Whole Core Analysis - Experience and Challenges

2005 ◽  
Vol 8 (06) ◽  
pp. 460-469 ◽  
Author(s):  
Mehdi M. Honarpour ◽  
Nizar F. Djabbarah ◽  
Krishnaswamy Sampath

Summary Whole-core analysis is critical for characterizing directional permeability in heterogeneous, fractured, and/or anisotropic rocks. Whole-core measurements are essential for heterogeneous reservoirs because small-scale heterogeneity may not be appropriately represented in plug measurements. For characterization of multiphase-flow properties (special core analysis) in heterogeneous rocks, whole-core analysis is also required. Few commercial laboratories are equipped to conduct routine measurements on whole cores up to 4 in. in diameter and up to 8 in. long and, importantly, under simulated reservoir net confining stress (NCS). Special whole-core analyses are rarely conducted because of the difficulties associated with establishing a representative water saturation in drainage capillary pressure experiments and measuring directional effective permeabilities. Electrical properties also can be measured on whole cores to determine porosity and saturation exponents for situations in which resistivity tools are used in horizontal or highly deviated wells. In this paper, we provide an overview of routine and special core-analysis measurements on whole cores. Results from selected heterogeneous sandstone and carbonate rocks will be discussed. We also will show how the results relate to data obtained from plug analysis, with particular emphasis on directional absolute permeability, trapped-gas and fluid saturations, and the effect of NCS. Finally, we will describe a novel apparatus for special core analysis on whole cores and provide examples of the capabilities of the system. In this paper, we will present:• Recommended techniques for the determination of directional absolute and effective permeability and for establishing initial water saturation in whole cores.• Improved understanding of the effect of scale (sample size) on the measured properties.• Description of a novel whole-core apparatus with measurement of fluid-saturation distribution using in-situ saturation monitoring. Introduction Reservoir rocks are heterogeneous, especially carbonate rocks, in which more than 50% of the world's hydrocarbon reserves are deposited. Fig. 1 shows an example of variability in rock characteristics as observed in a carbonate-rockout crop in Oman. The heterogeneous nature of these rocks tends to become more apparent as attempts are made to measure their petrophyscal properties at various scales. An example of permeability variation in a plug from a carbonate formation is shown in Fig. 2. Single-phase air permeability varies by three orders of magnitude over the distance of a few centimeters in this core plug. This dual-porosity behavior impacts the spontaneous-imbibition performance significantly (Fig. 3). Technology at Commercial Laboratories Selected commercial laboratories have capabilities to appropriately clean and prepare whole cores, perform core X-ray imaging, and measure basic properties such as directional permeability and porosity under a maximum confining stress of 5,000 psi. Available technologies for imaging, sample preparation, and routine core analysis are summarized in the following sections. Special-core-analysis capabilities at commercial laboratories are rare. Only one or two laboratories are capable of measuring primary-drainage gas/water capillary pressure and gas/water or oil/water electrical properties on whole cores at confining stress. Whole-Core Imaging and Screening Whole-core photography and X-ray imaging provide information about surface features and internal structure. The computed tomography (CT) scan provides evidence of fractures, vugs, and heterogeneities as indicated by the extent in the variation of CT density. X-ray fluoroscopy and CT are two of the most practical X-ray scanning techniques used to characterize core-level heterogenieties and to explain their effect on horizontal and vertical permeabilities. CT-scanning algorithms should often be modified to obtain images free of artifacts and with better than0.5-mm horizontal and 1-mm vertical resolutions.

1998 ◽  
Vol 18 (3) ◽  
pp. 251-255 ◽  
Author(s):  
S. Migeon ◽  
O. Weber ◽  
J. -C. Faugeres ◽  
J. Saint-Paul

2006 ◽  
Vol 9 (06) ◽  
pp. 647-653 ◽  
Author(s):  
Shameem Siddiqui ◽  
Taha M. Okasha ◽  
James J. Funk ◽  
Ahmad M. Al-Harbi

