scholarly journals SEM/EDX Spectrum Imaging and Statistical Analysis of a Metal/Ceramic Braze

1999 ◽  
Vol 589 ◽  
Author(s):  
Paul G. Kotula ◽  
Michael R. Keenan ◽  
Ian M. Anderson
Keyword(s):  
Electron Microscope ◽  
Statistical Analysis ◽  
Image Data ◽  
Relevant Information ◽  
Elemental Distribution ◽  
Data Set ◽  
X Ray ◽  
Metal Ceramic ◽  
Spectrum Imaging ◽  
Scanning Electron

AbstractEnergy dispersive x-ray (EDX) spectrum imaging has been performed in a scanning electron microscope (SEM) on a metal/ceramic braze to characterize the elemental distribution near the interface. Statistical methods were utilized to extract the relevant information (i.e., chemical phases and their distributions) from the spectrum image data set in a robust and unbiased way. The raw spectrum image was over 15 Mbytes (7500 spectra) while the statistical analysis resulted in five spectra and five images which describe the phases resolved above the noise level and their distribution in the microstructure

Information Extraction: Statistical Analysis to Get the Most from Spectrum Images

2000 ◽  
Vol 6 (S2) ◽  
pp. 1052-1053
Author(s):  
P. G. Kotula ◽  
M. R. Keenan
Keyword(s):  
Image Data ◽  
Relevant Information ◽  
Data Sets ◽  
Double Precision ◽  
Data Set ◽  
X Ray ◽  
Conventional Analysis ◽  
Actual Signal ◽  
Spectrum Imaging ◽  
Automated Methods

As more x-ray energy dispersive spectroscopy (EDS) manufacturers begin to offer spectrum imaging (a complete x-ray spectrum from each pixel in an image), there is a clear need for robust and automated methods for quickly extracting the relevant information from the large spectrum image data sets. A typical spectrum image may consist of 100 x 100 pixels (10000 spectra) each with 1000 channels which (when stored at double precision) is 80 Mbytes. It is clear that a large four-dimensional data set such as this cannot be viewed in its entirety and the time to analyze individual spectra by hand is prohibitive. Conventional analysis of spectrum images by mapping energy windows is useful as a first pass only for finding the elements present and only if at sufficient concentrations. Additional problems with mapping include systematic overlaps of other x-ray peaks, changes in the background shape and displaying the maps so they faithfully portray the actual signal intensity.

scholarly journals Visualizing Low Contrast Compositional Microstructures with SDD-EDS X-ray Spectrum Imaging in the Scanning Electron Microscope

2010 ◽  
Vol 16 (S2) ◽  
pp. 920-921
Author(s):  
D Newbury
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Low Contrast ◽  
X Ray ◽  
Spectrum Imaging ◽  
Scanning Electron

Extended abstract of a paper presented at Microscopy and Microanalysis 2010 in Portland, Oregon, USA, August 1 – August 5, 2010.

scholarly journals Multivariate Statistical Analysis of Low-voltage EDS Spectrum Images

1998 ◽  
Vol 4 (S2) ◽  
pp. 272-273 ◽  
Author(s):  
Ian M. Anderson
Keyword(s):  
Statistical Analysis ◽  
Multivariate Statistical Analysis ◽  
Low Voltage ◽  
Compositional Analysis ◽  
Spot Size ◽  
Multivariate Statistical ◽  
X Ray ◽  
Active Layers ◽  
Spectrum Imaging ◽  
Scanning Electron

Whereas energy-dispersive X-ray spectrometry (EDS) has been used for compositional analysis in the scanning electron microscope (SEM) for 30 years, the benefits of using low (<5 kV) operating voltages for such analyses have been explored only during the last few years. This paper couples low-voltage EDS with two other emerging areas of characterization: spectrum imaging and multivariate statistical analysis (MSA). The specimen analyzed for this study was a finished Intel Pentium processor, with the polyimide protective coating stripped o ff to expose the final active layers. Data acquisition was performed with a Philips XL30-FEG SEM operated at 2 kV and equipped with an Oxford super-ATW detector and XP3 pulse processor. The specimen was normal to the electron beam and the take-off angle for acquisition was 35°. The microscope was operated with a 150 μm diameter final aperture at spot size 6, which yielded an X-ray count rate of ∼1000 s-1.

scholarly journals Can X-ray Spectrum Imaging (XSI) Replace Backscattered Electron (BSE) Imaging for Compositional Contrast in the Scanning Electron Microscope?

2009 ◽  
Vol 15 (S2) ◽  
pp. 666-667 ◽  
Author(s):  
DE Newbury
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
X Ray ◽  
Backscattered Electron ◽  
Spectrum Imaging ◽  
Scanning Electron

Extended abstract of a paper presented at Microscopy and Microanalysis 2009 in Richmond, Virginia, USA, July 26 – July 30, 2009

X-ray micro tomography in the scanning electron microscope

1978 ◽  
Vol 36 (1) ◽  
pp. 106-107 ◽  
Author(s):  
W. Brünger
Keyword(s):  
Electron Beam ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Target Surface ◽  
The Body ◽  
X Rays ◽  
Cross Sectional ◽  
X Ray ◽  
Micro Tomography ◽  
Scanning Electron

Reconstructive tomography is a new technique in diagnostic radiology for imaging cross-sectional planes of the human body /1/. A collimated beam of X-rays is scanned through a thin slice of the body and the transmitted intensity is recorded by a detector giving a linear shadow graph or projection (see fig. 1). Many of these projections at different angles are used to reconstruct the body-layer, usually with the aid of a computer. The picture element size of present tomographic scanners is approximately 1.1 mm2.Micro tomography can be realized using the very fine X-ray source generated by the focused electron beam of a scanning electron microscope (see fig. 2). The translation of the X-ray source is done by a line scan of the electron beam on a polished target surface /2/. Projections at different angles are produced by rotating the object.During the registration of a single scan the electron beam is deflected in one direction only, while both deflections are operating in the display tube.

