New Single-Phase Retarded Acid System Boosts Production after Acid Fracturing in Kazakhstan

2018 ◽  
Author(s):  
Dmitriy Abdrazakov ◽  
Mohan Kanaka Raju Panga ◽  
Christopher Daeffler ◽  
Duman Tulebayev
Keyword(s):  
Single Phase ◽  
Acid System ◽  
Acid Fracturing

scholarly journals Pre-acid system for improving the hydraulic fracturing effect in low-permeability tight gas reservoir

2021 ◽  
Vol 11 (4) ◽  
pp. 1761-1780
Author(s):  
Nianyin Li ◽  
Fei Chen ◽  
Jiajie Yu ◽  
Peihong Han ◽  
Jia Kang
Keyword(s):  
Hydraulic Fracturing ◽  
Filter Cake ◽  
Low Permeability ◽  
Tight Gas ◽  
Acid System ◽  
Fracturing Fluid ◽  
Gas Reservoirs ◽  
Tight Gas Reservoirs ◽  
Acid Fracturing ◽  
Performance Requirements

AbstractHydraulic fracturing is an important technical means to improve the development effect of low-permeability oil and gas reservoirs. However, for low pressure, low-permeability, tight, and high-clay sandstone gas reservoirs, conventional propped fracturing can cause serious damage to the reservoir and restrict the fracturing effect. The pre-acid fracturing technology combines acid treatment technology with sand-fracturing technology. A pre-acid system that meets special performance requirements is injected before fracturing. The pre-acid reduces the formation fracture pressure and removes clay damage. During acid flowback, the fracturing fluid is promoted to break the gel, dissolve the fracturing fluid residue and polymer filter cake, clean the supporting cracks, and effectively improve the fracturing effect. This study analyzes the process principle and technical advantages of the pre-acid fracturing technology based on the laboratory evaluation of the fracturing damage mechanism of low-permeability tight gas reservoirs. To meet the performance requirements of low-permeability tight gas reservoirs and pre-acid fracturing technology, a set of polyhydrogen acid system with long-lasting slow reactivity, low damage, and low corrosion was developed and used as the pre-fracturing acid. The acid system is mainly composed of the main agent SA601 and the auxiliary agent SA701. Then, on the basis of laboratory experiments, this acid system is used as the fracturing pre-acid to evaluate the fracturing improvement effect. The results show that the fracturing fluid system can better dissolve the fracturing fluid filter cake and remove the fracturing fluid damage.

scholarly journals Research and Evaluation of a New Autogenic Acid System Suitable for Acid Fracturing of a High-Temperature Reservoir

ACS Omega ◽  
2020 ◽  
Vol 5 (33) ◽  
pp. 20734-20738
Author(s):  
Yang Wang ◽  
Changlin Zhou ◽  
Xiangyi Yi ◽  
Li Li ◽  
Jun Zhou ◽  
...  
Keyword(s):  
High Temperature ◽  
Acid System ◽  
Acid Fracturing

Optimization of Acid Fracturing Design in Yubei Fractured Reservoir

2014 ◽  
Vol 580-583 ◽  
pp. 2495-2501 ◽  
Author(s):  
Li Yang Song ◽  
Xiao Ru He ◽  
Ji Cheng Zhang
Keyword(s):  
Numerical Simulation ◽  
Horizontal Wells ◽  
Simulation Method ◽  
Injection Rate ◽  
Acid System ◽  
Fractured Reservoir ◽  
Fracture Conductivity ◽  
Acid Fracturing ◽  
Numerical Simulation Method ◽  
Half Length

This paper recommends the application of acidic fracturing technology for horizontal wells in Yubei region basing on its fractured reservoir’s characteristics, and the numerical simulation method is used to optimize the parameters of acidic fracturing. According to the results of optimization, the proper acid system is selected, and the construction parameters of acidic fracturing are optimized. According to the results of numerical simulation, we recommend the fracture half-length to be 120m, the fracture conductivity to be 30D.cm, and the fracture number to be 5. According to the properties of reservoir in Yubei region and the optimization results of fracture half-length and fracture conductivity, the alternative injection of crosslinked acid and ordinary gelled acid is recommend. The injection rate of crosslinked acid is 5m3/min, with volume 300m3. The injection rate of ordinary gelled acid is 6m3/min, with volume 300m3.

