Processing of Clay/Epoxy Nanocomposites with A Three-Roll Mill Machine

2002 ◽  
Vol 740 ◽  
Author(s):  
Asma Yasmin ◽  
Jandro L. Abot ◽  
Isaac M. Daniel
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Mixing Time ◽  
Clay Content ◽  
Epoxy Nanocomposites ◽  
Clay Particles ◽  
Roll Mill ◽  
Short Period ◽  
Mixing Techniques ◽  
Xrd And Tem

ABSTRACTIn the present study, a three-roll mill machine was used to disperse/exfoliate the nanoclay particles in an epoxy matrix. The compounding process was carried out with varying mixing time and concentrations of clay particles (1 to 10 wt.%). It was found that the longer the mixing time, the higher the degree of intercalation. Mechanical properties, XRD and TEM were used to characterize the nanocomposites. Elastic modulus was found to increase with increasing clay content, however, the tensile strength was not found to vary accordingly. Compared to conventional direct and solution mixing techniques, the compounding of clay/epoxy nanocomposites by a three-roll mill was found to be highly efficient in achieving higher levels of intercalation/exfoliation in a short period of time and also environmentally friendly.

Effects of Surfactant Content and Clay Content on Properties of NR Nanocomposites

2010 ◽  
Vol 123-125 ◽  
pp. 55-58 ◽  
Author(s):  
Chalermpan Keawkumay ◽  
Kasama Jarukumjorn ◽  
Nitinat Suppakarn
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Natural Rubber ◽  
Cation Exchange ◽  
Cation Exchange Capacity ◽  
Clay Content ◽  
Exchange Capacity ◽  
Cure Characteristics ◽  
Roll Mill ◽  
Cure Time

Montmorillonite (MMT) was modified by octadecylamine (ODA) surfactant. The surfactant contents were varied, i.e. 0.5, 1.0 and 2.0 times the cation exchange capacity (CEC) of the MMT. XRD and FTIR spectra of the organoclay revealed that ODA molecules intercalated into MMT layers. The MMT-ODA was melt-mixed with natural rubber (NR) using a two roll mill. Effects of surfactant content and organoclay content on cure characteristics, mechanical properties, and morphologies of NR nanocomposites were investigated. Morphologies of the NR nanocomposites, with increasing surfactant content, revealed the exfoliated structure and the good dispersion of the organoclay in the NR matrix. These caused the enhancement of mechanical properties of the NR nanocomposites. With increasing the MMT-ODA2 content up to 5 phr, scorch time and cure time of the NR nanocomposites decreased while their tensile strength increased.

Effect of Mixing Condition on the Mechanical Properties of Magnesium Based Composites

2015 ◽  
Vol 1087 ◽  
pp. 434-438
Author(s):  
Wan Nur Azrina Wan Muhammad ◽  
Yoshiharu Mutoh
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Mixing Time ◽  
Mixing Conditions ◽  
Mixing Condition ◽  
Mixing Speed ◽  
Sic Particle

The effects of mixing conditions, i.e; mixing speed and mixing duration on the mechanical properties of the magnesium based composites were investigated. The hardness, tensile strength and microstructure of composites were studied. It was found that increase of the mixing speed and prolong the mixing time can improved the distribution of SiC particle and mechanical properties of magnesium based composites.

Effects of Mixing Parameters on Tensile Strength of TPU/NR Blends

2013 ◽  
Vol 291-294 ◽  
pp. 2654-2656
Author(s):  
Nor Azwin Ahad ◽  
Sahrim Hj Ahmad ◽  
Norazwani Muhammad Zain
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Natural Rubber ◽  
Polymer Blends ◽  
Mixing Time ◽  
Thermoplastic Polyurethane ◽  
Mixing Times ◽  
Melt Mixing ◽  
Mixing Parameters ◽  
The Poor

The blends of thermoplastic polyurethane (TPU) with natural rubber (NR) were prepared via melt mixing technique, at four different blending temperature at range 180°C - 210°C and mixing times of 8, 10, 12, 14 min. The effects of both mixing parameters on tensile strength of the blends were investigated. The blend of 85TPU15NR shows the maximum tensile strength at 180°C and 10 min mixing. The viscosity of the polymer blends will decrease as the temperature increased. The movements of molecules are more worthy because of the poor molecules interaction. The increasing of mixing time will increase the compatibility of the blends and also increase in mechanical properties. Mixing time and mixing temperature are important parameters in acquiring blends having optimum mechanical properties.