Summary The data generated from special-core-analysis (SCAL) tests have a significant impact on the development of reservoir engineering models. This paper describes some of the criteria and tests required for the selection of representative samples for use in SCAL tests. The proposed technique ensures that high-quality core plugs are chosen to represent appropriate flow compartments or facies within the reservoir. Visual inspection and, sometimes, computerized tomography (CT) images are the main tools used for assessing and selecting the core plugs for SCAL studies. Although it is possible to measure the brine permeability (kb), there is no direct method for determining the porosity (f) of SCAL plugs without compromising their wettability. Other selection methods involve using the conventional-core-analysis data (k and f) on "sister plugs" as a general indicator of the properties of the SCAL samples. A selective technique ideally suited for preserved or "native-state" samples has been developed to identify reservoir intervals with similar porosity/permeability relationships. It uses a combination of wireline log, gamma scan, quantitative CT, and preserved-state brine-permeability data. The technique uses these data to calculate appropriate depth-shifted reservoir-quality index (RQI) and flow-zone indicator (FZI) data, which are then used to select representative plug samples from each reservoir compartment. As an example application, approximately 400 SCAL plugs from an Upper Jurassic carbonate reservoir in the Middle East were tested using the selection criteria. This paper describes the step-by-step procedure to select representative plugs and criteria for combining the plugs for meaningful SCAL tests. Introduction The main goal of coring is to retrieve core samples from a well to get the maximum amount of information about the reservoir. Core samples collected provide important petrophysical, petrographic, paleontological, sedimentological, and diagenetic information. From a petrophysical point of view, the whole-core and plug samples typically undergo the following tests: CT scan, gamma scan, conventional tests, SCAL tests, rock mechanics, and other special tests. The data are combined to get information on heterogeneity, depth shift between core and log data, whole-core and plug porosity and permeability, porosity/permeability relationship, fluid content (Dean-Stark), RQI, FZI, wettability, relative permeability, capillary pressure, stress/strain relationship, and compressibility. The petrophysical data generated in this way play important roles in reservoir characterization and modeling, log calibration, reservoir simulation, and overall field production and development planning. Among all the petrophysical tests, the SCAL tests (which include wettability, capillary pressure, and relative permeability determination) are critical and time-consuming. A reservoir-condition relative permeability test can sometimes run for several months when mimicking the actual flow mechanisms taking place in the field. Therefore, it is very important to design these tests properly and, in particular, to select the samples that ensure meaningful results. In short, the samples must be "representative samples," which can capture the overall variability within the reservoir in a more scientific way. Unfortunately, the most important aspect of all SCAL procedures, the sample selection, is one of those least discussed. According to Corbett et al. (2001), API's RP40 (Recommended Practices for Core Analysis) makes very little reference to sampling; similarly, textbooks on petrophysics do not have sections on sampling. The Corbett et al. paper reviewed the statistical, petrophysical, and geological issues for sampling and proposed a series of considerations. This has led to the development of a method (Mohammed and Corbett 2002) using hydraulic units in a relatively simple clastic reservoir. In this paper, some issues related to sample-selection criteria (with special focus on carbonate reservoirs) will be discussed. A large data set of conventional, whole-core, and special-core analyses on a well in an Upper Jurassic carbonate reservoir was used to characterize representative samples for SCAL tests.


SPE Journal ◽  
2020 ◽  
pp. 1-17
Author(s):  
Artur Posenato Garcia ◽  
Zoya Heidari

Summary Cost-effective exploitation of heterogeneous/anisotropic reservoirs (e.g., carbonate formations) relies on accurate description of pore structure, dynamic petrophysical properties (e.g., directional permeability, saturation-dependent capillary pressure), and fluid distribution. However, techniques for reliable quantification of permeability still rely on model calibration using core measurements. Furthermore, the assessment of saturation-dependent capillary pressure has been limited to experimental measurements, such as mercury injection capillary pressure (MICP). The objectives of this paper include developing a new multiphysics workflow to quantify rock-fabric features (e.g., porosity, tortuosity, and effective throat size) from integrated interpretation of nuclear magnetic resonance (NMR) and electric measurements; introducing rock-physics models that incorporate the quantified rock fabric and partial water/hydrocarbon saturation for assessment of directional permeability and saturation-dependent capillary pressure; and validating the reliability of the new workflow in the core-scale domain. To achieve these objectives, we introduce a new multiphysics workflow integrating NMR and electric measurements, honoring rock fabric, and minimizing calibration efforts. We estimate water saturation from the interpretation of dielectric measurements. Next, we develop a fluid-substitution algorithm to estimate the T2 distribution corresponding to fully water-saturated rocks from the interpretation of NMR measurements. We use the estimated T2 distribution for assessment of porosity, pore-body-size distribution, and effective pore-body size. Then, we develop a new physically meaningful resistivity model and apply it to obtain the constriction factor and, consequently, throat-size distribution from the interpretation of resistivity measurements. We estimate tortuosity from the interpretation of dielectric-permittivity measurements at 960 MHz by applying the concept of capacitive formation factor. Finally, throat-size distribution, porosity, and tortuosity are used to calculate directional permeability and saturation-dependent capillary pressure. We test the reliability of the new multiphysics workflow in the core-scale domain on rock samples at different water-saturation levels. The introduced multiphysics workflow provides accurate description of the pore structure in partially water-saturated formations with complex pore structure. Moreover, this new method enables real-time well-log-based assessment of saturation-dependent capillary pressure and directional permeability (in presence of directional electrical measurements) in reservoir conditions, which was not possible before. Quantification of capillary pressure has been limited to measurements in laboratory conditions, where the differences in stress field reduce the accuracy of the estimates. We verified that the estimates of permeability, saturation-dependent capillary pressure, and throat-size distribution obtained from the application of the new workflow agreed with those experimentally determined from core samples. We selected core samples from four different rock types, namely Edwards Yellow Limestone, Lueders Limestone, Berea Sandstone, and Texas Cream Limestone. Finally, because the new workflow relies on fundamental rock-physics principles, permeability and saturation-dependent capillary pressure can be estimated from well logs with minimum calibration efforts, which is another unique contribution of this work.


