Adhesion Evaluation of TiN and (Ti, Al)N Coatings on Titanium 6Al-4V

1995 ◽  
Vol 410 ◽  
Author(s):  
R. D. James ◽  
D. L. Paisley ◽  
K. A. Gruss ◽  
S. Parthasarthi ◽  
B. R. Tittmann ◽  
...  
Keyword(s):  
Adhesion Strength ◽  
High Speed ◽  
Electron Beam Evaporation ◽  
Acoustic Microscopy ◽  
Microscopy Analysis ◽  
Cathodic Arc Evaporation ◽  
Tensile Adhesion ◽  
Arc Evaporation ◽  
Cathodic Arc ◽  
Titanium Aluminum Nitride

ABSTRACTTo assess the adhesion of nitride coatings on metals, titanium 6% aluminum 4% vanadium substrates were coated with titanium nitride (TiN) using both cathodic arc and electron beam evaporation. Titanium aluminum nitride ((Ti, Al)N) was also deposited using cathodic arc evaporation. The interfaces of the coated samples were loaded in tension using a high speed shock wave which caused spallation either at the interface, in the coating or in the metal. Scanning acoustic microscopy analysis of the spalled samples detected delaminations at the interface in the samples deposited by cathodic arc evaporation. DYNA2D modeling of plate impact spallation experiments revealed the tensile adhesion strength for TiN deposited by both techniques was ≈ 2.0 GPa. The tensile adhesion strength for (Ti, Al)N was less than 1.5 GPa.

THE EFFECT OF NITROGEN GAS FLOW RATE ON THE PROPERTIES OF TiN-COATED HIGH-SPEED STEEL (HSS) USING CATHODIC ARC EVAPORATION PHYSICAL VAPOR DEPOSITION (PVD) TECHNIQUE

2005 ◽  
Vol 12 (04) ◽  
pp. 631-643 ◽  
Author(s):  
ALI MUBARAK ◽  
ESAH BINTI HAMZAH ◽  
MOHD RADZI HJ. MOHD TOFF ◽  
ABDUL HAKIM BIN HASHIM
Keyword(s):  
Flow Rate ◽  
Physical Vapor Deposition ◽  
High Speed ◽  
Gas Flow ◽  
High Speed Steel ◽  
Gas Flow Rate ◽  
Nitrogen Gas ◽  
Cathodic Arc Evaporation ◽  
Arc Evaporation ◽  
Cathodic Arc

Cathodic arc evaporation (CAE) is a widely-used technique for generating highly ionized plasma from which hard and wear resistant physical vapor deposition (PVD) coatings can be deposited. A major drawback of this technique is the emission of micrometer-sized droplets of cathode material from the arc spot, which are commonly referred to as "macroparticles." In present study, titanium nitride ( TiN ) coatings on high-speed steel (HSS) coupons were produced with a cathodic arc evaporation technique. We studied and discussed the effect of various nitrogen gas flow rates on microstructural and mechanical properties of TiN -coated HSS coupons. The coating properties investigated in this work included the surface morphology, thickness of deposited coating, adhesion between the coating and substrate, coating composition, coating crystallography, hardness and surface characterization using a field emission scanning electron microscope (FE-SEM) with energy dispersive X-ray (EDX), X-ray diffraction (XRD) with glazing incidence angle (GIA) technique, scratch tester, hardness testing machine, surface roughness tester, and atomic force microscope (AFM). An increase in the nitrogen gas flow rate showed decrease in the formation of macro-droplets in CAE PVD technique. During XRD-GIA studies, it was observed that by increasing the nitrogen gas flow rate, the main peak [1,1,1] shifted toward the lower angular position. Surface roughness decreased with an increase in nitrogen gas flow rate but was higher than the uncoated polished sample. Microhardness of TiN -coated HSS coupons showed more than two times increase in hardness than the uncoated one. Scratch tester results showed good adhesion between the coating material and substrate. Considerable improvement in the properties of TiN -deposited thin films was achieved by the strict control of all operational steps.

Surface modification of Ti–Al targets during cathodic arc evaporation

2011 ◽  
Vol 205 (21-22) ◽  
pp. 5116-5123 ◽  
Author(s):  
David Rafaja ◽  
Conrad Polzer ◽  
Gerhard Schreiber ◽  
Peter Polcik ◽  
Martin Kathrein
Keyword(s):  
Surface Modification ◽  
Cathodic Arc Evaporation ◽  
Arc Evaporation ◽  
Cathodic Arc

scholarly journals Erosion and Corrosion Behaviors of ADI Deposited TiN/TiAlN Coatings by Cathodic Arc Evaporation

2005 ◽  
Vol 46 (6) ◽  
pp. 1417-1424 ◽  
Author(s):  
Cheng-Hsun Hsu ◽  
Jung-Kai Lu ◽  
Kuei-Liang Lai ◽  
Ming-Li Chen
Keyword(s):  
Corrosion Behaviors ◽  
Cathodic Arc Evaporation ◽  
Arc Evaporation ◽  
Cathodic Arc

scholarly journals Investigation on Microblasting Applied to CrN Coatings

2016 ◽  
Vol 2016 ◽  
pp. 1-7 ◽  
Author(s):  
Lorenzo Montesano ◽  
Annalisa Pola ◽  
Marcello Gelfi ◽  
Giovina Marina La Vecchia
Keyword(s):  
Wear Behavior ◽  
Corrosion And Wear ◽  
Crn Coating ◽  
Evaporation Technique ◽  
Cathodic Arc Evaporation ◽  
Quenched And Tempered Steel ◽  
Pin On Disk ◽  
Arc Evaporation ◽  
Cathodic Arc ◽  
Crn Coatings

A microblasting treatment carried out on CrN coated samples was studied to investigate the induced effect on corrosion and wear resistance. CrN coating was deposited through Cathodic Arc Evaporation technique on quenched and tempered steel. The properties of the coating were studied by hardness measurements, scratch, potentiodynamic, and pin-on-disk tests. The results show that microblasting reduces the corrosion resistance while improving the wear behavior.

Utilization of cathodic arc evaporation for the deposition of boron nitride thin films

1997 ◽  
Vol 90 (1-2) ◽  
pp. 178-183 ◽  
Author(s):  
F. Richter ◽  
G. Krannich ◽  
J. Hahn ◽  
R. Pintaske ◽  
M. Friedrich ◽  
...  
Keyword(s):  
Thin Films ◽  
Boron Nitride ◽  
Cathodic Arc Evaporation ◽  
Arc Evaporation ◽  
Cathodic Arc
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