scholarly journals The Effect of Variation on Solvent Type and Starch Extraction Time on the Increased Level of Reducing Sugar from Jackfruit Straw Waste

2020 ◽  
Vol 13 (1) ◽  
pp. 159-163
Author(s):  
Harimbi Setyawati ◽  
Yepta Octaria ◽  
Enggar Saraswati H ◽  
Erni Yunita

: Jackfruit straw is a part of jackfruit that does not experience pollination in the form of yellow fibers. Jackfruit straw has a composition consisting of 13.45% starch, 65.05% water. The potential content of jackfruit straw starch can be used as an alternative fuel, it was, bioethanol. This material can be converted to bioethanol through hydrolysis and fermentation processes. This study aimed to determine the effect of variations in the type of solvent and extraction time, used the type of solvent H2O, NaOH and NaHCO3 for starch which was then hydrolyzed and produced glucose as a raw material for making bioethanol. The initial content of jackfruit straw was carbohydrate of 11.5%, fat of 16.22% and protein of 8.38%. The first step was drying so that the jackfruit straw became powder with a moisture content <14%. Then extraction with a solvent to dissolve compounds that can interfere with the hydrolysis process such as fats and proteins. This research was conducted by extracting jackfruit straw powder into starch. Variation of the extraction process was the type of solvent (H2O, NaOH of 0.2%, and NaHCO3 of 0.2%) and the extraction time (5, 10, 15, 20, and 25 minutes) at room temperature. The results showed that the highest reducing sugar concentration of 2.16% was in the type of NaOH solvent for 25 minutes.

2018 ◽  
Vol 156 ◽  
pp. 03006
Author(s):  
Nadiem Anwar ◽  
Iman Mukhaimin ◽  
Mining Harsanti ◽  
Ate Romli

Organic wastes from Swiettenia marcophylla L, Artocarpus heterophyllus L, Mangifera indica L, and Annona muricata L were prepared by grinding into 0.1875, 0.3750, 0.7500 mm of particle size and delignified by 2% NaOH at 80°C for 90 minutes. Acid dilution hydrolysis process with H2SO4 1% was performed at 150°C for 120 minutes in a closed reactor. The effect of particle size and delignification on and reducing sugar concentration were investigated. The result showed (1) leaves that can be used as raw material to produce hydrogen should have 38–49% cellulose and hemicellulose. (2) Reducing sugar concentration increased with particle size reduction and delignification. (3) the best result with the highest reducing sugar concentration was achieved by 0.1875 mm particle size with delignification on Annona muricata L.


2013 ◽  
Vol 763 ◽  
pp. 246-249
Author(s):  
Xiao Song ◽  
Peng Zhao

Flavonoids from Tussilago farfara L. was extracted with the assistance of microwave.Box-Behnken design (BBD) was employed to optimize extraction time; microwave power and ratio of water to raw material to obtain a high flavonoids yield.The optimum extraction conditions were as follows: 73.3% ethanol-water solvent, time 16.25 min and ratio of solvent to raw material 36.2ml/g.The yield of flavonoids was 11.37% based on the above mentioned conditions.


2014 ◽  
Vol 1014 ◽  
pp. 61-64
Author(s):  
Xiao Song ◽  
Peng Zhao ◽  
Qing Hua Meng ◽  
Zhi Shu Tang ◽  
Chang Li Wang

Flavonoids from Platycarya Strobi lacea Sieb.et Zucc. was extracted with the assistance of microwave.Box-Behnken design (BBD) was employed to optimize extraction time; microwave power and ratio of solvent to raw material to obtain a high flavonoids yield. The optimum extraction conditions were as follows: 65.32% ethanol-water solvent, time 3.96 min and ratio of solvent to raw material 20.8 ml/g.The yield of flavonoids was 3.41% based on the above mentioned conditions.


Food Research ◽  
2020 ◽  
Vol 4 (S6) ◽  
pp. 124-131
Author(s):  
Rabiatul Amirah R. ◽  
Ellya Hazreera A.J. ◽  
Nor Qhairul Izzreen M.N. ◽  
Rozzamri A. ◽  
Umi Hartina M.R.

