IDENTIFICATION OF POTENTIALLY TOXIC COMPOUNDS IN COMPLEX EXTRACTS OF ENVIRONMENTAL SAMPLES USING GAS CHROMATOGRAPHY–MASS SPECTROMETRY AND MULTIVARIATE DATA ANALYSIS

2007 ◽  
Vol 26 (2) ◽  
pp. 208 ◽  
Author(s):  
Magnus Bergknut ◽  
Adam Kucera ◽  
Kristina Frech ◽  
Erika Andersson ◽  
Magnus Engwall ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Data Analysis ◽  
Environmental Samples ◽  
Multivariate Data Analysis ◽  
Multivariate Data ◽  
Gas Chromatography Mass Spectrometry ◽  
Toxic Compounds ◽  
Chromatography Mass Spectrometry

Irace Level Detection of Chlorinated Paraffins in Biological and Environmental Samples, Using Gas Chromatography/Mass Spectrometry with Negative-Ion Chemical Ionization

1985 ◽  
Vol 68 (3) ◽  
pp. 427-430
Author(s):  
Peter P Schmid ◽  
Markus D Muller
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Environmental Samples ◽  
Chemical Ionization ◽  
Negative Ion ◽  
Gas Chromatography Mass Spectrometry ◽  
Chromatography Mass Spectrometry ◽  
Biological And Environmental Samples ◽  
Chlorinated Paraffins ◽  
Negative Ion Chemical Ionization

Abstract A method is described for detection of chlorinated paraffins (CPs) in biological and environmental samples. Sample preparation includes sulfuric acid treatment followed by adsorption chromatography on ilumina, which yields the CPs in one fraction that is almost free of interfering material. Using gas chromatography/mass spectrometry j with negative-ion chemical ionization, the limit of detection is 5 ng (corresponding to the lower ppb range). CP levels of 30 ppm, 200 ppb, ' and 5 ppb were found in sewage sludge, human fat, and sediment, respectively.

scholarly journals Identification of Chemical Substances in Environmental Samples by Gas Chromatography/Mass Spectrometry.

1995 ◽  
Vol 5 (1) ◽  
pp. 47-64 ◽  
Author(s):  
Yoshifumi HANADA ◽  
Kiwao KADOKAMI ◽  
Hiroaki SHIRAISHI ◽  
Kiyoshi IMAMURA ◽  
Shigeru SUZUKI ◽  
...  
Keyword(s):  
Mass Spectrometry ◽  
Gas Chromatography ◽  
Environmental Samples ◽  
Gas Chromatography Mass Spectrometry ◽  
Chemical Substances ◽  
Chromatography Mass Spectrometry
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