scholarly journals Soft x-ray shock loading and momentum coupling in meteorite and planetary materials.

2010 ◽  
Author(s):  
R. Jeffery Lawrence ◽  
John L. Remo ◽  
Michael David Furnish
2012 ◽  
Vol 79 (2) ◽  
pp. 121-141 ◽  
Author(s):  
JOHN L. REMO ◽  
MICHAEL D. FURNISH ◽  
R. JEFFERY LAWRENCE

AbstractX-ray momentum coupling coefficients, CM, were determined by measuring stress waveforms in planetary materials subjected to impulsive radiation loading from the Sandia National Laboratories Z-machine. Velocity interferometry (VISAR) diagnostics provided equation-of-state data. Targets were iron and stone meteorites, magnesium-rich olivine (dunite) solid and powder (~5–300 μm), and Si, Al, and Fe calibration targets. Samples were ~1-mm thick and, except for Si, backed by LiF single-crystal windows. X-ray spectra combined thermal radiation (blackbody 170–237 eV) and line emissions from pinch materials (Cu, Ni, Al, or stainless steel). Target fluences of 0.4–1.7 kJ/cm2 at intensities of 43–260GW/cm2 produced plasma pressures of 2.6–12.4 GPa. The short (~5 ns) drive pulses gave rise to attenuating stress waves in the samples. The attenuating wave impulse is constant, allowing accurate CM measurements from rear-surface motion. CM was 1.9 − 3.1 × 10−5 s/m for stony meteorites, 2.7 and 0.5 × 10−5 s/m for solid and powdered dunite, 0.8 − 1.4 × 10−5 s/m for iron meteorites, and 0.3, 1.8, and 2.7 × 10−5 s/m respectively for Si, Fe, and Al calibration targets. Results are consistent with geometric scaling from recent laser hohlraum measurements. CTH hydrocode modeling of X-ray coupling to porous silica corroborated experimental measurements and supported extrapolations to other materials. CTH-modeled CM for porous materials was low and consistent with experimental results. Analytic modeling (BBAY) of X-ray radiation-induced momentum coupling to selected materials was also performed, often producing higher CM values than experimental results. Reasons for the higher values include neglect of solid ejecta mechanisms, turbulent mixing of heterogeneous phases, variances in heats of melt/vaporization, sample inhomogeneities, wave interactions at the sample/window boundary, and finite sample/window sizes. The measurements validate application of CM to (inhomogeneous) planetary materials from high-intensity soft X-ray radiation.


Author(s):  
J. M. Galbraith ◽  
L. E. Murr ◽  
A. L. Stevens

Uniaxial compression tests and hydrostatic tests at pressures up to 27 kbars have been performed to determine operating slip systems in single crystal and polycrystal1ine beryllium. A recent study has been made of wave propagation in single crystal beryllium by shock loading to selectively activate various slip systems, and this has been followed by a study of wave propagation and spallation in textured, polycrystal1ine beryllium. An alteration in the X-ray diffraction pattern has been noted after shock loading, but this alteration has not yet been correlated with any structural change occurring during shock loading of polycrystal1ine beryllium.This study is being conducted in an effort to characterize the effects of shock loading on textured, polycrystal1ine beryllium. Samples were fabricated from a billet of Kawecki-Berylco hot pressed HP-10 beryllium.


2021 ◽  
Vol 11 (1) ◽  
Author(s):  
Avanish Mishra ◽  
Cody Kunka ◽  
Marco J. Echeverria ◽  
Rémi Dingreville ◽  
Avinash M. Dongare

AbstractDuring the various stages of shock loading, many transient modes of deformation can activate and deactivate to affect the final state of a material. In order to fundamentally understand and optimize a shock response, researchers seek the ability to probe these modes in real-time and measure the microstructural evolutions with nanoscale resolution. Neither post-mortem analysis on recovered samples nor continuum-based methods during shock testing meet both requirements. High-speed diffraction offers a solution, but the interpretation of diffractograms suffers numerous debates and uncertainties. By atomistically simulating the shock, X-ray diffraction, and electron diffraction of three representative BCC and FCC metallic systems, we systematically isolated the characteristic fingerprints of salient deformation modes, such as dislocation slip (stacking faults), deformation twinning, and phase transformation as observed in experimental diffractograms. This study demonstrates how to use simulated diffractograms to connect the contributions from concurrent deformation modes to the evolutions of both 1D line profiles and 2D patterns for diffractograms from single crystals. Harnessing these fingerprints alongside information on local pressures and plasticity contributions facilitate the interpretation of shock experiments with cutting-edge resolution in both space and time.