Tensile Properties of 3D-Printed Polycarbonate/Carbon Nanotube Nanocomposites

2018 ◽  
Author(s):  
Karun Kalia ◽  
Amir Ameli
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Carbon Nanotube ◽  
Ultimate Tensile Strength ◽  
Tensile Properties ◽  
Modulus Of Elasticity ◽  
Nozzle Diameter ◽  
Fused Deposition ◽  
Short Period ◽  
Printing Direction

Fused deposition modeling (FDM) is highly commercialized Rapid Prototyping (RP) technology for its ability to build complex parts with low cost in a short period of time. The process parameters in the FDM play a vital role in the mechanical properties of the polymeric parts. Most of the research studies show that the variable parameters such as orientation, layer thickness, raster angle, raster width, and air gap are some of the key parameters that affect the mechanical properties of FDM-processed polymeric parts. However, no reports have been made regarding the influence of nozzle diameter with raster width on the tensile properties of FDM fabricated polymeric parts. This work was devoted to achieving improved and isotropic mechanical properties in polycarbonate (PC) and PC/carbon nanotube (PC/CNT) nanocomposites by investigating the effect of printing parameters in FDM process. The nozzle diameter to raster width ratio, α was found to significantly affect the mechanical properties. The printing direction dependency in tensile properties were studied with the ratio α < 1 and α≥ 1 at three different raster angles of 0°, 45°/−45° and 90°. For α < 1, Ultimate tensile strength and modulus of elasticity were higher for 0°, compared to 45°/−45° and 90° raster angles. However, for α ≥ 1, the ultimate tensile strength and the modulus of elasticity showed little dependency to print direction. This certainly determines the decrease in anisotropy at higher values of α. Mesostructure characterization with microscopy and image analysis were used to further explain the printing behavior and the resultant properties of the printed samples.

scholarly journals Effects of nano and micro size of clay particles on the compressive and tensile strength properties of self-consolidating concrete

2018 ◽  
Vol 162 ◽  
pp. 02030 ◽  
Author(s):  
Baydaa Alrashedi ◽  
Maan Hassan
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Physical And Mechanical Properties ◽  
Strength Properties ◽  
Pozzolanic Activity ◽  
Chemical Compositions ◽  
Particle Sizes ◽  
Self Consolidating Concrete ◽  
Clay Particles

Many past studies concerned about using of nanoclay (nC) particles as an active pozzolan to concrete and their influence on the physical and mechanical properties. In this study, the effects of various nanoclay particle sizes and dosages on the compressive and flexural tensile strengths of SCCs were investigated. Progressive nC percentages of 2%, 5% and 8% were replaced with cements and the produced SCCs were evaluated and compared with similar replacement levels of the metakaolin MK which have comparable chemical compositions. The produced SCCs were tested for compressive, flexural tensile and splitting tensile strengths in 28 and 90 days. Results indicated that nC replacement harmed all the studied mechanical properties at 28 days age. After 90 days, however, both compressive and tensile strengths of nC concretes show superior strengths than control concrete and also exceeded MK concretes made of equivalent replacement levels. This behavior demonstrates the pozzolanic activity of the nC particles at later ages and proved to be significantly more effective than early ages.

A Preliminary Study on Cryogenic Mechanical Properties of Epoxy Blend Matrices and SiO2/Epoxy Nanocomposites

2006 ◽  
Vol 312 ◽  
pp. 211-216 ◽  
Author(s):  
Shao Yun Fu ◽  
Qin-Yan Pan ◽  
Chuan Jun Huang ◽  
Guo Yang ◽  
Xin-Hou Liu ◽  
...  
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Room Temperature ◽  
Sol Gel ◽  
Sio2 Nanoparticles ◽  
Diglycidyl Ether ◽  
Slight Reduction ◽  
Epoxy Nanocomposites ◽  
Sol Gel Process ◽  
Cryogenic Mechanical Properties

Epoxy blend matrices were prepared by incorporating polyurethane-epoxy into diglycidyl ether of bisphenol-F (DGEBF) type epoxy while SiO2/epoxy nanocomposites were made using DGEBF type epoxy and tetraethylorthosilicate (TEOS) via a sol-gel process. The mechanical properties including tensile and impact properties at 77 K of the matrices and nanocomposites were studied. The mechanical properties at room temperature were also given for the purpose of comparison with the cryogenic mechanical properties. The results showed that the incorporation of polyurethane-epoxy with a proper content into DGEBF type epoxy enhanced the mechanical properties at both room and cryogenic temperatures. Addition of SiO2 nanoparticles to DGEBF type epoxy led to significant increase in tensile strength at cryogenic temperature (77 K) while no evident change in tensile strength at room temperature. In addition, a slight enhancement by the addition of 2 wt % silica while a slight reduction by the addition of 4 wt % silica were observed in impact energy.

scholarly journals Some mechanical properties of aggregates of top soils from the IJsselmeer polders. 1. Undisturbed soil aggregates.

