Laser Powder Bed Fusion Produced Ti-6Al-4V: Influence of High-Energy Process Parameters on In-Situ Martensite Decomposition, Stress Relief and Prior Beta Grain Texture

2021 ◽  
Author(s):  
Gerrit Matthys Ter Haar ◽  
Thorsten Hermann Becker
Keyword(s):  
Process Parameters ◽  
Stress Relief ◽  
High Energy ◽  
Grain Texture ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Energy Process ◽  
High Energy Process

scholarly journals In situ microstructure analysis of Inconel 625 during laser powder bed fusion

2021 ◽  
Author(s):  
Felix Schmeiser ◽  
Erwin Krohmer ◽  
Christian Wagner ◽  
Norbert Schell ◽  
Eckart Uhlmann ◽  
...  
Keyword(s):  
Laser Power ◽  
Scanning Speed ◽  
High Energy ◽  
Mechanical Anisotropy ◽  
Ex Situ ◽  
Inconel 625 ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

AbstractLaser powder bed fusion is an additive manufacturing process that employs highly focused laser radiation for selective melting of a metal powder bed. This process entails a complex heat flow and thermal management that results in characteristic, often highly textured microstructures, which lead to mechanical anisotropy. In this study, high-energy X-ray diffraction experiments were carried out to illuminate the formation and evolution of microstructural features during LPBF. The nickel-base alloy Inconel 625 was used for in situ experiments using a custom LPBF system designed for these investigations. The diffraction patterns yielded results regarding texture, lattice defects, recrystallization, and chemical segregation. A combination of high laser power and scanning speed results in a strong preferred crystallographic orientation, while low laser power and scanning speed showed no clear texture. The observation of a constant gauge volume revealed solid-state texture changes without remelting. They were related to in situ recrystallization processes caused by the repeated laser scanning. After recrystallization, the formation and growth of segregations were deduced from an increasing diffraction peak asymmetry and confirmed by ex situ scanning transmission electron microscopy. Graphical Abstract

scholarly journals Laser Powder-Bed Fusion as an Alloy Development Tool: Parameter Selection for In-Situ Alloying Using Elemental Powders

Materials ◽  
2020 ◽  
Vol 13 (18) ◽  
pp. 3922
Author(s):  
Leonardo Shoji Aota ◽  
Priyanshu Bajaj ◽  
Hugo Ricardo Zschommler Sandim ◽  
Eric Aimé Jägle
Keyword(s):  
Process Parameters ◽  
Research Field ◽  
Beam Diameter ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Alloy Development ◽  
Chemical Homogeneity ◽  
Powder Mixtures ◽  
Powder Bed

The design of advanced alloys specifically tailored to additive manufacturing processes is a research field that is attracting ever-increasing attention. Laser powder-bed fusion (LPBF) commonly uses pre-alloyed, fine powders (diameter usually 15–45 µm) to produce fully dense metallic parts. The availability of such fine, pre-alloyed powders reduces the iteration speed of alloy development for LPBF and renders it quite costly. Here, we overcome these drawbacks by performing in-situ alloying in LPBF starting with pure elemental powder mixtures avoiding the use of costly pre-alloyed powders. Pure iron, chromium, and nickel powder mixtures were used to perform in-situ alloying to manufacture 304 L stainless steel cube-shaped samples. Process parameters including scanning speed, laser power, beam diameter, and layer thickness were varied aiming at obtaining a chemically homogeneous alloy. The scientific questions focused on in this work are: which process parameters are required for producing such samples (in part already known in the state of the art), and why are these parameters conducive to homogeneity? Analytical modelling of the melt pool geometry and temperature field suggests that the residence time in the liquid state is the most important parameter controlling the chemical homogeneity of the parts. Results show that in-situ alloying can be successfully employed to enable faster and cost-efficient rapid alloy development.

scholarly journals A laser powder bed fusion system for in situ x-ray diffraction with high-energy synchrotron radiation

2020 ◽  
Vol 91 (7) ◽  
pp. 075104
Author(s):  
Eckart Uhlmann ◽  
Erwin Krohmer ◽  
Felix Schmeiser ◽  
Norbert Schell ◽  
Walter Reimers
Keyword(s):  
Synchrotron Radiation ◽  
High Energy ◽  
Fusion System ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
X Ray Diffraction ◽  
Powder Bed ◽  
X Ray

scholarly journals On the Relevance of Volumetric Energy Density in the Investigation of Inconel 718 Laser Powder Bed Fusion

Materials ◽  
2020 ◽  
Vol 13 (3) ◽  
pp. 538 ◽  
Author(s):  
Fabrizia Caiazzo ◽  
Vittorio Alfieri ◽  
Giuseppe Casalino
Keyword(s):  
Surface Roughness ◽  
Energy Density ◽  
Process Parameters ◽  
Vickers Hardness ◽  
Powder Bed Fusion ◽  
Processing Conditions ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Fractional Density ◽  
Experimental Variation

