A Centrifuge Method To Predict Matrix-Block Recovery in Fractured Reservoirs

1970 ◽  
Vol 10 (02) ◽  
pp. 164-170 ◽  
Author(s):  
J.R. Kyte

Abstract Previous laboratory investigations to predict recovery from matrix blocks in a fractured reservoir have been primarily concerned with the imbibition oil recovery process. Gravity segregation can sometimes be more important than imbibition as a mechanism for oil recovery from matrix blocks. This paper describes a new method to predict oil recovery behavior for matrix blocks in a fractured-matrix reservoir. Centrifuge tests are performed with preserved reservoir core samples to scale the effects of both gravity and capillarity. The tests are easy to perform. Yet, The results should be more reliable than results obtained by other available methods for predicting matrix-block recoveries. Centrifuge tests were performed on different-sized reservoir rock samples to confirm the scaling theory. These tests were performed to simulate a water-oil displacement in a weakly water-wet reservoir. The method is equally applicable to other reservoir wettabilities and gas-oil displacements. In the weakly water-wet system, oil recovered by imbibition was found to be almost negligible as compared with the amount of oil recovered by gravity segregation. Introduction In many fractured-matrix reservoirs, most of the oil is contained in matrix blocks that are surrounded by a high-permeability fracture system. The flowing pressure gradient in the fractures is small, and pressure gradient in the fractures is small, and local capillary and gravity forces will dominate the recovery process for each matrix block. The unit matrix-block behavior then becomes an important factor in predicting reservoir oil recovery and assessing secondary or tertiary recovery prospects. Other investigators have used synthetic models and reservoir core samples to study the imbibition oil recovery process in fractured-matrix reservoirs. The methods they used to predict matrix-block recoveries are applicable when the reservoir rock is strongly wet by water and imbibition is the dominant mechanism for oil recovery. Wettability studies show that some reservoir rocks are not strongly wet by water in the presence of crude oil so that imbibition oil recovery will be low. Under these circumstances, gravity segregation can be an important mechanism for oil recovery, and its influence should be included in predicting matrix-block recovery. Marx has previously used scaling principles to show that the gas-oil gravity drainage characteristics of long, linear columns can be predicted from centrifuge tests on reconstituted core samples. In the current work, application of the scaling theory is extended to include three-dimensional systems and water-oil displacements. In addition, procedures are suggested to either duplicate or scale reservoir wettability and interfacial tension. The objectives of the present work are to present a centrifuge method that can be used to predict the effects of both gravity and capillarity on matrix-block oil recovery and to demonstrate the importance of gravity in recovering oil from matrix blocks in fractured reservoirs. In this paper, discussion of the centrifuge method will be limited, for the most part, to water-oil displacements. Application of the method to gas-oil displacements is discussed briefly near the end of the paper. PROCEDURE FOR PREDICTING PROCEDURE FOR PREDICTING MATRIX-BLOCK RECOVERY The laboratory procedure developed for predicting matric-block recovery consists of the predicting matric-block recovery consists of the following.Select a preserved core believed to have the same wettability, porosity and permeability as the prototype reservoir matrix block. prototype reservoir matrix block. A preserved core is defined as one cut and stored under conditions designed to preserve the original reservoir wettability.Cut a sample (or model) from the core so that it will simulate the reservoir matrix-block geometry in the centrifuge tests. SPEJ P. 164