Advanced Fracturing Design Simulator-Assisted Modeling Coupled with Application of Enhanced Stimulation Fluids Raises Performance of Acid Fractured Wells

2021 ◽  
Author(s):  
Ruslan Kalabayev ◽  
Dmitriy Abdrazakov ◽  
Yeltay Juldugulov ◽  
Vladimir Stepanov ◽  
Denis Emelyanov ◽  
...  
Keyword(s):  
Single Phase ◽  
Viscous Fingering ◽  
Low Ph ◽  
Transport Processes ◽  
Carbonate Reservoirs ◽  
Productivity Index ◽  
Fracture Geometry ◽  
Acid Fracturing ◽  
Fracture Simulation ◽  
Half Length

Abstract Important factors affecting acid fracturing efficiency include etched fracture geometry, cleanup, and optimum differential etching to retain open channels after fracture closure. A recently applied integrated approach combined improvements in all three factors: new fracture simulation techniques enabled fracture geometry optimization, single-phase retarded acid provided significant increase in half-length, and high retained permeability viscous fluids supported better fracture cleanup. The approach was successfully implemented in several carbonate oil fields and resulted in a substantial productivity index increase. The approach enables acid fracture optimization in three steps. First, the high retained permeability, low-pH pad fluids and polymer-free leakoff control acids are used in combination to enhance formation cleanup after a treatment and to reduce the concentration of polymers in fissures network of naturally fractured carbonate reservoirs. Second, a new single-phase retarded acid is used to achieve longer half-length due to retarded reaction with formation rock and favorable viscous fingering effects. Third, a new acid fracturing simulation model is used to optimize fracture geometry. The simulation technique employs an innovative transport model that includes the viscous fingering effect, advanced leakoff simulation, changing acid rheology upon spending, and a novel calculation approach to mixed fluids' rheology. This combined concept was applied during acid fracturing treatments in moderate permeability wells of carbonate reservoirs with target intervals up to 4,600 m TVD and temperatures up to 125°C. The treatments consisted of guar-free low-pH pad fluid, polymer-free leakoff control acid, and single-phase retarded acid. Treatment optimization was performed using an advanced acid fracturing simulator to properly address the transport processes within the fracture in a low-stress-contrast environment. After the treatments, the pressure transient analysis indicated a strong linear regime for more than 15 hours, indicating effective fracture half-length at least 25% higher than average half-length after acid fracturing in offset wells where the conventional approach had been applied. Post-treatment half-length calculations showed a good match with advanced simulator results and proved the importance of accounting for viscous fingering effects during acid fracture half-length calculations. Calculation of the productivity index from the production data showed at least 15% increase compared to conventional acid fracturing treatments. The post-fracturing production decline rate was at least 20% slower than that of the conventional treatment in offset wells, which can be explained by the longer conductive fracture.

Single Phase Retarded Acid System with Degradable Fibers Unlocks Production Potential in Tuba Formation, North Kuwait

2019 ◽  
Author(s):  
Badriya Al-Enezi ◽  
Peiwu Liu ◽  
Hai Liu ◽  
Kousic Theja Kanneganti ◽  
Samir Aloun ◽  
...  
Keyword(s):  
Single Phase ◽  
Acid System ◽  
Production Potential

Influence of Heat Treatments on Microstructures in an Fe-Co-V Alloy

1974 ◽  
Vol 32 ◽  
pp. 512-513
Author(s):  
S. Mahajan ◽  
M. R. Pinnel ◽  
J. E. Bennett
Keyword(s):  
Single Phase ◽  
Alloy Composition ◽  
Supersaturated Solid Solution ◽  
Cell Formation ◽  
Heat Treatments ◽  
Air Cooling ◽  
Iced Brine ◽  
Transmission Electron ◽  
The Matrix ◽  
Bcc Structure

The microstructural changes in an Fe-Co-V alloy (composition by wt.%: 2.97 V, 48.70 Co, 47.34 Fe and balance impurities, such as C, P and Ni) resulting from different heat treatments have been evaluated by optical metallography and transmission electron microscopy. Results indicate that, on air cooling or quenching into iced-brine from the high temperature single phase ϒ (fcc) field, vanadium can be retained in a supersaturated solid solution (α2) which has bcc structure. For the range of cooling rates employed, a portion of the material appears to undergo the γ-α2 transformation massively and the remainder martensitically. Figure 1 shows dislocation topology in a region that may have transformed martensitically. Dislocations are homogeneously distributed throughout the matrix, and there is no evidence for cell formation. The majority of the dislocations project along the projections of <111> vectors onto the (111) plane, implying that they are predominantly of screw character.