The study aimed to determine the characteristics of gelatin from water buffalo (Bubalus bubalis) skin pre-treated with NaOH and Ca(OH)2 at different concentrations (0.3 M, 0.5 M and 0.7 M) and extracted at 65˚C for 6 hrs and 24 hrs respectively. The gelatin obtained was evaluated for its moisture, protein and ash content, UV-vis absorption value, colour, emulsifying and foaming properties. The highest yield (20.25%) was observed for gelatin extracted by 0.5 M NaOH at 24 hrs extraction time. For alkaline pre-treatment, it was found that NaOH was more efficient than Ca(OH)2 in terms of preparing the skin for subsequent extraction process. The protein content of the extracted gelatin samples was in the range of 71.76% - 87.83%, showing that the varying processing conditions are sufficiently to recover protein from the raw material. Ash content for all samples was in agreement with USDA standard, which was below than 3%. The extracted gelatin had varying pH values which were from 5.47 to 7.02. The gelatin was colourless with ‘L’ values of more than 80, except for 0.7 M Ca(OH)2 at 24 hrs which showed slightly darker properties. The intensity of the UV-vis absorption spectrum showed that a high absorption peak was observed at 6 hrs of extraction time (230 – 250 nm) compared to 24 hrs extraction time. Emulsifying properties of buffalo gelatin increased with increasing concentrations of alkaline except for 0.7 M NaOH and 0.7 M Ca(OH)2 for both extraction time. Meanwhile, foam expansion of the gelatin extracted from the different extraction conditions was observed to have a significant difference (p < 0.05) for all samples. To our knowledge, buffalo skin has the potential to be an alternative source of gelatin in the diversified industrial application by modifying the extraction conditions in order to produce gelatin with desired quality.


Processes ◽  
2020 ◽  
Vol 8 (2) ◽  
pp. 173 ◽  
Author(s):  
Quoc Toan Tran ◽  
Thu Le Vu Thi ◽  
Tien Lam Do ◽  
Hong Minh Pham Thi ◽  
Bich Hoang Thi ◽  
...  

Callicarpa candicans (Burm. f.) Hochr. (Callicarpa cana L.) is a medicinal plant that is distributed mainly in the tropics and subtropics of Asia and finds a wide range of uses in traditional medicine. In this study, we attempted and optimized the microwave-assisted hydro-distillation (MAHD) process to obtain essential oil from the leaves of C. candicans. In addition, the obtained oil was analyzed for volatile composition by gas chromatography–mass spectrometry (GC-MS) and assayed for bioactivity against several bacteria and cancer cell lines. To optimize the extraction process, response surface methodology (RSM) in combination with central composite design (CCD) was adopted. Experimental design and optimization were carried out with respect to three experimental factors including the ratio of water to raw material, extraction time, and microwave power. The optimal extraction conditions were obtained as follows: water to raw material ratio of 6/1 (v/w), extraction time 42 min, and microwave power 440 W. Composition determination of the obtained C. candicans essential oil indicated the presence of predominant components including caryophyllene <b-> (10.45%), cadinene <d-> (10.28%), gurjunene <a-> (8.95%), muurolene <g-> (8.92%), selinene <a-> (7.06%), selinene <b-> (5.59%), and copaene <a-> (5.40%). In comparison with the essential oils obtained via traditional hydro-distillation method, the essential oil extracted by MAHD exhibited superior anti-proliferative activity on all tested cancer cell lines. Current results imply that the MAHD is capable of recovering biologically-active natural products of greater quantity than that recovered by the conventional distillation.


2011 ◽  
Vol 140 ◽  
pp. 385-393 ◽  
Author(s):  
Xian Feng Shi ◽  
Yuan Xu ◽  
Yu Hua Li ◽  
Hong Xia Zeng ◽  
Yu Hong Sun

The extraction processing of lycopene from watermelon was investigated in this paper. Based on single factor experiments, response surface methodology (RSM) was adopted to study the key parameters such as number of extraction, extraction temperature, extraction time in order to increase extraction rate of lycopene. A second order quadratic equation was established and the applicability of model and interaction involved factors on predicting the lycopene extracting content was verified. The results indicated that the optimum extraction conditions were hexane (containing 2% dichloromethane) as extraction solvent, ratio of solvent to raw material of 3:1 (mL/g), number of extraction of 2, extraction time of 1.9 h and extraction temperature of 29.8°C. Under these conditions the extracting content of lycopene was 14.71±0.22 mg/kg, which is well in agreement with value predicted by the model.


