scholarly journals Magnetite-Containing Sulfonated Polyacrylamide as a Nanocatalyst for the Preparation of Biscoumarins

2017 ◽  
pp. 692-700 ◽  
Author(s):  
Kaveh Parvanak Boroujeni ◽  
Shahla Hadizadeh ◽  
Sodabeh Hasani ◽  
Abdulhamid Fadavi ◽  
Mansooreh Shahrokh
BMC Chemistry ◽  
2019 ◽  
Vol 13 (1) ◽  
Author(s):  
Hossein Shahbazi-Alavi ◽  
Sheida Khojasteh-Khosro ◽  
Javad Safaei-Ghomi ◽  
Maryam Tavazo

Abstract Crosslinked sulfonated polyacrylamide (Cross-PAA-SO3H) attached to nano-Fe3O4 as a superior catalyst has been used for the synthesis of 3-alkyl-4-phenyl-1,3-thiazole-2(3H)-thione derivatives through a three-component reactions of phenacyl bromide or 4-methoxyphenacyl bromide, carbon disulfide and primary amine under reflux condition in ethanol. A proper, atom-economical, straightforward one-pot multicomponent synthetic route for the synthesis of 1,3-thiazoles in good yields has been devised using crosslinked sulfonated polyacrylamide (Cross-PAA-SO3H) tethered to nano-Fe3O4. The catalyst has been characterized by Fourier-transform infrared spectroscopy (FT-IR), scanning electron microscope (SEM), dynamic light scattering (DLS), X-ray powder diffraction (XRD), energy-dispersive X-ray spectroscopy (EDS), thermogravimetric analysis (TGA) and vibrating-sample magnetometer (VSM).


Polymers ◽  
2019 ◽  
Vol 11 (6) ◽  
pp. 1046 ◽  
Author(s):  
Saeed Akbari ◽  
Syed Mohammad Mahmood ◽  
Hosein Ghaedi ◽  
Sameer Al-Hajri

Copolymers of acrylamide with the sodium salt of 2-acrylamido-2-methylpropane sulfonic acid—known as sulfonated polyacrylamide polymers—had been shown to produce very promising results in the enhancement of oil recovery, particularly in polymer flooding. The aim of this work is to develop an empirical model through the use of a design of experiments (DOE) approach for bulk viscosity of these copolymers as a function of polymer characteristics (i.e., sulfonation degree and molecular weight), oil reservoir conditions (i.e., temperature, formation brine salinity and hardness) and field operational variables (i.e., polymer concentration, shear rate and aging time). The data required for the non-linear regression analysis were generated from 120 planned experimental runs, which had used the Box-Behnken construct from the typical Response Surface Methodology (RSM) design. The data were collected during rheological experiments and the model that was constructed had been proven to be acceptable with the Adjusted R-Squared value of 0.9624. Apart from showing the polymer concentration as being the most important factor in the determination of polymer solution viscosity, the evaluation of the model terms as well as the Sobol sensitivity analysis had also shown a considerable interaction between the process parameters. As such, the proposed viscosity model can be suitably applied to the optimization of the polymer solution properties for the polymer flooding process and the prediction of the rheological data required for polymer flood simulators.


2010 ◽  
Vol 119 (6) ◽  
pp. 3623-3629 ◽  
Author(s):  
Masoud Rashidi ◽  
Anne Marit Blokhus ◽  
Arne Skauge

2016 ◽  
Vol 66 (3) ◽  
pp. 477-484 ◽  
Author(s):  
Ehsan Alvand ◽  
Jamal Aalaie ◽  
Mahmood Hemmati ◽  
Vali Ahmad Sajjadian

2014 ◽  
Vol 35 (5) ◽  
pp. 663-671 ◽  
Author(s):  
Mahsa Baghban Salehi ◽  
Mohsen Vafaie Sefti ◽  
Ebrahim Vasheghani-Farahani ◽  
Asefe Mousavi Moghadam

2012 ◽  
Author(s):  
Ming Han ◽  
Xianmin Zhou ◽  
Alhasan B. Fuseni ◽  
Badr H. Al-Zahrani ◽  
Abdulkareem M. AlSofi

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