1992 ◽  
Vol 36 ◽  
pp. 595-601
Author(s):  
P. Newcomer ◽  
B. Morosin ◽  
R. A. Graham

AbstractX-ray diffraction line-profile analysis on tetragonal forms of SnO2 (cassiterite), MnO2 (pyrolusite), and previously studied TiO2 (rutile), which were subjected to high pressure shock loading, show that residual lattice strain and coherent “crystal” size are a function of shock parameters. An interesting observation on a sample of MnO2 concerns the recovery of cubic Mn2O3 (bixbyite) in the material subjected to 22 GPa, indicating a shock-induced chemical synthesis.


1983 ◽  
Vol 24 ◽  
Author(s):  
B. Morosin ◽  
R. A. Graham

ABSTRACTPowders of AlN, TiC and TiB2 have been subjected to controlled shock loading with peak pressures in the samples between 14 to 27 GPa and preserved for post-shock study. Broadened x-ray diffraction peak profiles are analyzed by a simplified method and show increases in residual lattice strain and small decreases in crystallite size. Strain values range from 10−5 to 10−4 for TiB2 and to values larger than 10−3 for TiC and AlN.


Author(s):  
Camille Chauvin ◽  
Frédéric Zucchini ◽  
David Palma de Barros

Abstract We propose to study experimentally the polymorphic transition of Tin under dynamic compression. These transformations have been investigated for a long time through usual velocity measurements under shock from ambient condition. At CEA Gramat we have improved our understanding of such phase transformations through both experimental and theoretical means. Experimental velocity measurements have long suggested that non equilibrium behavior and kinetics is an important part of the dynamic compression response of materials undergoing phase transformations. Empirical kinetic models can in many cases reproduce the experimental velocity profiles, but without clearly identifying the nature of the transition. For nearly two decades, the CEA Gramat operates several gas guns for shock loading and high pulsed power (HPP) drivers dedicated to Isentropic Compression Experiments (ICE) up to several GPa. These experimental devices and associated diagnostics (velocimetry and temperature measurements and x-ray diffraction experiments) help to begin to study kinetics under dynamic transition in a more rigorous manner. We have used these experiments to examine various compression paths and have used the results to improve equation of state (EOS) models incorporated in our numerical codes. The latter can be used to run simulations starting with ambient initial conditions, then load metallic materials from various non ambient initial temperatures. This can significantly extend the range of our studies into previously unexplored thermodynamic paths. We propose to describe our preheating devices for gas gun experiments and our HPP driver, and to present our preliminary results on shock loading and on isentropic compression at various initial temperatures, to explore the phase diagram of Tin. In addition, we present the design of promising testing on X-ray diffraction under shock to help to develop a more physical kinetic model relying on nucleation and growth mechanisms, which are implemented in our continuum level codes.


Author(s):  
L.M. LEE ◽  
D.E. JOHNSON ◽  
F. BAUER ◽  
R.P. REED ◽  
J.I. GREENWOLL

1983 ◽  
Vol 27 ◽  
pp. 369-378
Author(s):  
B. Morosin ◽  
E. J. Graeber ◽  
R. A. Graham

Enhanced solid state reactivity of materials both during and after shock compression has been attributed to the introduction of large numbers of defects into the crystalline lattices and to reduction in the particle and crystallite size of powders [1,2]. Line broadening of x-ray diffraction profiles provides a means to determine the residual lattice strain resulting from such defect concentrations as well as a means to determine the coherent crystallite size. Various diffraction studies on shock-loaded powder materials have previously been reported and much of this work primarily by Soviet and Japanese scientists has recently been reviewed [2]. Cohen has reported results on shock-loaded copper [3]. In prior work, however, shock, pressures have not typically been quantified and there are few detailed line broadening investigations of refractory inorganic powders [1,4,5]. The present study on shock-loaded alumina powders is a detailed investigation of the influence of shock loading on residual lattice strain and coherent crystallite size.


2016 ◽  
Vol 129 ◽  
pp. 384-388 ◽  
Author(s):  
J.L. Remo ◽  
R.J. Lawrence ◽  
S.B. Jacobsen ◽  
M.D. Furnish

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