Jurnal BIOMA ◽  
2017 ◽  
Vol 13 (1) ◽  
pp. 1-8
Author(s):  
Siska Handayani ◽  
Zulkifliani Zulkifliani ◽  
Adisyahputra Adisyahputra ◽  
Devitra Sakarani

This study aims to determine the most effective compound used to hydrolyze soy husk waste to produce reducing sugar as raw material for bioethanol fermentation. The study was conducted at the Laboratory of Bioprocess PPPTMGB "LEMIGAS" in April-September 2015. The method used is experiment using a randomized block design consisting of two factors. The first factor is the type of compounds used in the process of hydrolysis, namely H2SO4, HCl, NaOH, and NH3. The second factor is the concentration of hydrolyze compound 0.2%, 0.4%. 0.6%, 0.8%, and 1% (v/v) and every treatment repeated 4 times. Parameters measured were content of reduced sugar hydrolysis product, and secondary data that content of cellulose and hemicellulose also the density of ethanol. Concentration of reducing sugar from hydrolysis of soybean husk is analyzed by two-way ANOVA test. ANOVA analysis result indicate that the best hydrolysis compounds in hydrolizing soybean husk is HCl with the optimum concentration is 0,4%. And there are interactions between treatment of compound used to hydrolyze as well as concentration on reducing sugar concentration (mg/mL) as product from soybean husk waste hydrolysis. Post-hoc test showed that HCl 0,4% produce the highest concentration of reducing sugar at 31.23 mg/mL.


Author(s):  
Nik ‘Amirah Farhana Nik Ahmad Lutfi ◽  
Mohd Farid Atan ◽  
Nazeri Abdul Rahman ◽  
Shanti Faridah Salleh ◽  
Noraziah Abdul Wahab

The main objective of this study is to improve the mathematical modelling of Cymbopogon winterianus essential oil extraction by steam distillation proposed by Cassel and Vargas by minimum 5% error reduction. Two process variable of steam distillation which are extraction time and raw material state (dry or natural) has been optimized by using factorial experimental planning to obtain high yields of citronella essential oil from twig and leaves of lemongrass species Cymbopogon winterianus (C.winterianus). The optimal condition for maximum yield (0.942%) were found to be an extraction time, 4 hr, state, natural plant. The study of Cassel and Vargas was subsequently continued with five proposed kinetics model of the extraction process. The modelling of the extraction process is optimized by using one adjustable parameter of the model and the adequacy of the fit of the models to the experimental data are analyzed by using three statistical criteria that are correlation coefficient (r) ,the root mean square error (RMSE) and the mean relative deviation modulus (E). The result has shown that the mathematical model developed by Ana based on mass transfer fundamentals is the optimum mathematical model for the extraction of Cymbopogon winterianus essential oil by steam distillation.


2011 ◽  
Vol 317-319 ◽  
pp. 321-324
Author(s):  
Peng Zhao ◽  
Ou Li ◽  
A Ping Liu

Polysaccharide from Limonium bicolor Kunze (Bge.)(LBPs) was extracted with the assistance of ultrasonic.Box-Behnken design(BBD) was employed to optimize extraction time; extraction temperature;ultrasonic extraction power and ratio of water to raw material to obtain a high LBPs yield.The optimum extraction conditions were as follows: extraction temperature 81.23°C, ultrasonic power 190.86W, extraction time 42.39 min and ratio of water to raw material 15.4ml/g.The yield of polysaccharide was 7.11% based on the above mentioned conditions. Close agreement between experimetal and predicted values was found.


2012 ◽  
Vol 512-515 ◽  
pp. 2386-2389
Author(s):  
Xiao Rong Li ◽  
Peng Zhao

Polysaccharide from Acanthopanax obouatus Hoo(AHPs) was extracted with the hot water.Box-Behnken design(BBD) was employed to optimize extraction temperature; extraction time and ratio of water to raw material to obtain a high AHPs yield. The yield of polysaccharide was 4.68% based on the above mentioned conditions.Close agreement between experimetal and predicted values was found.


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