Deformation Mechanisms in a Proton-Irradiated Austenitic Stainless Steel

1994 ◽  
Vol 373 ◽  
Author(s):  
R.D. Carter ◽  
M. Atzmon ◽  
G.S. Was ◽  
S.M. Bruemmer

AbstractSamples of austenitic 304L stainless steel have been irradiated with 3.4 MeV protons to atotal dose of 1 dpa. The microstructure of the irradiated stainless steel has been quantified by transmission electron microscopy and shown to be similar to that found in neutron-irradiated core components. Constant extension rate tensile tests have been performed at strain rates of 3x10−7 s−1 and 3x10−8 s−1 to strains of up to 27% at 23°C and 288°C. The resulting microstructures were characterized using electron and optical microscopy. Deformation of the unirradiated material is similar to that reported by others in previous work on austenitic steels, consisting of dislocation source activation and formation of dense dislocation networks with increasing strain. In the irradiated samples tested at 288°C, deformation consists of dislocation source activation at grain boundaries punching dislocations through the grain interior to the opposing grain boundaries. The dislocations create channels that are free of radiation-produced defects and on which dislocation motion is concentrated. Dislocations in the channels pile-up at the boundaries, creating regions of highly localized stress concentration at the grain boundary. The mechanism by which this stress is relieved is still unknown. Deformation at 23°C consists of the nucleation and propagation of microtwins across the width of the grains.

Further experiments by transmission electron microscopy on thin sections of stainless steel deformed by small amounts have enabled extended dislocations to be observed directly. The arrangement and motion of whole and partial dislocations have been followed in detail. Many of the dislocations are found to have piled up against grain boundaries. Other observations include the formation of wide stacking faults, the interaction of dislocations with twin boundaries, and the formation of dislocations at thin edges of the foils. An estimate is made of the stacking-fault energy from a consideration of the stresses present, and the properties of the dislocations are found to be in agreement with those expected from a metal of low stacking-fault energy.


1987 ◽  
Vol 2 (4) ◽  
pp. 436-440 ◽  
Author(s):  
G. M. Bond ◽  
I. M. Robertson ◽  
H. K. Birnbaum

The effect of boron on the mechanism of strain transfer across grain boundaries in Ni3Al has been investigated by dynamic recording of events occurring during in-situ straining in the transmission electron microscope. Boundaries in both doped and undoped material can act as effective barriers to dislocation motion, large numbers of dislocations being incorporated into the boundary without any plastic strain occurring in the adjacent grain. In the undoped material, the grain-boundary strain is relieved by the sudden failure of the grain boundary. In the doped material the strain is relieved by the sudden generation and emission of large numbers of dislocations from the grain boundary. This effect may be understood by boron either increasing the grain-boundary cohesion or reducing the stress required to operate grain-boundary dislocation sources, rather than easing the passage of slip dislocations through the grain boundary.


Author(s):  
A. R. Pelton

Although many similarities exist in the precipitation behavior in ferritic and austenitic steels, the nucleation and growth mechanisms in these systems have eluded full comprehension. However, it is apparent that the initial clustering of substitutional and interstitial atoms can dictate the structure and orientation relationships of subsequent phases. Hence, in order to realize the benefits of these decomposition transformations, a better understanding of the incipient nucleation event is imperative. Therefore, a transmission electron microscopy study of a quenched-aged 18-10 stainless steel doped with 0.3 w/o P was undertaken as part of a more comprehensive research program. The precipitation reactions in this austenitic stainless steel were originally surveyed by Rowcliffe and Nicholson [1] and Rowcliffe and Eyre [2], These investigators observed a variety of defects ranging from vacancy defects on {100} planes at lower aging temperatures to Cr3P laths with {100} habit planes at higher aging temperatures.