SPE Journal ◽  
2010 ◽  
Vol 16 (01) ◽  
pp. 78-94 ◽  
Author(s):  
Timothy J. Kneafsey ◽  
Yongkoo Seol ◽  
Arvind Gupta ◽  
Liviu Tomutsa

Summary Methane hydrate was formed in two moist sands and a sand/silt mixture under a confining stress in an X-ray-transparent pressure vessel. Three initial water saturations were used to form three different methane-hydrate saturations in each medium. X-ray computed tomography (CT) was used to observe location-specific density changes caused by hydrate formation and flowing water. Gas-permeability measurements in each test for the dry, moist, frozen, and hydrate-bearing states are presented. As expected, the effective permeabilities (intrinsic permeability of the medium multiplied by the relative permeability) of the moist sands decreased with increasing moisture content. In a series of tests on a single sample, the effective permeability typically decreased as the pore space became more filled in the order of dry, moist, frozen, and hydrate-bearing. In each test, water was flowed through the hydrate-bearing medium and we observed the location-specific changes in water saturation using CT scanning. We compared our data to a number of models, and our relative permeability data compare most favorably with models in which hydrate occupies the pore bodies rather than the pore throats. Inverse modeling (using the data collected from the tests) will be performed to extend the relative permeability measurements.


Author(s):  
M.G. Baldini ◽  
S. Morinaga ◽  
D. Minasian ◽  
R. Feder ◽  
D. Sayre ◽  
...  

Contact X-ray imaging is presently developing as an important imaging technique in cell biology. Our recent studies on human platelets have demonstrated that the cytoskeleton of these cells contains photondense structures which can preferentially be imaged by soft X-ray imaging. Our present research has dealt with platelet activation, i.e., the complex phenomena which precede platelet appregation and are associated with profound changes in platelet cytoskeleton. Human platelets suspended in plasma were used. Whole cell mounts were fixed and dehydrated, then exposed to a stationary source of soft X-rays as previously described. Developed replicas and respective grids were studied by scanning electron microscopy (SEM).


Author(s):  
James F. Mancuso ◽  
William B. Maxwell ◽  
Russell E. Camp ◽  
Mark H. Ellisman

The imaging requirements for 1000 line CCD camera systems include resolution, sensitivity, and field of view. In electronic camera systems these characteristics are determined primarily by the performance of the electro-optic interface. This component converts the electron image into a light image which is ultimately received by a camera sensor.Light production in the interface occurs when high energy electrons strike a phosphor or scintillator. Resolution is limited by electron scattering and absorption. For a constant resolution, more energy deposition occurs in denser phosphors (Figure 1). In this respect, high density x-ray phosphors such as Gd2O2S are better than ZnS based cathode ray tube phosphors. Scintillating fiber optics can be used instead of a discrete phosphor layer. The resolution of scintillating fiber optics that are used in x-ray imaging exceed 20 1p/mm and can be made very large. An example of a digital TEM image using a scintillating fiber optic plate is shown in Figure 2.


Author(s):  
Ann LeFurgey ◽  
Peter Ingram ◽  
J.J. Blum ◽  
M.C. Carney ◽  
L.A. Hawkey ◽  
...  

Subcellular compartments commonly identified and analyzed by high resolution electron probe x-ray microanalysis (EPXMA) include mitochondria, cytoplasm and endoplasmic or sarcoplasmic reticulum. These organelles and cell regions are of primary importance in regulation of cell ionic homeostasis. Correlative structural-functional studies, based on the static probe method of EPXMA combined with biochemical and electrophysiological techniques, have focused on the role of these organelles, for example, in maintaining cell calcium homeostasis or in control of excitation-contraction coupling. New methods of real time quantitative x-ray imaging permit simultaneous examination of multiple cell compartments, especially those areas for which both membrane transport properties and element content are less well defined, e.g. nuclei including euchromatin and heterochromatin, lysosomes, mucous granules, storage vacuoles, microvilli. Investigations currently in progress have examined the role of Zn-containing polyphosphate vacuoles in the metabolism of Leishmania major, the distribution of Na, K, S and other elements during anoxia in kidney cell nuclel and lysosomes; the content and distribution of S and Ca in mucous granules of cystic fibrosis (CF) nasal epithelia; the uptake of cationic probes by mltochondria in cultured heart ceils; and the junctional sarcoplasmic retlculum (JSR) in frog skeletal muscle.


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