1984 ◽  
Vol 32 (3) ◽  
pp. 205-214
Author(s):  
A.R. Dexter ◽  
B. Kroesbergen ◽  
H. Kuipers
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Soil Aggregates ◽  
Clay Content ◽  
Water Stability ◽  
Undisturbed Soil

Aggregates were collected from the arable layer at eight sites in the IJsselmeer polders. The compositions of the soils were determined, and measurements were made of porosities, tensile strengths and water stabilities of undisturbed aggregates. Porosity was negatively correlated with the age of the soils since reclamation. Tensile strength of dry aggregates and water stability were both positively correlated with the clay content. The soils had extremely high values of friability. Tensile strength was negatively correlated with porosity. Porosity had no clear influence on water stability. (Abstract retrieved from CAB Abstracts by CABI’s permission)

Cure and Mechanical Properties of Natural Rubber Filled Bacterial Cellulose

2016 ◽  
Vol 705 ◽  
pp. 40-44
Author(s):  
Chaiwute Vudjung
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Natural Rubber ◽  
Bacterial Cellulose ◽  
Elongation At Break ◽  
Roll Mill ◽  
Cure Time ◽  
Mooney Viscosity

Natural rubber (NR) containing the nata de coco fiber or Bacterial cellulose (BC) was prepared by co-coagulation of BC and concentrated NR latex with CaCl2 and compounded by two roll mill. The effect of BC content was the important factor in this study. It was that found tensile strength and elongation at break of NR filled BC (NR/BC) decreased with increasing BC content. The addition of BC into NR affect Mooney viscosity of NR/BC masterbatch, with increasing BC content, scorch time and cure time of their compound decreased.

Structure and Mechanical Properties of Carboxylated Styrene-Butadiene Rubber (XSBR)/Pristine Clay Nanocomposites

e-Polymers ◽  
2007 ◽  
Vol 7 (1) ◽  
Author(s):  
Mahdi Abdollahi ◽  
Ali Rahmatpour ◽  
Homayon Hossein Khanli
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Tensile Strain ◽  
Clay Content ◽  
Mechanical Tests ◽  
Styrene Butadiene Rubber ◽  
Clay Nanocomposites ◽  
Butadiene Rubber ◽  
Carboxylated Styrene Butadiene Rubber ◽  
Styrene Butadiene

AbstractCarboxylated styrene- butadiene rubber (XSBR)/clay nanocomposites were prepared by mixing the XSBR latex with aqueous clay dispersion and cocoagulating the mixture. TEM and XRD were applied to characterize the structure of nanocomposites. Fully exfoliated structure was observed for the nanocomposites containing equal to or less than 10 phr (weight parts per hundred) clay. With increasing the clay content to 20 phr, both non-exfoliated (stacked layers) and exfoliated structures can be observed simultaneously in the nanocomposites. The results of mechanical tests on the vulcanized clay-free XSBR and XSBR/clay nanocomposites showed that the nanocomposites present better mechanical properties than clay-free XSBR vulcanizate. Furthermore, modulus, tensile strength, tensile strain at break and hardness (shore A) increased with increasing the clay content, indicating the nanoreinforcement effect of clay on the mechanical properties of XSBR/ clay nanocomposites.

Thermal stability, mechanical and adsorption resistant properties of HDPE/PEG/Clay nanocomposites on exposure to electron beam

e-Polymers ◽  
2008 ◽  
Vol 8 (1) ◽  
Author(s):  
Ahmad Mohaddespour ◽  
Seyed Javad Ahmadi ◽  
Hossein Abolghasemi ◽  
Shahryar Jafarinejad
Keyword(s):  
Mechanical Properties ◽  
Tensile Strength ◽  
Electron Beam ◽  
Ethylene Glycol ◽  
Thermal Resistance ◽  
Young’S Modulus ◽  
Clay Content ◽  
Poly Ethylene Glycol ◽  
The Matrix ◽  
Poly Ethylene

AbstractThe Influence of electron beam on behaviors of high density polyethylene/poly(ethylene glycol)/organoclay nanocomposites has been studied. Nanocomposite compounds were prepared by melt intercalation method. X-ray diffraction (XRD) and transition electron microscopy (TEM) revealed the combination of nanocomposite morphology. Thermal and mechanical properties of nanocomposites were studied by using Thermogravimetric analysis (TGA), Young's modulus, tensile strength and hardness tests. The results show that at 500 KGy dose of irradiation the Young’s modulus and tensile strength values have been enhanced in comparison with pure blend by cross-linking and the surface hardness of samples raises by increasing the clay content The samples with the clay content of 5 wt% in the matrix with 500KGy dose of irradiation have shown satisfactory thermal resistance.The irradiation at high levels has degraded the nanocomposites and an optimum dose must be employed to enhance their properties. The presence of poly(ethylene glycol) as a compatibilizer has improved the dispersion of clay layers into the matrix and has enhanced the mechanical properties and thermal resistance of nanocomposites. The presence of the clay in the matrix has increased the adsorption amount of xylene and toluene into the bulk of nanocomposites and the irradiation has decreased this capacity by the dose level.

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