Asphalt Binder Aging Methods to Accurately Reflect Mixture Aging

2021 ◽  
Author(s):  
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Jeramie J. Adams Western Research Institute ◽  
David A. Anderson ◽  
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...  
Keyword(s):  
2020 ◽  
Vol 13 (6) ◽  
pp. 697-706
Author(s):  
Yuhong Wang ◽  
Kecheng Zhao ◽  
Fangjin Li ◽  
Qi Gao ◽  
King Wai Chiu Lai

AbstractThe microscopic surface features of asphalt binders are extensively reported in existing literature, but relatively fewer studies are performed on the morphology of asphaltene microstructures and cross-examination between the surface features and asphaltenes. This paper reports the findings of investigating six types of asphalt binders at the nanoscale, assisted with atomic force microscopy (AFM) and scanning transmission electron microscopy (STEM). The surface features of the asphalt binders were examined by using AFM before and after being repetitively peeled by a tape. Variations in infrared (IR) absorbance at the wavenumber around 1700 cm−1, which corresponds to ketones, were examined by using an infrared s-SNOM instrument (scattering-type scanning near-field optical microscope). Thin films of asphalt binders were examined by using STEM, and separate asphaltene particles were cross-examined by using both STEM and AFM. In addition, connections between the microstructures and binder’s physicochemical properties were evaluated. The use of both microscopy techniques provide comprehensive and complementary information on the microscopic nature of asphalt binders. It was found that the dynamic viscosities of asphalt binders are predominantly determined by the zero shear viscosity of the corresponding maltenes and asphaltene content. Limited samples also suggest that the unique bee structures are likely related to the growth of asphaltene content during asphalt binder aging process, but more asphalt binders from different crude sources are needed to verify this finding.


Materials ◽  
2019 ◽  
Vol 12 (7) ◽  
pp. 1067 ◽  
Author(s):  
Hechuan Li ◽  
Jianying Yu ◽  
Shaopeng Wu ◽  
Quantao Liu ◽  
Yuanyuan Li ◽  
...  

Induction heating is a valuable technology to repair asphalt concrete damage inside. However, in the process of induction heating, induced particles will release a large amount of heat to act on asphalt binder in a short time. The purpose of this paper was to study the effect of induction heating on asphalt binder aging in steel fibers modified asphalt concrete. The experiments were divided into two parts: induction heating of Dramix steel fibers coated with asphalt binder (DA) and steel wool fibers modified asphalt concrete. After induction heating, the asphalt binders in the samples were extracted for testing aging indices with Fourier Transform Infrared (FTIR), Dynamic Shear Rheometer (DSR), and Four-Components Analysis (FCA) tests. The aging of asphalt binder was analyzed identifying the change of chemical structure, the diversification of rheological properties, and the difference of component. The experiments showed that the binder inside asphalt concrete began aging during induction heating due to thermal oxygen reaction and volatilization of light components. However, there was no peak value of the carbonyl index after induction heating of ten cycles, and the carbonyl index of DA was equivalent to that of binder in asphalt concrete after three induction heating cycles, which indicated the relatively closed environment inside asphalt concrete can inhibit the occurrence of the aging reaction.


2012 ◽  
Vol 535-537 ◽  
pp. 1686-1692
Author(s):  
Yong Chun Qin ◽  
Sui Yuan Wang ◽  
Wei Zeng ◽  
Xiao Pei Shi ◽  
Jian Xu ◽  
...  

One of the main benefits advertised with the use of warm mix asphalt (WMA) is the decreasing aging of the asphalt binder resulting from the lower production temperature compared to conventional hot mix asphalt (HMA). Some tests were performed to determine the asphalt binder aging properties from WMA and HMA. Asphalt binders were recovered by extraction and distillation from asphalt mixtures premixed at different temperatures (140°C, 160°C, 180°C for HMA, 100°C and 120°C for WMA) in the mixing plant. Penetration@25°C, softening point (R&B) and rotational Brookfield viscosity tests were carried out. Results show that the aging of asphalt binder increases as the mixing temperature is elevated, and remarkably accelerates at the temperatures higher than 150°C. Warm mix asphalt (for example, mixing temperature at 100°Cor 120°C) can greatly reduce the aging of asphalt. Aging of the asphalt binder is one of the factors that would affect the mixture’s fatigue life. Four-point beam fatigue test samples were mixed and compacted at 140°C for HMA and 120°C for WMA, and fatigue tests with a frequency of 10 Hz and three constant strain levels (150 micro-strain, 300 micro-strain, 450 micro-strain, respectively) were performed. Results show that WMA’s fatigue life was higher than the control HMA, which indicates that it may reduce aging of asphalt binder and improve fatigue performance of asphalt mixture at lower production temperatures.