2010 ◽  
Vol 24 (15n16) ◽  
pp. 2537-2542 ◽  
Author(s):  
GUOYONG WANG ◽  
ZHONGHAO JIANG ◽  
JIANSHE LIAN

A fully dense electrodeposited microcrystalline copper with nano-scale twins was synthesized by electrodeposition. The microstructure of this copper was analyzed X-ray diffractometer (XRD) and by transmission electron microscopy (TEM). The grains of mean size about 2mm were divided by high density of growth twins with mean lamellar thickness of about 90 nm. Tensile tests at different strain rates and room temperature showed that the strength increased from 379 MPa to 458 MPa with strain rate increasing from 10-5 s-1 to 0.1 s-1. The elongations to fracture were in the range of 13.6~15.5%. So this Cu has good combination of strength and ductility. The strengths are much higher than that determined by Hall-Petch relation with the same grain size, which means that twin boundaries are effective in blocking dislocation motion. The strain rate sensitivity and activation volume estimated from the flow stress versus strain curves was 0.016 and 84 b3~69b3, respectively. Such a large activation volume indicates that the deformation of this copper was controlled by dislocation process.


Author(s):  
L.E. Murr

Although it now seems to be generally recognized that grain boundaries and other interfaces are sources for dislocations, there are only scant few observations which tend to show convincing evidence for this. Murr earlier suggested that dislocation pile-ups in deformed metals and alloys (especially of low stacking-fault free energy) were primarily dislocation emission profiles, and more recent quantitative studies tend to unambiguously confirm this for uniaxial tensile deformation. Some of these features are illustrated in Fig. 1(a) and (b) which show a systematic increase in the number of dislocation profiles associated with grain boundary ledges at increasing tensile strains; observed in a Hitachi H.U. 200 F transmission electron microscope.The results shown in Fig. 1(a) and (b) were obtained as part of a systematic study of dislocation emission following the straining of 304 stainless steel sheet samples in separate, conventional tensile tests. Consequently these observations, while qualitatively and even quantitatively convincing, lack the force of direct, in-situ observations.


1996 ◽  
Vol 439 ◽  
Author(s):  
J. T. Busby ◽  
T. R. Allen ◽  
R. D. Carter ◽  
E. A. Kenik ◽  
G. S. Was

AbstractThe dose dependence of radiation-induced segregation (RIS) is investigated for proton irradiated ultra high-purity (UHP) 304L stainless steel and Fe-20Cr-24Ni. Grain boundary compositions were measured in samples irradiated with 3.2 MeV protons at 400°C to doses ranging from 0.1 to 3.0 dpa. RIS measurements were made using scanning transmission electron microscopy with energy dispersive x-ray spectroscopy (STEM/EDS) and compared to results from Auger electron spectroscopy (AES). Comparison of the dose dependence for HP-304L and Fe- 20Cr-24Ni shows that RIS is alloy specific. The approach to steady-state Cr depletion was observed to be more rapid in the alloy with higher Ni content. Fe-2OCr-24Ni reaches a steady-state Cr depletion level by 0.5 dpa, and the amount of Cr depletion in HP-304L SS is still increasing between 1.0 and 3.0 dpa. RIS in the stainless steel alloys irradiated with 3.2 MeV protons is comparable to that in neutron irradiated steels of similar composition.


2013 ◽  
Vol 762 ◽  
pp. 487-492 ◽  
Author(s):  
Laurent Waltz ◽  
Delphine Retraint ◽  
Arjen Roos

The aim of the present study is first to describe an original process, the so called duplex process, whose feature is the coupling between the well-known SMAT (Surface Mechanical Attrition Treatment) and the traditional co-rolling. The first step of this process consists of SMA-Treatment of 316L stainless steel sheets to generate nanocrystalline layers on their top surfaces according to the grain refinement mechanism of austenitic steels which is well described in the literature. During the second step, three treated sheets are co-rolled at 550°C to obtain a semi-massive nanocrystallised multilayer structure with improved mechanical strength alternating nanocrystalline, transition and coarse grain layers. The second part of this work deals with the mechanical and the microstructural characterization of the as-obtained structures. Thus, sharp nanoindentation tests performed over the cross section of the laminates coupled with Transmission Electron Microscopy (TEM) confirm the presence of nanograins after the thermomechanical treatment. In addition, the enhanced yield strength demonstrated by tensile tests correlate well with the theoretical volume fractions of nanoand transition layers. The interface cohesion between the sheets is tested by three-point bending tests and the interface bonding is evaluated by microstructural observations.


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