1962 ◽  
Vol 2 (02) ◽  
pp. 177-184 ◽  
Author(s):  
C.C. Mattax ◽  
J.R. Kyte

Abstract Previous workers have developed differential equations to describe oil displacement by water imbibition, but have not explicitly defined the relationship between recovery behavior for a single reservoir matrix block and its size. In the present work, imbibition theory is extended to show that the time required to recover a given fraction of the oil from a matrix block is proportional to the square of the distance between fractures. Using this relationship, recovery behavior for a large reservoir matrix block is predicted from an imbibition test on a small reservoir core sample. The prediction is then extended to analyze recovery behavior for fractured - matrix, water - drive reservoirs in which imbibition is the dominant oil-producing mechanism. Experimental data are presented to support the basic imbibition theory relating matrix block size, fluid viscosity level and permeability to recovery behavior. Introduction Imbibition has long been recognized as an important factor in recovering oil from water - wet, fractured-matrix reservoirs subjected to water flood or water drive. Recently, two approaches have been published which might be used to predict imbibition oil-recovery behavior for reservoir - sized matrix blocks. Graham and Richardson used a synthetic model to scale a single element of a fractured-matrix reservoir. Blair, on the other hand, used numerical techniques to solve the differential equations describing imbibition in linear and radial systems. This latter method requires auxiliary experimental data in the form of capillary pressure and relative permeability functions. These two approaches, i.e., synthetic models and numerical techniques, have been used to study a variety of reservoir fluid-flow problems. One purpose of this work is to present, with experimental verification, a third method for predicting imbibition oil recovery for large reservoir matrix blocks. This method uses scaled imbibition tests on small reservoir core samples to predict field performance. The imbibition tests are easier to perform than the capillary pressure and relative permeability tests required to apply the numerical method. Furthermore, when suitably preserved reservoir-rock samples are used, the properties of the laboratory system are the same as those of the field. This offers an important advantage over the use of synthetic models because there is usually some question as to how accurately reservoir-rock properties can be duplicated in such models. Based on the recovery behavior for a unit matrix block, an analysis is presented to predict oil recovery for a fractured, water-drive reservoir made up of many such unit blocks. In the analysis, it is assumed that the flow resistance and the volume of the reservoir fracture system are negligible compared with that of the porous matrix. These assumptions are generally consistent with observed characteristics of many fractured-matrix reservoirs, and have been employed in previous studies. It is further assumed that the effect of gravity on flow in the matrix blocks is negligible. On first thought, the latter assumption might appear to seriously limit application of the method. However, in a fractured reservoir, the effect of gravity on flow in a matrix block will be restricted by the height of the block. Furthermore, matrix permeabilities are often very low (10 md or less) in such reservoirs. This means that capillary or imbibition forces will be large, thus tending to minimize the relative importance of gravity. For these reasons, imbibition should be the dominant oil-recovery mechanism in many fractured-matrix, water-drive reservoirs. The predictive method presented in this report is applicable to such reservoirs. SPEJ P. 177^


2021 ◽  
Author(s):  
Tinuola Udoh

Abstract In this paper, the enhanced oil recovery potential of the application of nanoparticles in Niger Delta water-wet reservoir rock was investigated. Core flooding experiments were conducted on the sandstone core samples at 25 °C with the applications of nanoparticles in secondary and tertiary injection modes. The oil production during flooding was used to evaluate the enhanced oil recovery potential of the nanoparticles in the reservoir rock. The results of the study showed that the application of nanoparticles in tertiary mode after the secondary formation brine flooding increased oil production by 16.19% OIIP. Also, a comparison between the oil recoveries from secondary formation brine and nanoparticles flooding showed that higher oil recovery of 81% OIIP was made with secondary nanoparticles flooding against 57% OIIP made with formation brine flooding. Finally, better oil recovery of 7.67% OIIP was achieved with secondary application of nanoparticles relative to the tertiary application of formation brine and nanoparticles flooding. The results of this study are significant for the design of the application of nanoparticles in Niger Delta reservoirs.


2017 ◽  
Vol 35 (2) ◽  
pp. 237-258 ◽  
Author(s):  
Xiaoyu Wang ◽  
Xiaolin Wang ◽  
Wenxuan Hu ◽  
Ye Wan ◽  
Jian Cao ◽  
...  

Studying the interactions between CO2-rich fluid and reservoir rock under reservoir temperature and pressure is important for investigating CO2 sequestration and the CO2-enhanced oil recovery processes. Using high-concentration CaCl2-type formation water as an example, this study performed a CO2-rich fluid–rock interaction experiment at 85℃ and compared the dissolution of calcite and sandstone samples, as well as sandstone powder and thin-slice samples. This study also investigated the effects of the sample surface area, the CO2 partial pressure ( PCO2 = 10 and 20 MPa), and the composition of formation water (3 mol/kg NaCl and 1 mol/kg CaCl2–2 mol/kg NaCl) on the water–rock interaction mechanism and process by weighing, ion chromatography, and scanning electron microscopy observations. The results showed that the injection of CO2 resulted in the dissolution of reservoir minerals such as carbonate cements and feldspar. The mineral dissolution increased with increasing PCO2. The dissolution of minerals such as calcite in the CaCl2-type formation water was significantly decreased because of the high concentration of Ca2+. Under the same conditions, more sandstone dissolved than calcite and more sandstone powder dissolved than sandstone thin slices. Dissolution of the potassium feldspar occurred in the sandstone, whereas the albite was nearly unaffected. No new minerals formed during the experimental process. The experimental results and a PHREEQC calculation demonstrated that the injection of CO2 causes a significant pH drop in the formation water, which improves the porosity and permeability of the reservoir, increases the capacity of the reservoir to store CO2, and facilitates the progression of the CO2-enhanced oil recovery process. However, if alkaline minerals in the caprocks of the reservoir are also dissolved by the CO2-rich fluid, the sealing capacity of the caprocks may be reduced.


