  
Solid State ◽  
Hydrogen Storage ◽  
In Situ Measurement ◽  
Hydrogen Storage Materials ◽  
Storage Materials

scholarly journals In-situ hydrogen gas loading setup for synchrotron X-ray total scattering

2014 ◽  
Vol 70 (a1) ◽  
pp. C868-C868
Author(s):  
Hyunjeong Kim ◽  
Kouji Sakaki ◽  
Kohta Asano ◽  
Miho Yamauchi ◽  
Akihiko Machida ◽  
...  
Keyword(s):  
Hydrogen Storage ◽  
Structural Features ◽  
Hydrogen Gas ◽  
Hydrogen Storage Materials ◽  
Energy Agency ◽  
Promising Alternative ◽  
Total Scattering ◽  
X Ray ◽  
Storage Materials

Hydrogen has been considered as a promising alternative fuel for transportation, provided we can find a way to store a large amount of hydrogen in a compact way. The realization of such a storage system can be achieved by developing materials that can easily absorb, safely store, and rapidly release hydrogen repeatedly. However, there is currently no material to meet all the requirements for on board storage. Great efforts have been made to understand hydrogenation properties of currently available materials to look for a way to improve properties or to prepare new materials. However, investigating the structure of some of these materials is challenging since their hydrides are only available under hydrogen gas pressure. Furthermore, many novel materials with improved properties often show heavily disordered or nanoscale structural features which are difficult to characterize using conventional crystallographic technique alone (crystallographically challenged hydrogen storage materials). In order to investigate the structural change in crystallographically challenged hydrogen storage materials during hydrogenation or dehydrogenation processes we have developed in-situ hydrogen gas loading setup for synchrotron X-ray total scattering experiments at the Japan Atomic Energy Agency (JAEA) beamline of BL22XU [1] at SPring-8. Coupled to an area detector [1,2], this setup allows us to obtain the atomic pair distribution function (PDF) [3] of metal hydrides either in equilibrium or in non-equilibrium state with hydrogen. In this poster, we will introduce our in-situ setup and present some preliminary results on AB5-type intermetallic compounds and Pd nanoparticles.

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