ATOMIC FORCE MICROSCOPIC AND ELECTROCHEMICAL CHARACTERIZATION OF THE MODIFIED SCREEN PRINTED CARBON ELECTRODE BY SELF ASSEMBLED DEPOSITION OF CHITOSAN AND ACTIVATED CARBON

2016 ◽  
Author(s):  
Porntip Wongkaew
Keyword(s):  
Activated Carbon ◽  
Electrochemical Characterization ◽  
Carbon Electrode ◽  
Atomic Force ◽  
Screen Printed Carbon Electrode ◽  
Self Assembled ◽  
Screen Printed

Application of Gold Nanoparticles with 1,6-Hexanedithiol Modified Screen-Printed Carbon Electrode as a Sensor for Determination of Arsenic in Environmental Samples

2019 ◽  
Vol 17 (10) ◽  
pp. 762-768
Author(s):  
A. M. Etorki ◽  
Labib A. Awin ◽  
M. El-Rais ◽  
M. S. Elhabbat ◽  
I. S. Shaban
Keyword(s):  
Gold Nanoparticles ◽  
Self Assembled Monolayers ◽  
Carbon Electrode ◽  
Total Arsenic ◽  
Au Nps ◽  
Screen Printed Carbon Electrode ◽  
Anodic Stripping ◽  
Assembled Monolayers ◽  
Self Assembled ◽  
Screen Printed

We have described the development of electrochemical nano sensor for the detection of total arsenic in groundwater, soil, food and honey samples based on the formation of gold nanoparticles. Screen printed carbon electrodes were modified with gold nanoparticles and linked with 1,6-hexanedithiol self-assembled monolayers. The electrodeposition of Au nanoparticles was applied in 10 mL of the solution that totally cover the screen-printed carbon electrode while applying a constant potential of –0.4 V (vs. Ag within SPCE) for 600 sec. Cyclic voltammetry was used to characterize the gold nanoparticles before and after modified with 1,6-hexanedithiol self-assembled monolayers on screen printed carbon electrode. Square wave anodic stripping voltammetry with multi point standard addition method was examined for the detection of As(III) and As(V) on Au NPs-1,6-hexanedithiol modified screen printed carbon electrode under optimized conditions. As(III) and As(V) was firstly, deposited for 60 seconds by the reduction of arsenic in buffer solution: (citric acid, sodium chloride and ascorbic acid pH 2.0), followed by As stripping between –0.20 and 0.35 V at the following parameters: scan rate: 100 mV s–1, frequency: 60 Hz, amplitude: 0.025 V and increment: 5.0 mV. it was found that Au-NPs with 1,6-hexanedithiol modified screen-printed carbon electrode had a highest anodic stripping peak current at 0.201 V. The limit of detection value for arsenic was identified to be 1.7 ng ml –1. Also, the electrochemical nanosensor showed excellent reproducibility and high stability. The developed method was successfully applied to detect total arsenic in ground water, soil and honey samples.

Biological Multilayer Films Assembled by Redox Polymer and HRP on Screen-Printed Carbon Electrode

2012 ◽  
Vol 571 ◽  
pp. 56-59
Author(s):  
Yu Fang Sha ◽  
Mei Zhao ◽  
Ming Quan Yang ◽  
Hai Xin Bai ◽  
Man Zhao
Keyword(s):  
Horseradish Peroxidase ◽  
Electrostatic Interaction ◽  
Electrode Surface ◽  
Multilayer Films ◽  
Carbon Electrode ◽  
Layer By Layer ◽  
Redox Polymer ◽  
Screen Printed Carbon Electrode ◽  
Positively Charged ◽  
Screen Printed

Biological multilayer films of redox polymer and horseradish peroxidase (HRP) were successfully assembled on a screen-printed carbon electrode using layer-by-layer (LBL) assembled method based on the electrostatic interaction. The screen-printed carbon electrode surface was modified by the positively charged redox polymer, and the negatively charged HRP by LBL method.

Screen-printed carbon electrode for the electrochemical detection of conjugated bilirubin

2021 ◽  
pp. 130574
Author(s):  
P.E. Resmi ◽  
Jeethu Raveendran ◽  
P.V. Suneesh ◽  
T. Ramanchandran ◽  
Bipin G Nair ◽  
...  
Keyword(s):  
Electrochemical Detection ◽  
Carbon Electrode ◽  
Screen Printed Carbon Electrode ◽  
Conjugated Bilirubin ◽  
Screen Printed
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