PHAX-SCAN: Functional integration of a Scanning Electron Microscope and an energy-dispersive x-ray analyser

1989 ◽  
Vol 47 ◽  
pp. 56-57
Author(s):  
Marc H. Peeters ◽  
Max T. Otten
Keyword(s):  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
High Speed ◽  
High Performance ◽  
Functional Integration ◽  
Energy Dispersive ◽  
X Rays ◽  
X Ray ◽  
High Speed Analysis ◽  
Scanning Electron

Over the past decades, the combination of energy-dispersive analysis of X-rays and scanning electron microscopy has proved to be a powerful tool for fast and reliable elemental characterization of a large variety of specimens. The technique has evolved rapidly from a purely qualitative characterization method to a reliable quantitative way of analysis. In the last 5 years, an increasing need for automation is observed, whereby energy-dispersive analysers control the beam and stage movement of the scanning electron microscope in order to collect digital X-ray images and perform unattended point analysis over multiple locations.The Philips High-speed Analysis of X-rays system (PHAX-Scan) makes use of the high performance dual-processor structure of the EDAX PV9900 analyser and the databus structure of the Philips series 500 scanning electron microscope to provide a highly automated, user-friendly and extremely fast microanalysis system. The software that runs on the hardware described above was specifically designed to provide the ultimate attainable speed on the system.

PENGGUNAAN TiO2 PARTIKEL NANO HASIL SINTESIS BERBASIS AIR MENGGUNAKAN METODA SOL-GEL PADA BAHAN KAPAS SEBAGAI APLIKASI UNTUK TEKSTIL ANTI UV

Arena Tekstil ◽  
2013 ◽  
Vol 28 (1) ◽  
Author(s):  
Maya Komalasari ◽  
Bambang Sunendar
Keyword(s):  
Fourier Transform ◽  
Electron Microscope ◽  
Scanning Electron Microscope ◽  
Sol Gel ◽  
Crosslinking Agent ◽  
X Ray Diffraction ◽  
Nano Tio2 ◽  
X Ray ◽  
Infra Red ◽  
Scanning Electron

Partikel nano TiO2 berbasis air dengan pH basa telah berhasil disintesis dengan menggunakan metode sol-gel dan diimobilisasi pada kain kapas dengan menggunakan kitosan sebagai zat pengikat silang. Sintesis dilakukan  dengan prekursor TiCl4 pada konsentrasi 0,3 M, 0,5 M dan 1 M, dan menggunakan templat kanji dengan proses kalsinasi pada suhu 500˚C selama 2 jam. Partikel nano TiO2 diaplikasikan ke kain kapas dengan metoda pad-dry-cure dan menggunakan kitosan sebagai crosslinking agent. Berdasarkan hasil Scanning Electron Microscope (SEM),diketahui bahwa morfologi partikel TiO2 berbentuk spherical dengan ukuran nano (kurang dari 100 nm). Karakterisasi X-Ray Diffraction (XRD) menunjukkan adanya tiga tipe struktur kristal utama, yaitu (100), (101) dan (102) dengan fasa kristal yang terbentuk adalah anatase dan rutile. Pada karakterisasi menggunakan SEM terhadap serbuk dari TiO2 yang telah diaplikasikan ke permukaan kain kapas, terlihat adanya imobilisasi partikel nano TiO2 melalui ikatan hidrogen silang dengan kitosan pada kain kapas. Hasil analisa tersebut kemudian dikonfirmasi dengan FTIR (Fourier Transform Infra Red) yang hasilnya memperlihatkan puncak serapan pada bilangan gelombang 3495 cm-1, 2546 cm-1, dan 511 cm-1,  yang masing-masing diasumsikan sebagai adanya vibrasi gugus fungsi O-H, N-H dan Ti-O-Ti. Hasil SEM menunjukkan pula bahwa kristal nano yang terbentuk diantaranya adalah fasa rutile , yang berdasarkan literatur terbukti dapatberfungsi sebagai anti UV.

Failure Analysis of Killer Defects and Yield Enhancement of Flat ROM Devices in Wafer Fabrication

2000 ◽  
Author(s):  
Y. N. Hua ◽  
Z. R. Guo ◽  
L. H. An ◽  
Shailesh Redkar
Keyword(s):  
Electron Microscope ◽  
Failure Analysis ◽  
Fault Isolation ◽  
Yield Enhancement ◽  
Wafer Fabrication ◽  
X Ray ◽  
Particle Contamination ◽  
Emission Microscopy ◽  
Microscopy Techniques ◽  
Scanning Electron

Abstract In this paper, some low yield cases in Flat ROM device (0.45 and 0.6 µm) were investigated. To find killer defects and particle contamination, KLA, bitmap and emission microscopy techniques were used in fault isolation. Reactive ion etching (RIE) and chemical delayering, 155 Wright Etch, BN+ Etch and scanning electron microscope (SEM) were used for identification and inspection of defects. In addition, energy-dispersive X-ray microanalysis (EDX) was used to determine the composition of the particle or contamination. During failure analysis, seven kinds of killer defects and three killer particles were found in Flat ROM devices. The possible root causes, mechanisms and elimination solutions of these killer defects/particles were also discussed.

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