2017 ◽  
Vol 5 (10) ◽  
pp. 114-123
Author(s):  
Hazim H. Al-Attar ◽  
Essa Lwisa

In this work the mathematical model developed by Aronovsky et. al. for predicting rates of free-water imbibition in naturally fractured oil reservoirs has been modified. The proposed model allows prediction of fractional oil recovery by spontaneous water imbibition in core samples with high accuracy. The proposed modification involves development of an empirical correlation for the reservoir rock/fluid system-dependent parameter (l) used in Aronofsky model and defined as rate of convergence. The key reservoir rock and fluid physical properties considered in this work include absolute permeability of the rock, porosity, initial water saturation, interfacial tension between oil and water (IFT), viscosity of oil, viscosity of water, and length of core sample. The accuracy of the modified model is evaluated using the results of laboratory imbibition tests on nine limestone core samples. All imbibition tests were conducted at 90 ° C. The absolute per cent error based on laboratory versus calculated values of (l) is found to range between 0.334 and 3.88. The proposed model may also be applied for predicting fractured reservoir performance on field scale by simply replacing the core length by matrix block length when the block is totally immersed in water. Additional experimental work and/or field observations would be necessary to verify the reliability of the proposed modification.


1971 ◽  
Vol 11 (02) ◽  
pp. 113-128 ◽  
Author(s):  
Roy H. Yamamoto ◽  
J.B. Padgett ◽  
Wayne T. Ford ◽  
Ahmed Boubeguira

Abstract A mathematical model is presented for the simulation of pressure, production and saturation behavior of a single block within a fissured system. The matrix block is represented by a tow-dimensional grid system with two-phase (oil and gas) flow through porous media defined by differential and algebraic relations and solved by quasi-implicit methods. The fissure is represented by a single mode opposite the mid-depth of the block and serves to define the boundary conditions around the block. The hydrocarbon system in simulated compositionally in terms of three equivalent components (methane, ethane through hexanes, and heptanes plus). Variable physical properties, drainage and imbibition capillary pressures, pore compressibility, and gravity are included in the formulation. The effects of mass transfer between hydrocarbon phases and of changing composition upon the phases and of changing composition upon the saturation and pressure distribution are considered through the use of known phase behavior concepts and correlations. This method provides a means of evaluating the effects of oil-vapor capillarity, solution gas drive, gravity drainage, fissure-matrix counterflow, effects of phase composition both in the fissures and in the matrix, and the pressure and fissure gas-oil level decline rates upon the pressure-production behavior of a matrix block in a fissured reservoir. The results of the simulation of pressure depletion and pressure maintenance processes obtained for blocks of various sizes reveal significant differences in performance under different environmental conditions in the fissures. Introduction Conventional methods used in the analysis of nonfractures reservoirs leave much to be desired in the proper evaluation of displacement mechanisms within naturally fractured reservoirs. In these reservoirs the fissure system provides paths of rapid pressure and fluid communication with the producing wells, and also offers very large surface producing wells, and also offers very large surface areas of the matrix rock for any pressure change to impinge upon. Basic to the evaluation and understanding of the displacement mechanisms in this type of reservoir is the simulation of performance within the matrix blocks for various performance within the matrix blocks for various environmental conditions that could exist in the adjacent fissures. Birks studied matrix block behavior for gas-oil and oil-water systems without solution drive. Aronofsky et al. studied recovery mechanisms in an oil-water system. Freeman and Natanson studied the highly fractured Kirkuk reservoir of Iraq with an abstract mathematical model. Andresen et al, described a mathematical model that judiciously applied well established physical principles to the evaluation and prediction of principles to the evaluation and prediction of performance of the fractured Asmari reservoirs of performance of the fractured Asmari reservoirs of Iran. These investigators and others have shed much light into behavior of fractured formations and fissure flow. It is the purpose of this paper to describe a new method which permits the simulation of block behavior under fissure environments that vary both in time and space for a two-phase (gas-oil) system. It does not, however, simulate flow through the reservoir fissure system. The mathematical model that is presented allows a more detailed evaluation of the physical processes that take place at the boundaries and interior of the blocks and thus affords a better understanding of the displacement efficiencies that result from various modes of reservoir operation. SPEJ p. 113


2013 ◽  
Vol 26 ◽  
pp. 9-16 ◽  
Author(s):  
Pouriya Esmaeilzadeh ◽  
Zahra Fakhroueian ◽  
Mohammad Nadafpour ◽  
Alireza Bahramian