Laser powder bed fusion (LPBF) can fabricate products with tailored mechanical and surface properties. In fact, surface texture, roughness, pore size, the resulting fractional density, and microhardness highly depend on the processing conditions, which are very difficult to deal with. Therefore, this paper aims at investigating the relevance of the volumetric energy density (VED) that is a concise index of some governing factors with a potential operational use. This paper proves the fact that the observed experimental variation in the surface roughness, number and size of pores, the fractional density, and Vickers hardness can be explained in terms of VED that can help the investigator in dealing with several process parameters at once.

scholarly journals Comparison of Phase Characteristics and Residual Stresses in Ti-6Al-4V Alloy Manufactured by Laser Powder Bed Fusion (L-PBF) and Electron Beam Powder Bed Fusion (EB-PBF) Techniques

Crystals ◽  
2021 ◽  
Vol 11 (7) ◽  
pp. 796
Author(s):  
Aya Takase ◽  
Takuya Ishimoto ◽  
Naotaka Morita ◽  
Naoko Ikeo ◽  
Takayoshi Nakano
Keyword(s):  
Electron Beam ◽  
Residual Stresses ◽  
Cooling Rate ◽  
Process Parameters ◽  
Phase Evolution ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Solidification Temperature ◽  
Powder Bed ◽  
Β Phase

Ti-6Al-4V alloy fabricated by laser powder bed fusion (L-PBF) and electron beam powder bed fusion (EB-PBF) techniques have been studied for applications ranging from medicine to aviation. The fabrication technique is often selected based on the part size and fabrication speed, while less attention is paid to the differences in the physicochemical properties. Especially, the relationship between the evolution of α, α’, and β phases in as-grown parts and the fabrication techniques is unclear. This work systematically and quantitatively investigates how L-PBF and EB-PBF and their process parameters affect the phase evolution of Ti-6Al-4V and residual stresses in the final parts. This is the first report demonstrating the correlations among measured parameters, indicating the lattice strain reduces, and c/a increases, shifting from an α’ to α+β or α structure as the crystallite size of the α or α’ phase increases. The experimental results combined with heat-transfer simulation indicate the cooling rate near the β transus temperature dictates the resulting phase characteristics, whereas the residual stress depends on the cooling rate immediately below the solidification temperature. This study provides new insights into the previously unknown differences in the α, α’, and β phase evolution between L-PBF and EB-PBF and their process parameters.

scholarly journals Role of laser powder bed fusion process parameters in crystallographic texture of additive manufactured Nb-48Ti alloy

2021 ◽  
Author(s):  
Rafael de Moura Nobre ◽  
Willy Ank de Morais ◽  
Matheus Tavares Vasques ◽  
Jhoan Guzmán ◽  
Daniel Luiz Rodrigues Junior ◽  
...  
Keyword(s):  
Process Parameters ◽  
Crystallographic Texture ◽  
Fusion Process ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed

scholarly journals Optimizing Laser Powder Bed Fusion Parameters for IN-738LC by Response Surface Method

Materials ◽  
2020 ◽  
Vol 13 (21) ◽  
pp. 4879
Author(s):  
Mireia Vilanova ◽  
Rubén Escribano-García ◽  
Teresa Guraya ◽  
Maria San Sebastian
Keyword(s):  
Response Surface ◽  
Response Surface Method ◽  
Process Parameters ◽  
Crack Density ◽  
Processing Parameters ◽  
Optimum Process ◽  
Powder Bed Fusion ◽  
Laser Powder Bed Fusion ◽  
Powder Bed ◽  
Surface Method

A method to find the optimum process parameters for manufacturing nickel-based superalloy Inconel 738LC by laser powder bed fusion (LPBF) technology is presented. This material is known to form cracks during its processing by LPBF technology; thus, process parameters have to be optimized to get a high quality product. In this work, the objective of the optimization was to obtain samples with fewer pores and cracks. A design of experiments (DoE) technique was implemented to define the reduced set of samples. Each sample was manufactured by LPBF with a specific combination of laser power, laser scan speed, hatch distance and scan strategy parameters. Using the porosity and crack density results obtained from the DoE samples, quadratic models were fitted, which allowed identifying the optimal working point by applying the response surface method (RSM). Finally, five samples with the predicted optimal processing parameters were fabricated. The examination of these samples showed that it was possible to manufacture IN738LC samples free of cracks and with a porosity percentage below 0.1%. Therefore, it was demonstrated that RSM is suitable for obtaining optimum process parameters for IN738LC alloy manufacturing by LPBF technology.

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