2005 ◽  
Vol 32 (6) ◽  
pp. 1166-1169 ◽  
Author(s):  
Katsuyuki Yamaguchi ◽  
Iwao Sasaki ◽  
Seishi Meiarashi

The photodegradation behavior of a straight asphalt was investigated using a new method "photodegradation test of asphalt binder using pressed thin film samples". Although the photodegradation caused by outdoor exposure is limited to the near surface, the results confirmed that the degree of degradation during 1 to 2 months is more severe than that by the pressure aging vessel (PAV) test, which is designed to simulate the degradation that will occur in the asphalt pavement over 5 to 10 service years.Key words: asphalt binder, aging, photodegradation, thin film, DSR, FTIR.


Author(s):  
Runhua Zhang ◽  
Jo E. Sias ◽  
Eshan V. Dave

Aging has a significant effect on performance of asphalt materials. Reliable characterization of asphalt binder properties with aging is crucial to improving asphalt binder specifications as well as modification and formulation methods. The objective of this study is to correlate the laboratory conditioning methods with field aging using evolution of binder rheological parameters with time and pavement depth. Loose mixtures are aged in the lab (5 and 12 days aging at 95°C, and 24 h at 135°C) and recovered binder rheological properties are compared with those from different layers of field cores. The virgin binder results with 20 h pressure aging vessel (PAV) aging are also included. Binder testing is conducted using a dynamic shear rheometer with a 4 mm plate over a wide range of frequencies and temperatures. Rheological parameters calculated from the master curves, performance grade system, and binder Christensen–Anderson–Marasteanu model are used to evaluate changes with aging. The field aging gradient is evaluated, and the laboratory conditioning durations corresponding with the field aging durations at different pavement depths are calculated. The results show that 5 days of aging can simulate around 8 years of field aging (in New Hampshire) for the top 12.5 mm pavement, and 12 days’ aging can simulate approximately 20 years; 20 h PAV binder aging is not adequate to capture the long-term performance of the pavement. This study provides a way to optimize the laboratory conditioning durations and evaluate the performance of asphalt material with respect to pavement life (time) and depth (location) within the pavement structure.


2014 ◽  
Vol 68 ◽  
pp. 172-182 ◽  
Author(s):  
P.E. Yuhong Wang ◽  
Yong Wen ◽  
Kecheng Zhao ◽  
Dan Chong ◽  
Alvin S.T. Wong

2015 ◽  
Vol 101 ◽  
pp. 611-616 ◽  
Author(s):  
Rodolfo Rascon De Lira ◽  
Douglas D. Cortes ◽  
Cesar Pasten

Author(s):  
Fujie Zhou ◽  
Pravat Karki ◽  
Soohyok Im

Current Superpave® PG specification uses parameter | G*|sin(δ) to quantify asphalt binder fatigue resistance. The parameter’s effectiveness has been debated for a long time. AASHTO recently adopted the linear amplitude sweep test as a provisional standard, AASHTO TP 101-12. The authors evaluated the sensitivity of this standard to different aging conditions: unaged original binders, rolling thin-film oven-aged binders, and 20- to 80-h pressure aging vessel–aged binders. Test results showed, in many cases, longer predicted fatigue lives for more-aged binders. Thus this study developed a simple fatigue cracking test for asphalt binders. In this new test, the pure linear amplitude sweep (PLAS) test, peak shear strain was increased linearly from 0% to 30% over a course of 3,000 oscillatory cycles. A new fatigue parameter, the fatigue resistance energy index (FREI), was derived with fracture mechanics. The PLAS test and FREI parameter were sensitive to both binder aging conditions and rejuvenator type and dosage. Four laboratory mixtures were employed to evaluate the correlation between this new binder fatigue test and the two mixture cracking tests: the Texas overlay test and the Illinois flexibility index test. The results showed that the PLAS and FREI correlated well with the mixture cracking tests. Additionally, the proposed method was preliminarily verified with the FHWA accelerated loading facility test, and a fair relationship with the full-scale fatigue test data was observed. It is obvious that the PLAS and associated FREI need further validation through more field test sections.


2010 ◽  
Vol 38 (1) ◽  
pp. 101934 ◽  
Author(s):  
M. R. Mitchell ◽  
R. E. Link ◽  
Tejash Gandhi ◽  
Chandrakiran Akisetty ◽  
Serji Amirkhanian
Keyword(s):  

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