scholarly journals Void Morphology in Polyethylene/Carbon Black Composites

1996 ◽  
Vol 461 ◽  
Author(s):  
D.W.M. Marr ◽  
M. Wartenberg ◽  
KB. Schwartz ◽  
M. M. Agamalian ◽  
G. D. Wignall

ABSTRACTA combination of small angle neutron scattering (SANS) and contrast matching techniques is used to determine the size and quantity of voids incorporated during fabrication of polyethylene/carbon black composites. The analysis used to extract void morphology from SANS data is based on the three-phase model of microcrack determination via small angle x-ray scattering (SAXS) developed by W. Wu12 and applied to particulate reinforced composites.

2012 ◽  
Vol 45 (3) ◽  
pp. 1529-1543 ◽  
Author(s):  
Huan Zhang ◽  
Arthur K. Scholz ◽  
Jordan de Crevoisier ◽  
Fabien Vion-Loisel ◽  
Gilles Besnard ◽  
...  

Langmuir ◽  
2000 ◽  
Vol 16 (13) ◽  
pp. 5588-5592 ◽  
Author(s):  
Thomas P. Rieker ◽  
Manuela Hindermann-Bischoff ◽  
Françoise Ehrburger-Dolle

2014 ◽  
Vol 576 ◽  
pp. 33-37
Author(s):  
Song Li Zhang ◽  
Zhen Kun Zhang ◽  
Yuao Zhao

The properties of in-situ (Si+Al2O3)/Al composites fabricated from Al-SiO2 reaction system are investigated by X-Ray Diffraction, Scanning Electron Microscope and Differential Scanning Calorimetry technologies. The results indicate that the Si phase is plate shaped and the Al2O3 phase is mainly round and ellipsoidal. The composite prepared by this method have performances of low density, high conductivity and small thermal expansion coefficient (<10×10-6/K) which meets the performance requirements of electronic packaging materials.


1987 ◽  
Vol 111 ◽  
Author(s):  
J Goodtsman ◽  
M. G. Phillips ◽  
H. Brumberger

AbstractThe slit-smeared intensity of X-radiation scattered from carbon-supported metal catalysts behaves as clh−1 + c2h−3 for higher h-values in the small-angle region (h+4πλ−1 sinθ, λ + X-ray wavelength,θ + half of scattering angle, c1, c2 are constants). For three-phase systems with sharp phase boundaries, uniform electron-densities in the metal and void phases, and lamellar electrondensity fluctuations in the carbon phase, the small-angle X-ray scattering (SAXS) can be described in terms of inter- and intraphase electron-density correlation functions, and can be shown to yield the observed behavior. Further assumptions are required to separate these contributions and calculate interfacial specific surfaces. SAXS measurements on Pt, Ru, Pd, and Rh/C are presented.


Langmuir ◽  
2001 ◽  
Vol 17 (2) ◽  
pp. 329-334 ◽  
Author(s):  
Françoise Ehrburger-Dolle ◽  
Manuela Hindermann-Bischoff ◽  
Frédéric Livet ◽  
Françoise Bley ◽  
Cyrille Rochas ◽  
...  

Soft Matter ◽  
2018 ◽  
Vol 14 (48) ◽  
pp. 9786-9797 ◽  
Author(s):  
Jung-Shiun Jiang ◽  
Rong-Hao Guo ◽  
Yu-Shuen Chiu ◽  
Chi-Chung Hua

The percolation behaviors of a series of high-structured carbon black (CB) pastes (CB weight fractions 10–25 wt%, ethyl cellulose as the binder, α-terpineol as the solvent) were systematically investigated using analyses of rheology and impedance spectra together with characterization via small-angle X-ray scattering (SAXS) and scanning electron microscopy (SEM).


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