scholarly journals The Relationship between Cyclic Fatigue Properties and Microstructures of Sintered Silicon Nitride Ceramics

1990 ◽  
Vol 98 (1137) ◽  
pp. 490-498 ◽  
Author(s):  
Manabu TAKATSU ◽  
Kanji OHYA ◽  
Masashi ANDO
Keyword(s):  
Silicon Nitride ◽  
Cyclic Fatigue ◽  
Fatigue Properties ◽  
Nitride Ceramics ◽  
The Relationship ◽  
Sintered Silicon

High Temperature Fatigue Properties of Silicon Nitride in Nitrogen Atmosphere

1992 ◽  
Vol 287 ◽  
Author(s):  
Yasuhiro Shigegaki ◽  
Takashi Inamura ◽  
Akihiko Suzuki ◽  
Tadashi Sasa
Keyword(s):  
Silicon Nitride ◽  
Fatigue Behavior ◽  
Cyclic Fatigue ◽  
Nitrogen Atmosphere ◽  
Fatigue Tests ◽  
Fatigue Properties ◽  
Static Fatigue ◽  
Four Point Bending ◽  
Bending Mode ◽  
Sintered Silicon

ABSTRACTCyclic and static fatigue properties of pressure-less sintered silicon nitride were evaluated at 1000° C in air and in nitrogen using four-point bending mode. The data of cyclic fatigue tests or static fatigue tests and the morphology of the fractured surfaces in nitrogen were compared with those in air. The cyclic fatigue behavior was remarkably influenced by the atmosphere, while the static fatigue was less influenced. Crack healing effect due to the oxidation around the crack are thought to be the most probable mechanism to affect the cyclic fatigue rate in air.

Novel Microstructures in Microwave Sintered Silicon Nitride

1996 ◽  
Vol 430 ◽  
Author(s):  
M. E. Brito ◽  
K. Hirao ◽  
M. Toriyama ◽  
M. Hirota
Keyword(s):  
Grain Size ◽  
Silicon Nitride ◽  
Size Distribution ◽  
Grain Size Distribution ◽  
Mechanical Performance ◽  
Microwave Sintering ◽  
Preliminary Results ◽  
Nitride Ceramics ◽  
Positive Effect ◽  
Sintered Silicon

AbstractPreliminary results on microwave sintering of seeded silicon nitride show that a well defined bi-modal grain size distribution is attainable in Si3N4-Y2O3-Al2O 3-MgO sintered bodies by microwave sintering at 28 GHz of materials seeded with ß-Si3N4 particles (2 vol. %). A positive effect on the mechanical performance is anticipated for these microstructurally controlled silicon nitride ceramics

Vacuum Heat Treatment of MgO -Densified Pressureless Sintered Silicon Nitride Ceramics

2007 ◽  
Vol 554 ◽  
pp. 107-112 ◽  
Author(s):  
V. Demir ◽  
Derek P. Thompson
Keyword(s):  
Heat Treatment ◽  
Silicon Nitride ◽  
Pressureless Sintering ◽  
Vacuum Heat Treatment ◽  
Sem Images ◽  
Edx Analysis ◽  
Heat Treated ◽  
Nitride Ceramics ◽  
Different Temperatures ◽  
Sintered Silicon

Silicon nitride samples were pressureless sintered with up to 5 w/o MgO to give densities in the range 98-99% of theoretical. After pressureless sintering, selected samples were placed in a vacuum heat treatment furnace surrounded by a carbon bed in a carbon crucible at a pressure of less than 4x10-4 mbar, and vacuum heat treated at different temperatures and times to remove grainboundary glass. The results showed that this was substantially achieved at 1575oC for 3h and that increasing the time to 5 hours gave still further improvement. SEM images, EDX analysis and oxidation tests provided additional evidence for the removal of Mg from the samples.

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