scholarly journals Synthesis and Crystal Structure Refinement of Sb2Se3-xSx Solid Solutions by Rietveld Analysis of X-Ray Powder Diffraction Data

2009 ◽  
Vol 32 (1) ◽  
pp. 71-80
Keyword(s):  
Crystal Structure ◽  
Powder Diffraction ◽  
Solid Solutions ◽  
Diffraction Data ◽  
Structure Refinement ◽  
Rietveld Analysis ◽  
Crystal Structure Refinement ◽  
Powder Diffraction Data ◽  
Synthesis And Crystal Structure ◽  
X Ray

Crystal-structure refinement of τ3-Cr4(Al, Si)11 by full-profile Rietveld analysis

2007 ◽  
Vol 22 (3) ◽  
pp. 253-255 ◽  
Author(s):  
Franz Weitzer ◽  
Hailin Chen ◽  
Julius C. Schuster
Keyword(s):  
Crystal Structure ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Ternary Phase ◽  
Structure Refinement ◽  
Rietveld Analysis ◽  
Crystal Structure Refinement ◽  
Powder Diffraction Data ◽  
Full Profile

Crystal structure of the triclinic ternary phase Cr4(Al, Si)11 was investigated by full-profile Rietveld analysis of powder diffraction data. Four hundred eighty-four reflections were refined to a final RBragg value of 5.00%. Cr4(Al, Si)11 is isostructural to Mn4Al11. Silicon atoms enter into the structure by partially replacing aluminium on the Al(1) and Al(2) sites.

scholarly journals RbCa2Nb3O10from X-ray powder data

2009 ◽  
Vol 65 (6) ◽  
pp. i44-i44 ◽  
Author(s):  
Zhen-Hua Liang ◽  
Kai-Bin Tang ◽  
Qian-Wang Chen ◽  
Hua-Gui Zheng
Keyword(s):  
Crystal Structure ◽  
Solid State ◽  
Powder Diffraction ◽  
Diffraction Data ◽  
Solid State Reaction ◽  
Perovskite Structure ◽  
Three Dimensional ◽  
Rietveld Analysis ◽  
Powder Diffraction Data ◽  
X Ray

Rubidium dicalcium triniobate(V), RbCa2Nb3O10, has been synthesized by solid-state reaction and its crystal structure refined from X-ray powder diffraction data using Rietveld analysis. The compound is a three-layer perovskite Dion–Jacobson phase with the perovskite-like slabs derived by termination of the three-dimensional CaNbO3perovskite structure along theabplane. The rubidium ions (4/mmmsymmetry) are located in the interstitial space.

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