scholarly journals FINAL REPORT: DOE CONTRACT NUMBER FG0205ER64026 Biological Neutron Scattering: A Collaboration with the Oak Ridge Center for Structural Molecular Biology

2011 ◽  
Author(s):  
Jill Trewhella
Science ◽  
1978 ◽  
Vol 199 (4329) ◽  
pp. 673-673 ◽  
Author(s):  
A. L. ROBINSON
Keyword(s):  

2018 ◽  
Vol 51 (2) ◽  
pp. 242-248 ◽  
Author(s):  
William T. Heller ◽  
Matthew Cuneo ◽  
Lisa Debeer-Schmitt ◽  
Changwoo Do ◽  
Lilin He ◽  
...  

Oak Ridge National Laboratory is home to the High Flux Isotope Reactor (HFIR), a high-flux research reactor, and the Spallation Neutron Source (SNS), the world's most intense source of pulsed neutron beams. The unique co-localization of these two sources provided an opportunity to develop a suite of complementary small-angle neutron scattering instruments for studies of large-scale structures: the GP-SANS and Bio-SANS instruments at the HFIR and the EQ-SANS and TOF-USANS instruments at the SNS. This article provides an overview of the capabilities of the suite of instruments, with specific emphasis on how they complement each other. A description of the plans for future developments including greater integration of the suite into a single point of entry for neutron scattering studies of large-scale structures is also provided.


2011 ◽  
Vol 1334 ◽  
Author(s):  
Dipendu Saha ◽  
Lilin He ◽  
Cristian I. Contescu ◽  
Nidia C. Gallego ◽  
Yuri B. Melnichenko

ABSTRACTEntrapping hydrogen molecules within the nanopores of solid adsorbents serves as a unique alternative for on-board storing of hydrogen for transportation purposes. The key advantage of the physisorption process for hydrogen storage is the higher density values achieved with the adsorbed gas, compared to that of the compressed phase, translating into higher storage capacities at lower pressures. The necessary condition for effective adsorption is the presence of narrow micropores of < 2 nm in width which provide the most suitable environment of hydrogen adsorption. Despite numerous theoretical calculations or indirect experimental estimations, there has not been a direct experimental measurement of the density of adsorbed hydrogen as a function of pressure and/or pore size. In the present study, we report on the use of in-situ small angle neutron scattering (SANS) to study the phase behavior of hydrogen confined in narrow micropores. We provide for the first time direct experimental measurements of the effect of pore size and pressure on hydrogen adsorbed on a polyfurfuryl alcohol-derived activated carbon (PFAC), at room temperature and pressures up to 207 bar. SANS studies were carried out at the General-Purpose Small-Angle Neutron Scattering spectrometer of the High Flux Isotope Reactor at Oak Ridge National Laboratory. The measurements covered the Q-range from 0.01 to 0.8 Å-1, covering the pores in the range of 9 to 34 Å of the PFAC material. Initial results suggest that the density of adsorbed hydrogen is higher than the density of bulk hydrogen gas and increases with decreasing pore size.


MRS Bulletin ◽  
1999 ◽  
Vol 24 (12) ◽  
pp. 34-39 ◽  
Author(s):  
Peter Lindner ◽  
George Wignall

Neutron scattering had its origin in 1932, the year that marked the discovery of the neutron by Chadwick, and the first nuclear reactors were successfully operated in Chicago and Oak Ridge, Tenn., in the early 1940s. During its initial stages, neutron scattering was used mainly for the study of “hard” crystalline materials. For example, Shull and Wollan's pioneering research, which led to the 1994 Nobel Prize in physics, began with studies of iron, chromium, and iridium, and was followed by the development of polarization analysis to determine the structure of magnetic materials. Such studies continue to yield important structural information (see the articles on magnetism by Aeppli and Hayden and on crystallography by Radaelli and Jorgensen in this issue of MRS Bulletin), although during the last two decades, the technique has been increasingly used by scientists from other disciplines (chemistry, biology, polymer science), and many of these newer applications have involved “soft” matter such as polymers, colloids, and gels. By definition, these substances are “plastic” or “squishy,” and easy to mold into different shapes; because of this flexibility, they have become some of the most practical and widely used materials today.


Neutron News ◽  
2008 ◽  
Vol 19 (2) ◽  
pp. 22-23 ◽  
Author(s):  
William T. Heller ◽  
Gary W. Lynn ◽  
Volker S. Urban ◽  
Kevin Weiss ◽  
Dean A.A. Myles

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