ZnO nanosphericals and nanorods have interesting potential applications in various fields such as antibacterial and enhanced oil recovery process. In this work, it was shown that 30 ml of a water-based solution containing 3% of ZnO nanofluids could significantly change the wettability of a carbonate reservoir rock from a strongly oil-wet alter to a strongly water-wet condition, after 3 days aging of the rock at 70°C in the designed solution. Moreover, we have studied air-water and oil-water interfacial tensions of system containing nanofluids. Fluids included ZnO nanoparticles and quantum dots nanostructures (QDOTs ZnO) could effectively decrease the n-decane/water interfacial tension and air/water surface tension. So their efficiency is much higher in comparison with distilled water.The stabilization of various aqueous ZnO nanostructured in mixtures of NaCl, CaCl2, MgCl2and Na2SO4salts were investigated, and 50000-163000 ppm transparent and stable nanosalt fluids were fabricated. Wettability of an oil-wet carbonate rock aged for 3 days at 70°C in the designed ZnO nanosalt fluids was studied by measuring the contact angles. The results show a strong change in wettability of carbonate rocks from oil-wet to more water-wet condition. These nanosalt fluids performed an excellent trend of surface tension and IFT reduction in comparison with distilled water too.


2014 ◽  
Vol 2 (4) ◽  
pp. 432-436 ◽  
Author(s):  
Kalpajit Hazarika ◽  
Subrata Borgohain Gogoi

This paper reports the effect of using black liquor whose main constituent is Na- lignosulfonate, which is the effluent from Nagaon paper Mill, Jagiroad, Assam, along with Alkali and Co-surfactant in enhanced crude oil recovery from Upper Assam porous media. In this paper an attempt has been done to study the change in Inter Facial Tension (IFT) with different concentration of Surfactant and also a comparative study has been done determine the change in IFT with or without Alkali and Co-Surfactant. Increasing the surfactant concentration reduces the IFT, hence increases the recovery efficiency. Alkali changes the Wettability of reservoir rock and reduces the surfactant adsorption and also act as an in-situ surfactant production.DOI: http://dx.doi.org/10.3126/ijasbt.v2i4.11047 Int J Appl Sci Biotechnol, Vol. 2(4): 432-436 


1980 ◽  
Vol 20 (03) ◽  
pp. 139-150 ◽  
Author(s):  
J. Hagoort

Abstract Recent observations have indicated surprisingly high oil recoveries for gravity drainage. This has prompted us to reexamine gravity drainage as an prompted us to reexamine gravity drainage as an oil-recovery process. It is shown that oil relative pumeability is a key factor. For accurate measurement pumeability is a key factor. For accurate measurement of this oil relative permeability, we have developed a new method based on centrifugal gas/oil displacement in small cores. Several oil relative permeabilities for various rock types are presented. permeabilities for various rock types are presented. These relative permeabilities confirm that gravity drainage in water-wet, connate-water-bearing reservoirs can be very effective for oil-recovery. Introduction Gravity drainage is a recovery process in which gravity acts as the main driving force and where gas replaces the voidage volume. In other words, it is a gas/oil displacement in which gravity forces are dominating. It may occur in primary stages of oil production (gas-cap expansion drive or segregation production (gas-cap expansion drive or segregation drive), as well as in supplemental stages where gas is supplied from an external source.Two recent studies have indicated surprisingly high oil recoveries for gravity drainage. During their capillary-pressure studies, Dumore and Schols discovered that residual oil saturation after gas invasion in highly permeable sandstone cores containing connate water can be extremely low (5%). They also found low residual oil saturations in sandpack gravity-drainage experiments.A field study by King and Stiles concerns the East Texas Hawkins reservoir, in which a very high displacement efficiency for gravity drainage was reported (87%).These findings prompted us to reexamine the gravity-drainage process. Using the classical description of immiscible two-phase flow applied to a one-dimensional vertical gravity-drainage system, we easily can pinpoint the key factors of the process. One of the most important quantities appears to be the oil relative permeability. For quick and accurate measurement of the oil relative permeability, we present a new technique based on centrifugal gas/oil present a new technique based on centrifugal gas/oil displacement.The results of this study enable us to evaluate gravity drainage better. Using the results of the simple one-dimensional description, we can make quick first judgements of the process. Further, the new measuring technique provides basic input data for more comprehensive mathematical simulation studies. Vertical Displacement Efficiency of Gravity Drainage Classical Description We can think of gravity drainage as a displacement process in which gas displaces oil. Then, by using the process in which gas displaces oil. Then, by using the concepts of relative permeability and capillary pressure, together with the continuity equation and pressure, together with the continuity equation and Darcy's law, the displacement can be described mathematically. For the simple case of a stable, vertical, downward displacement of oil by gas (Fig. 1), we end up with a single equation:(1) where fo is the oil fractional flow function as defined in Appendix A.To gain more insight into the effect of the various parameters, we put Eq. 1 in dimensionless form. parameters, we put Eq. 1 in dimensionless form. Therefore, we introduce the reduced oil saturation and reduced porosity: SPEJ P. 139


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