Raman And Fluorescence Spectra Observed in Laser Microprobe Measurements of Several Compositions in the Ln-Ba-Cu-O System

1990 ◽  
Vol 48 (2) ◽  
pp. 278-279
Author(s):  
Edgar S. Etz ◽  
Thomas D. Schroeder ◽  
Winnie Wong-Ng
Keyword(s):  
Fluorescence Spectra ◽  
Single Phase ◽  
X Ray Diffraction ◽  
Ceramic Powders ◽  
Conventional Solid State Reaction ◽  
X Ray ◽  
Raman Microprobe ◽  
Methods Of Synthesis ◽  
Compositional Homogeneity ◽  
Processing Techniques

We are investigating by Raman microprobe measurements the superconducting and related phases in the LnBa2Cu3O7-x (for x=0 to 1) system where yttrium has been replaced by several of the lanthanide (Ln = Nd,Sm,Eu,Ho,Er) elements. The aim is to relate the observed optical spectra (Raman and fluorescence) to the compositional and structural properties of these solids as part of comprehensive materials characterization. The results are correlated with the methods of synthesis, the processing techniques of these materials, and their superconducting properties. Of relevance is the substitutional chemistry of these isostructural systems, the differences in the spectra, and their microanalytical usefulness for the detection of impurity phases, and the assessment of compositional homogeneity. The Raman spectra of most of these compounds are well understood from accounts in the literature.The materials examined here are mostly ceramic powders prepared by conventional solid state reaction techniques. The bulk samples are of nominally single-phase composition as determined by x-ray diffraction.

Observation of pseudo 10-fold symmetry in the ordered iron-zinc delta phase

1992 ◽  
Vol 50 (1) ◽  
pp. 36-37
Author(s):  
L. A. Giannuzzi ◽  
A. S. Ramani ◽  
P. R. Howell ◽  
H. W. Pickering ◽  
W. R. Bitler
Keyword(s):  
Single Phase ◽  
X Ray Diffraction ◽  
Rich Region ◽  
Average Cell ◽  
X Ray ◽  
Delta Phase ◽  
Cell Dimensions ◽  
Δ Phase ◽  
Morphological Differences ◽  
Concentration Discontinuity

The δ phase is a Zn-rich intermetallic, having a composition range of ∼ 86.5 - 92.0 atomic percent Zn, and is stable up to 665°C. The stoichiometry of the δ phase has been reported as FeZn7 and FeZn10 The deviation in stoichiometry can be attributed to variations in alloy composition used by each investigator. The structure of the δ phase, as determined by powder x-ray diffraction, is hexagonal (P63mc or P63/mmc) with cell dimensions a = 1.28 nm, c = 5.76 nm, and 555±8 atoms per unit cell. Later work suggested that the layer produced by hot-dip galvanizing should be considered as two distinct phases which are characterized by their morphological differences, namely: the iron-rich region with a compact appearance (δk) and the zinc-rich region with a columnar or palisade microstructure (δp). The sub-division of the δ phase was also based on differences in diffusion behavior, and a concentration discontinuity across the δp/δk boundary. However, work utilizing Weisenberg photographs on δ single crystals reported that the variation in lattice parameters with composition was small and hence, structurally, the δk phase and the δp phase were the same and should be thought of as a single phase, δ. Bastin et al. determined the average cell dimensions to be a = 1.28 nm and c = 5.71 nm, and suggested that perhaps some kind of ordering process, which would not be observed by x-ray diffraction, may be responsible for the morphological differences within the δ phase.

A TEM study of the influence of microstructure on the superplastic behavior of a U-5.8 wt.% Nb alloy

1986 ◽  
Vol 44 ◽  
pp. 568-569
Author(s):  
G. Mackiewicz Ludtka
Keyword(s):  
Grain Size ◽  
Heating Rate ◽  
Phase Field ◽  
Single Phase ◽  
Superplastic Behavior ◽  
Two Phase ◽  
Single Phase Field

Historically, metals exhibit superplasticity only while forming in a two-phase field because a two-phase microstructure helps ensure a fine, stable grain size. In the U-5.8 Nb alloy, superplastici ty exists for up to 2 h in the single phase field (γ1) at 670°C. This is above the equilibrium monotectoid temperature of 647°C. Utilizing dilatometry, the superplastic (SP) U-5.8 Nb alloy requires superheating to 658°C to initiate the α+γ2 → γ1 transformation at a heating rate of 1.5°C/s. Hence, the U-5.8 Nb alloy exhibits an anomolous superplastic behavior.

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