Crystal structure of the high-pressure phase of calcium hydroxide, portlandite: In situ powder and single-crystal X-ray diffraction study

2013 ◽  
Vol 98 (8-9) ◽  
pp. 1421-1428 ◽  
Author(s):  
R. Iizuka ◽  
T. Yagi ◽  
K. Komatsu ◽  
H. Gotou ◽  
T. Tsuchiya ◽  
...  
2017 ◽  
Vol 102 (3) ◽  
pp. 666-673 ◽  
Author(s):  
Anna Pakhomova ◽  
Leyla Ismailova ◽  
Elena Bykova ◽  
Maxim Bykov ◽  
Tiziana Boffa Ballaran ◽  
...  

2019 ◽  
Vol 36 (4) ◽  
pp. 046103 ◽  
Author(s):  
Sheng Jiang ◽  
Jing Liu ◽  
Xiao-Dong Li ◽  
Yan-Chun Li ◽  
Shang-Ming He ◽  
...  

2007 ◽  
Vol 52 (4) ◽  
pp. 195-199 ◽  
Author(s):  
S. K. Filatov ◽  
N. A. Bendeliani ◽  
B. Albert ◽  
J. Kopf ◽  
T. I. Dyuzheva ◽  
...  

2019 ◽  
Vol 75 (12) ◽  
pp. 1605-1612 ◽  
Author(s):  
Keishiro Yamashita ◽  
Kazuki Komatsu ◽  
Takanori Hattori ◽  
Shinichi Machida ◽  
Hiroyuki Kagi

A high-pressure phase of magnesium chloride hexahydrate (MgCl2·6H2O-II) and its deuterated counterpart (MgCl2·6D2O-II) have been identified for the first time by in-situ single-crystal X-ray and powder neutron diffraction. The crystal structure was analyzed by the Rietveld method for the neutron diffraction pattern based on the initial structure determined by single-crystal X-ray diffraction. This high-pressure phase has a similar framework to that in the known ambient-pressure phase, but exhibits some structural changes with symmetry reduction caused by a subtle modification in the hydrogen-bond network around the Mg(H2O)6 octahedra. These structural features reflect the strain in the high-pressure phases of MgCl2 hydrates.


2019 ◽  
Vol 274 ◽  
pp. 171-175 ◽  
Author(s):  
Davide Comboni ◽  
Paolo Lotti ◽  
G. Diego Gatta ◽  
Maria Lacalamita ◽  
Ernesto Mesto ◽  
...  

Author(s):  
Gary C. Vezzoli

AbstractA body-centered orthorhombic structure is proposed for the high-pressure phase of tellurium which has been observed between 40 kbar and 70 kbar. This structure is based on the in situ data of others using high-pressure x-ray diffraction. The proposed structure is in agreement with density data, and appears related to a distorted


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